31.
    发明专利
    未知

    公开(公告)号:FI970789A

    公开(公告)日:1997-02-25

    申请号:FI970789

    申请日:1997-02-25

    Applicant: BASF AG

    Abstract: PCT No. PCT/EP95/03230 Sec. 371 Date Feb. 18, 1997 Sec. 102(e) Date Feb. 18, 1997 PCT Filed Aug. 16, 1995 PCT Pub. No. WO96/06891 PCT Pub. Date Mar. 7, 1996 gamma -Fe2O3 pigments and Fe3O4 pigments with a particle diameter of 2 to 100 nm, a saturation magnetization above 40 nTm3/g, a remanence below 10 nTm3/g, a Cr content below 40 mg/kg of pigment, a Cu content below 40 mg/kg of pigment and C content below 100 mg/kg of pigment and aqueous suspension of these pigments. The pigments are used in aqueous suspension in the medical sector, in particular as contrast agents in magnetic resonance imaging.

    38.
    发明专利
    未知

    公开(公告)号:ES2190000T3

    公开(公告)日:2003-07-16

    申请号:ES98107122

    申请日:1998-04-20

    Applicant: BASF AG

    Abstract: Production of Si-containing Fe powder comprises thermally decomposing a gas mixture containing Fe-pentacarbonyl and a volatile Si-compound. The volatile Si-compound is a silane or organosilane, except triethylsilane and tetraethoxysilane. Also claimed is an apparatus for carrying out the process comprising: (a) a heated decomposition pipe; (b) a device for adjusting two different temperature zones; (c) a device for vaporising liquid Fe-pentacarbonyl; (d) a device for dosing and mixing gases; and (e) a separator for Si-containing Fe powder.

    39.
    发明专利
    未知

    公开(公告)号:ES2185071T3

    公开(公告)日:2003-04-16

    申请号:ES98102811

    申请日:1998-02-18

    Applicant: BASF AG

    Abstract: A process for producing finely divided phosphorus-containing iron involves gaseous phase reaction of iron pentacarbonyl with a phosphorus compound, preferably phosphine. Preferably, the reaction is carried out in the presence of ammonia at above 200 degrees C. Also claimed is a finely divided phosphorus-containing iron which consists of spherical particles with 1-10 mu mean particle diameter or of filament aggregates of spheres with 0.2-3 mu diameter. Preferably, the iron contains 0.1-50 wt.% P, less than 1 wt.% C, less than 1 wt.% N, less than 0.5 wt.% H and less than 0.1 wt.% total of other impurity elements and is produced by the above process. Further claimed is apparatus for carrying out the above process, including a heated decomposition tube, devices for producing two different temperature zones, for evaporating liquid iron pentacarbonyl and for gas dosing and mixing, and a separator for finely divided phosphorus-containing iron.

    40.
    发明专利
    未知

    公开(公告)号:ES2157619T3

    公开(公告)日:2001-08-16

    申请号:ES98102700

    申请日:1998-02-17

    Applicant: BASF AG

    Abstract: A process for producing phosphorus-containing iron powder involves heating a mixture of finely divided carbonyl iron and elemental phosphorus and pulverising the product. Preferably, a mixture of 70-99 wt.% finely divided carbonyl iron powder and 1-30 wt.% red phosphorus is heated at above 300 degrees C in an inert gas atmosphere. Also claimed is a phosphorus-containing iron powder of less than 10 mu mean particle diameter, containing 0.1-80 wt.% P, less than 1 wt.% C, less than 1 wt.% N, less than 0.5 wt.% H and less than 0.1 wt.% total of other impurity elements except oxygen.

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