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    마이크로-매크로 채널 반응기
    34.
    发明公开
    마이크로-매크로 채널 반응기 有权
    微通道反应器

    公开(公告)号：KR1020110122541A

    公开(公告)日：2011-11-10

    申请号：KR1020100042107

    申请日：2010-05-04

    Applicant: 한국과학기술연구원

    Inventor： 문동주 ,  이상득 ,  임형식 ,  강정식 ,  이윤주 ,  김소정 ,  박문주 ,  허은 ,  조수현 ,  이병권

    IPC: B01J8/04 ,  B01J19/32 ,  H01M8/06 ,  C01B3/38

    CPC classification number: B01J19/0093 ,  B01J2219/00783 ,  B01J2219/00822 ,  B01J2219/00835 ,  B01J2219/00844 ,  B01J2219/00873 ,  B01J2219/00898

    Abstract: PURPOSE: A micro-macro channel reactor is provided to improve the performance per volume of the reactor and to improve the distribution, the flux increase of reactants and the efficiency of the reactor. CONSTITUTION: A micro-macro channel reactor includes an upper end plate(20), a lower end plate(60), a heat exchanging plate(30), a catalyst plate(40), and a supporting plate(50). The catalyst plate is stacked to the thermal exchanged plate. The catalyst plate includes a catalyst part(41). While reactants pass through the catalyst part, the catalytic reaction of the reactants is generated. The supporting plate is stacked to the catalyst plate and provides a flow path(52) through which the reactants pass. The heat exchanging plate, the catalyst plate, and the supporting plate are stacked between the upper end plate and the lower end plate.

    Abstract translation: 目的：提供微宏通道反应器，以提高反应器体积的性能，并改善反应物的分布，反应物的通量增加和反应器的效率。 构成：微宏通道反应器包括上端板（20），下端板（60），热交换板（30），催化剂板（40）和支撑板（50）。 催化剂板堆叠在热交换板上。 催化剂板包括催化剂部分（41）。 当反应物通过催化剂部分时，产生反应物的催化反应。 支撑板堆叠在催化剂板上，并提供反应物通过的流路（52）。 热交换板，催化剂板和支撑板堆叠在上端板和下端板之间。

    기상 연속식 촉매 공정에 의한 퍼플루오로알킬요오드의제조방법
    35.
    发明公开
    기상 연속식 촉매 공정에 의한 퍼플루오로알킬요오드의제조방법 有权
    气相色谱法制备全氟代环戊二烯的方法

    公开(公告)号：KR1020060115803A

    公开(公告)日：2006-11-10

    申请号：KR1020050038117

    申请日：2005-05-06

    Applicant: 한국과학기술연구원

    Inventor： 문동주 ,  이용준 ,  고영주 ,  김영철 ,  유계상 ,  김홍곤 ,  이상득 ,  안병성

    IPC: C07C17/07 ,  C07C17/278 ,  C07C19/16 ,  C07C17/269

    Abstract: Provided is a method for preparing perfluoroalkyl iodide through a vapor phase continuous catalytic process, which is performed under mild conditions to avoid explosion or other dangerous factors, gives a high yield of a desired product, and is amenable to mass production. The method for preparing perfluoroalkyl iodide comprises the step of performing telomerization of tetrafluoroethylene(C2F4) with perfluoroethyl iodide(C2F5I) in the presence of a catalyst. The telomerization is performed through a vapor phase continuous catalytic process in a fixed-bed tube shaped reactor, in which an alumina-supported transition metal catalyst is packed, by introducing tetrafluoroethylene and perfluoroethyl iodide in a vapor phase. The telomerization is performed under ambient pressure at a temperature of 250-450 deg.C.

    Abstract translation: 提供一种通过气相连续催化方法制备全氟烷基碘的方法，其在温和条件下进行以避免爆炸或其它危险因素，产生高产率的所需产物，并且适于批量生产。 制备全氟烷基碘的方法包括在催化剂存在下，用全氟乙基碘（C 2 F 5 I）进行四氟乙烯（C 2 F 4）调聚的步骤。 通过在气相中引入四氟乙烯和全氟乙基碘的固定床管状反应器中的气相连续催化方法进行调聚，其中填充有氧化铝负载的过渡金属催化剂。 调聚在250-450℃的环境压力下进行。

    테트라플루오로에틸렌의 이량화 반응용 촉매와 이의제조방법
    36.
    发明授权
    테트라플루오로에틸렌의 이량화 반응용 촉매와 이의제조방법 有权
    四氟乙烯二聚体催化剂及其制备方法

    公开(公告)号：KR100577692B1

    公开(公告)日：2006-05-10

    申请号：KR1020040028766

    申请日：2004-04-26

    Applicant: 한국과학기술연구원

    Inventor： 문동주 ,  이용준 ,  류종우 ,  김홍곤 ,  김훈식 ,  안병성

    IPC: C08F4/44

    Abstract: 본 발명은 테트라플루오로에틸렌의 이량화 반응용 촉매와 이의 제조방법에 관한 것으로서, 더욱 상세하게는 활성탄 촉매, 또는 활성탄에 루테늄(Ru), Ni(니켈) 및 아연(Zn)으로부터 선택된 전이금속이 담지된 활성탄 담지촉매를 제조하므로써, 테트라플루오로에틸렌(TFE)의 이량화 반응시 탄소침적 및 고분자 생성이 억제되며 전환율을 향상시킬 뿐만 아니라 불소계 고분자 수지산업에서 중요한 단량체인 헥사플루오로프로필렌(HFP)과 반도체 대체 세정제 및 소형 터보 압축기용 냉매로 사용 가능한 옥타플루오로사이클로부탄(RC318)의 선택도 제어가 가능한 테트라플루오로에틸렌의 이량화 반응용 촉매와 이의 제조방법에 관한 것이다.
    테트라플루오로에틸렌(TFE), 이량화 반응, 헥사플루오로프로필렌(HFP), 옥타플루오로사이클로부탄(RC318), 활성탄, 전이금속 촉매

    헥사플루오로프로필렌（ＨＦＰ）과옥타플루오로사이클로부탄（ＲＣ３１８）의 동시 제조방법
    38.
    发明授权
    헥사플루오로프로필렌（ＨＦＰ）과옥타플루오로사이클로부탄（ＲＣ３１８）의 동시 제조방법 失效
    （HFP）과옥타플루오로사이클로부탄（RC318）동시제조방헥

    公开(公告)号：KR100405895B1

    公开(公告)日：2003-11-14

    申请号：KR1020010008495

    申请日：2001-02-20

    Applicant: 한국과학기술연구원

    Inventor： 문동주 ,  정문조 ,  권영수 ,  안병성

    IPC: C07C23/06

    CPC classification number: C07C23/06 ,  C07C17/269 ,  C07C17/281 ,  C07C21/185

    Abstract: A method of simultaneous and selective perpararation of hexafluoropropylene and octafluorocyclebutane comprising the steps of: (a) thermally decomposing difluorochloromethane to obtain tetrafluoroethylene and then supplying the resulting tetrafluoroethylene into a bed reactor equipped with a distributor for supplying steam; and (b) supplying steam into a flow of tetrafluoroethylene supplied into the fluidized bed reactor, through a distributor for supplying steam at a certain molar ratio of tetrafluoroethylene/stream, and then performing dimerization of tetrafluoroethylene in the fluidized bed reactor under an atmospheric pressure.

    Abstract translation: 一种同时选择性地加入六氟丙烯和八氟环丁烷的方法，包括以下步骤：（a）将二氟氯甲烷热分解得到四氟乙烯，然后将所得的四氟乙烯供入装备有用于供应蒸汽的分配器的床式反应器; （b）通过用于以一定摩尔比率的四氟乙烯/料流供给蒸汽的分配器，将蒸汽供入供入流化床反应器的四氟乙烯流中，然后在大气压力下在流化床反应器中进行四氟乙烯的二聚反应。

    연료전지 자동차용 가솔린 개질촉매 및 이의 제조방법
    39.
    发明公开
    연료전지 자동차용 가솔린 개질촉매 및 이의 제조방법 失效
    燃料电池汽车用汽油改性催化剂及其制备方法

    公开(公告)号：KR1020030082762A

    公开(公告)日：2003-10-23

    申请号：KR1020020021236

    申请日：2002-04-18

    Applicant: 한국과학기술연구원

    Inventor： 문동주 ,  류종우 ,  이상득 ,  이병권 ,  안병성

    IPC: C10G11/02

    Abstract: PURPOSE: A gasoline reforming catalyst for fuel cell automobiles is provided, which has high catalyst activity, high hydrogen selectivity and low CO selectivity and has improved durability against carbon deposition or sulfur poisoning, and a preparation method of the same is provided. CONSTITUTION: The gasoline reforming catalyst for fuel cell automobiles is characterized in that the catalyst is manufactured by supporting 5 to 15 wt.% of Mg as a base catalyst constituent and two or more transition metals selected from transition metal group consisting of 2 to 15 wt.% of Ni, 0.1 to 15 wt.% of Co, 2 to 15 wt.% of Fe, 2 to 15 wt.% of Mo, 0.1 to 1.0 wt.% of Cr, 0 to 0.005 wt.% of Ti and 0 to 0.005 wt.% of Zr as active catalyst constituents onto a porous support of γ-alumina or silica-alumina(Si-Al), wherein content of the porous support is 21 to 42 wt.% based on the metal weight.

    Abstract translation: 目的：提供一种燃料电池汽车用汽油重整催化剂，其催化剂活性高，氢选择性高，CO选择性低，并且具有提高碳沉积或硫中毒的耐久性，并且提供了其制备方法。 构成：燃料电池汽车用汽油重整催化剂的特征在于，以5〜15重量％的Mg作为基础催化剂成分和2〜2重量％的过渡金属，由2〜15重量％ 的Ni，0.1〜15重量％的Co，2〜15重量％的Fe，2〜15重量％的Mo，0.1〜1.0重量％的Cr，0〜0.005重量％的Ti和 0〜0.005重量％的作为活性催化剂成分的Zr占γ-氧化铝或二氧化硅 - 氧化铝（Si-Al）的多孔载体，其中多孔载体的含量基于金属重量为21〜42重量％。

    디플루오로메탄과 1,1,1-트리플루오로에탄을 포함하는냉매 혼합물
    40.
    发明公开
    디플루오로메탄과 1,1,1-트리플루오로에탄을 포함하는냉매 혼합물 失效
    包含二氟甲磺酸和1,1,1-三氟乙烯的制冷混合物

    公开(公告)号：KR1020010074658A

    公开(公告)日：2001-08-04

    申请号：KR1020010034611

    申请日：2001-06-19

    Applicant: 한국과학기술연구원

    Inventor： 이병권 ,  임종성 ,  권영수 ,  김홍곤 ,  문동주

    IPC: C09K5/04

    CPC classification number: C09K5/045 ,  C09K2205/112 ,  C09K2205/12 ,  C09K2205/122 ,  C09K2205/43

    Abstract: PURPOSE: A refrigerant composition is provided which shows the similar performance to HCFC-22 that is currently used by additionally mixing one constituent from RC-270, HFC-227ea, HFC-245cb, HFC-236ea, R-600, HFE-134 or HFE-245 to a mixture of HFC-32 and HFC-143a. CONSTITUTION: In a composition of a refrigerant mixture which can be used instead of HCFC-22, the refrigerant mixture comprises 20 to 70 wt.% of difluoromethane (CH3F2, HFC-32) as a first constituent, 10 to 70 wt.% of 1,1,1-trifluoroethane (CH3CF3, CFC-143a) as a second constituent, and 45 wt.% or less of cyclopropane (C3H6, RC-270) or butane (C4H10, R-600) as a third constituent, wherein each of the HFC-32, HFC-143a and RC-270 comprise 20 to 40 wt.%, 30 to 70 wt.% and 30 wt.% or less respectively, and wherein each of the HFC-32, HFC-143a and R-600 comprise 30 to 50 wt.%, 38 to 70 wt.% and 12 wt.% or less respectively.

    Abstract translation: 目的：提供了一种制冷剂组合物，其显示了与通过额外混合来自RC-270，HFC-227ea，HFC-245cb，HFC-236ea，R-600，HFE-134的一种成分或目前使用的HCFC-22类似的性能 HFE-245与HFC-32和HFC-143a的混合物。 构成：在可用于代替HCFC-22的制冷剂混合物的组合物中，制冷剂混合物包含20至70重量％的作为第一组分的二氟甲烷（CH 3 F 2，HFC-32），10至70重量％ 作为第二成分的1,1,1-三氟乙烷（CH 3 CF 3，CFC-143a）和作为第三成分的环丙烷（C 3 H 6，RC-270）或丁烷（C 4 H 10，R-600）45重量％ HFC-32，HFC-143a和RC-270中的每一个分别包含20至40重量％，30至70重量％和30重量％或更少，并且其中每个HFC-32，HFC-143a和 R-600分别包含30至50重量％，38至70重量％和12重量％或更少。

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