公开(公告)号：ES2225764T3

公开(公告)日：2005-03-16

申请号：ES02708274

申请日：2002-01-11

Applicant: BASF AG

Inventor： MAASE MATTHIAS ,  DROEGEMUELLER MICHAEL

IPC: C07F9/38

Abstract: Procedimiento para la obtención de ácido N- fosfonometiliminodiacético mediante reacción de una sal metálica alcalina de ácido iminodiacético con tricloruro de fósforo en disolución acuosa, bajo formación de cloruro de ácido iminodiácetico, ácido fosforoso y del correspondiente cloruro metálico alcalino, subsiguiente reacción con una fuente de formaldehído, y en caso deseado obtención de ácido N-fosfonometildiaminodiacético a partir de la mezcla de reacción, caracterizado porque, durante la reacción de la sal metálica alcalina de ácido iminodiacético con tricloruro de fósforo, se elimina agua, que contiene, en caso dado, HCl, de la mezcla de reacción, hasta que se presenta una concentración en hidrocloruro de ácido iminodiacético en el intervalo de un 44 a un 55 % en peso, referido al peso de la mezcla de reacción menos el peso de cloruro metálico alcalino.

公开(公告)号：DE50200809D1

公开(公告)日：2004-09-16

申请号：DE50200809

申请日：2002-01-11

Applicant: BASF AG

Inventor： MAASE MATTHIAS ,  DROEGEMUELLER MICHAEL

IPC: C07F9/38

Abstract: The present invention relates to a process for the preparation of N-phosphonomethyliminodiacetic acid by reacting an alkali metal salt of iminodiacetic acid with phosphorus trichloride in aqueous solution with formation of the hydrochloride of iminodiacetic acid, phosphorous acid and of the corresponding alkali metal chloride, followed by reaction with a formaldehyde source and, if desired, recovery of the N-phosphonomethyliminodiacetic acid from the reaction mixture, in which water, which may comprise HCl, is removed from the reaction mixture during and/or after reacting the alkali metal salt of iminodiacetic acid with phosphorus trichloride until the concentration of iminodiacetic acid hydrochloride is at least 40% by weight, based on the weight of the reaction mixture minus the weight of alkali metal chloride. The process makes possible the preparation of N-phosphonomethyliminodiacetic acid in a simple fashion and in high yield.

公开(公告)号：DE10206117A1

公开(公告)日：2003-08-14

申请号：DE10206117

申请日：2002-02-13

Applicant: BASF AG

Inventor： NOE RALF ,  HENNE ANDREAS ,  MAASE MATTHIAS

IPC: C07F9/30 ,  C07F9/32 ,  C07F9/34 ,  C07F9/36 ,  C07F9/40 ,  C07F9/42 ,  C08F2/50 ,  C08F4/00 ,  G03F7/029 ,  C07F9/53 ,  C07F9/547 ,  C07F9/655 ,  C08G18/00 ,  C08L101/02

Abstract: The invention relates to the acyl- and bisacylphosphine derivatives according to formula (I), wherein Y represents O, S, NR3, N-OR3 or N-NR3R4, Z represents O, S, NR3, N-OR3, N-NR3R4 or a free pair of electrons, and FG represents a leaving group and the remaining groups are defined as in the description. The invention further relates to a method for the production of the inventive derivatives and to their use.

公开(公告)号：DE10206097A1

公开(公告)日：2003-08-14

申请号：DE10206097

申请日：2002-02-13

Applicant: BASF AG

Inventor： NOE RALF ,  HENNE ANDREAS ,  MAASE MATTHIAS

IPC: C07F9/32 ,  C07F9/36 ,  C07F9/46 ,  C07F9/553 ,  C07F9/655 ,  C08F2/50 ,  G03F7/029 ,  C07F9/40 ,  C07F9/53 ,  C07F9/547 ,  C07F9/6553 ,  C08G18/00 ,  C08L101/02

公开(公告)号：DE10206096A1

公开(公告)日：2003-08-14

申请号：DE10206096

申请日：2002-02-13

Applicant: BASF AG

Inventor： NOE RALF ,  BECK ERICH ,  MAASE MATTHIAS ,  HENNE ANDREAS

IPC: C07F9/32 ,  C07F9/36 ,  C07F9/40 ,  C07F9/44 ,  C07F9/59 ,  C07F9/6509 ,  C07F9/655 ,  C08F2/50 ,  C07F9/53 ,  C07F9/547 ,  C08G18/00 ,  C08L101/02

公开(公告)号：CA2473954A1

公开(公告)日：2003-07-31

申请号：CA2473954

申请日：2003-01-21

Applicant: BASF AG

Inventor： SEITZ VERENA ,  FLORES MIGUEL ,  STEGMANN VEIT ,  MAASE MATTHIAS ,  VOLLAND MARTIN ,  SIEGEL WOLFGANG ,  HALBRITTER KLAUS ,  BARTSCH MICHAEL ,  NOE RALF ,  PAPP RAINER ,  MASSONNE KLEMENS ,  BECKER MICHAEL ,  HUTTENLOCH OLIVER

IPC: C07D233/58 ,  B01J31/24 ,  C07B61/00 ,  C07B63/00 ,  C07B63/02 ,  C07C1/30 ,  C07C7/10 ,  C07C13/23 ,  C07C45/50 ,  C07C67/14 ,  C07C67/58 ,  C07C69/14 ,  C07C69/78 ,  C07C403/12 ,  C07D233/60 ,  C07D403/12 ,  C07F7/18 ,  C07F9/02 ,  C07F9/12 ,  C07F9/142 ,  C07F9/145 ,  C07F9/22 ,  C07F9/46 ,  C07F9/48 ,  C07F9/50 ,  C07F9/52 ,  C07F9/572 ,  C07F9/6503 ,  C07F9/6574 ,  C07F9/6584

Abstract: Disclosed is a method for producing aminodihalophosphines, diaminohalophosphines, triaminophosphines, phosphite diamides, aminophosphines, diaminophosphines, phosphite amide halogenides, and aminophosphine halogenides by separating an acid in the presence of an auxiliary base. Said auxiliary base b) forms a salt with an acid, which is liquid at temperatures at which the valuable product is not significantly decomposed during separation of the liquid salt, and c) the salt of the auxiliary base and the valuable product or the solution of the valuable product form two immiscible phases in a suitable solvent.

公开(公告)号：CA2566011C

公开(公告)日：2013-07-23

申请号：CA2566011

申请日：2005-05-27

Applicant: BASF AG

Inventor： SZARVAS LASZLO ,  MASSONNE KLEMENS ,  MAASE MATTHIAS ,  OFTRING ALFRED

IPC: C07C209/68 ,  C07C209/02 ,  C07C211/63 ,  C07C213/08 ,  C07C215/40 ,  C07D295/02 ,  C07D295/023 ,  C07D295/037

Abstract: The inventive method for producing quaternary ammonium compounds consists in reacting compounds containing an sp3 hybridised nitrogen atom with dialkyl sulphate or trialkyl phosphate and in exposing the thus obtained ammonium compound to an ion-exchange.

公开(公告)号：CA2473839C

公开(公告)日：2011-11-01

申请号：CA2473839

申请日：2003-01-21

Applicant: BASF AG

Inventor： MAASE MATTHIAS ,  MASSONNE KLEMENS ,  HALBRITTER KLAUS ,  NOE RALF ,  BARTSCH MICHAEL ,  SIEGEL WOLFGANG ,  STEGMANN VEIT ,  FLORES MIGUEL ,  HUTTENLOCH OLIVER ,  BECKER MICHAEL

IPC: C07B63/00 ,  C07D233/58 ,  B01J31/24 ,  C07B61/00 ,  C07B63/02 ,  C07C1/30 ,  C07C7/10 ,  C07C13/23 ,  C07C45/50 ,  C07C67/14 ,  C07C67/58 ,  C07C69/14 ,  C07C69/78 ,  C07C403/12 ,  C07D233/60 ,  C07D403/12 ,  C07F7/18 ,  C07F9/02 ,  C07F9/12 ,  C07F9/142 ,  C07F9/145 ,  C07F9/22 ,  C07F9/46 ,  C07F9/48 ,  C07F9/50 ,  C07F9/52 ,  C07F9/572 ,  C07F9/6503 ,  C07F9/6574 ,  C07F9/6584

Abstract: Disclosed is a method for separating acids from chemical reaction mixtures by means of an auxiliary base. Said auxiliary base b) forms a salt with the acid, which is liquid at temperatures at which the valuable product is not significantly decomposed during separation, and c) the salt of the auxiliary base and the valuable product or the solution of the valuable product form two immiscible fluid phases in a suitable solvent.

公开(公告)号：NZ562169A

公开(公告)日：2011-01-28

申请号：NZ56216906

申请日：2006-04-12

Applicant: BASF AG

Inventor： MAASE MATTHIAS ,  STEGMANN VEIT

IPC: C08B1/00 ,  C08J3/09 ,  C08L1/02

Abstract: Disclosed is a solution comprising cellulose, an ionic liquid as a solvent and 6 - 30% by weight of a nitrogen-comprising base, based on the total weight of the solution, wherein the ionic liquid comprises at least one cation of formula (IVe), wherein; R is unbranched and unsubstituted alkyl; R1 is unbranched or branched alkyl which is unsubstituted; and the radicals R2 to R4 are each, independently of one another, hydrogen, or unbranched or branched alkyl which is unsubstituted; and wherein the nitrogen-comprising base is an imidazole compound which is derived from the quaternary compounds of the formula (IVe), with the radical R forming the quaternary compounds not being present and R1-R4 independently of one another, are as defined above.

公开(公告)号：BRPI0609083A2

公开(公告)日：2010-11-16

申请号：BRPI0609083

申请日：2006-04-07

Applicant: BASF AG

Inventor： MAASE MATTHIAS ,  STEGMANN VEIT

IPC: C08B1/00 ,  C08L1/02

Abstract: Solution comprises cellulose and an ionic liquid containing anions and cations as solvent, where the cation exhibits at least one atom of nitrogen, oxygen, sulfur and phosphorus, which is present in protonated form. An independent claim is included for the preparation of the solution.