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    VERFAHREN ZUR HERSTELLUNG VON HALOGENE ENTHALTENDEN ORGANISCHEN PHOSPHORVERBINDUNGEN
    72.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON HALOGENE ENTHALTENDEN ORGANISCHEN PHOSPHORVERBINDUNGEN 有权
    用于生产含HALOGENE有机磷剂

    公开(公告)号：EP2044092A1

    公开(公告)日：2009-04-08

    申请号：EP07787009.5

    申请日：2007-07-03

    Applicant: BASF SE

    Inventor： BAUMANN, Robert ,  AECHTNER, Tobias ,  SIEGEL, Wolfgang ,  LUYKEN, Hermann ,  PFAB, Peter ,  SCHEIDEL, Jens ,  LEITNER, Andreas ,  GLASS, Andreas

    IPC: C07F9/48

    CPC classification number: C07F9/4891 ,  C07F9/4875

    Abstract: The invention relates to a method for producing compounds of general formula XPR2(OR1) (Ia), wherein X represents chlorine, bromine or iodine and R1 represents an organic radical, by reacting compounds of general formula X2PR2 (II), wherein X has the above-mentioned meaning and R2 represents an organic radical, with compounds of general formula R1OH (III), wherein R1 has the above-mentioned meaning, to form a mixture IV, wherein a) the secondary reaction is carried out at a temperature of between 50 to 240°C and at a pressure of 0,001 to 0,9 bar, b) from the mixture IV, the compounds (Ia) are separated from the compounds PR2(OR1)2 (Ib) and optionally from the compounds II and c) compounds (Ib) and optionally non-reacted compounds II are guided back to the synthesis step.

    PROCESS FOR MAKING MIXTURES OF ENANTIOMERS, AND MIXTURES OF ENANTIOMERS
    76.
    发明公开
    PROCESS FOR MAKING MIXTURES OF ENANTIOMERS, AND MIXTURES OF ENANTIOMERS 审中-公开
    用于制造混合物的混合物的过程以及混合物的混合物

    公开(公告)号：EP3268348A1

    公开(公告)日：2018-01-17

    申请号：EP16707147.1

    申请日：2016-03-02

    Applicant: BASF SE

    Inventor： FRANZKE, Constanze ,  REINOSO GARCIA, Marta ,  BAUMANN, Robert ,  GREINDL, Thomas

    IPC: C07C229/16 ,  C07C229/24 ,  C11D3/33

    CPC classification number: C11D3/33 ,  C07C227/18 ,  C07C253/00 ,  C07C253/06 ,  C07C255/25 ,  C07C229/16 ,  C07C229/24

    Abstract: Process for preparation of a mixture of methyl glycine diacetic acid (MGDA) or its respective mono-, di-, trialkali metal salt or its respective mono-, di- or tri-ammonium salt or mixtures thereof, and glutamic acid diacetic acid (GLDA) or its respective mono-, di-, tri-, or tetra-alkali metal or mono-, di-, tri- or tetra-ammonium salt or mixtures thereof, wherein said process com-prises the steps of: (a) dissolution in water of (a1) alanine in its L- or D-enantiomeric form or its respective monoalkali metal salt or mixtures thereof, and (a2) glutamic acid as L- or D-enantiomer or its respective mono-, or dialkali metal or mixtures thereof, wherein the molar ratio of alanine to glutamic acid is in the range of from 1:9 to 9:1, (b) converting the mixture obtained in step (a) with formaldehyde and hydrocyanic acid or alkali metal cyanide to the corresponding dinitriles, (c) saponification of the dinitriles resulting from step (b).

    VERFAHREN ZUR KONTINUIERLICHEN HERSTELLUNG VON ADIPODINITRIL
    77.
    发明公开
    VERFAHREN ZUR KONTINUIERLICHEN HERSTELLUNG VON ADIPODINITRIL 审中-公开

    公开(公告)号：EP3194361A1

    公开(公告)日：2017-07-26

    申请号：EP15770475.0

    申请日：2015-09-15

    Applicant: BASF SE

    Inventor： FISCHER, Rolf-Hartmuth ,  BAUMANN, Robert ,  WLOKA, Veronika ,  LUYKEN, Hermann

    IPC: C07C253/10 ,  C07C253/30 ,  C07C255/04 ,  C07C255/07

    CPC classification number: C07C253/30 ,  C07C253/10 ,  Y02P20/127 ,  C07C255/04 ,  C07C255/07

    Abstract: A method is described for continuous production of adiponitrile by hydrocyanation of 3-pentenenitrile in which a) 3-pentenenitrile is hydrocyanized to yield a reaction discharge which contains adiponitrile, b) in a work-up 1 of the reaction discharge of the reactor R1, a mixture containing cis-2-methyl-2-butenenitrile and cis-2-pentenenitrile is separated as a top product in a first distillation device, c) the mixture containing cis-2-methyl-2-butenenitrile and cis-2-pentenenitrile from step b) is continuously isomerized in a reactor R2 in the presence of aluminum oxide as catalyst to a product mixture containing 3-pentenenitrile, d) in a work-up 2, cis-2-methyl-2-butenenitrile is separated and discharged as top product from the reaction discharge of reactor R2 in a distillation device.

    Abstract translation: 描述了一种通过3-戊烯腈的氢氰化连续生产己二腈的方法，其中a）将3-戊烯腈氢氰化以产生含己二腈的反应排出物，b）在反应器R1的反应排出物的后处理1中， 在第一蒸馏装置中将含有顺式-2-甲基-2-丁烯腈和顺式-2-戊烯腈的混合物作为塔顶产物分离，c）将含有顺式-2-甲基-2-丁烯腈和顺式-2-戊烯腈 步骤b）在反应器R2中在作为催化剂的氧化铝存在下连续异构化为含3-戊烯腈的产物混合物，d）在后处理2中分离并排出顺式-2-甲基-2-丁烯腈 作为蒸馏装置中反应器R2的反应排出的顶部产物。

    Verfahren zur kontinuierlichen Herstellung von Adipodinitril
    79.
    发明公开
    Verfahren zur kontinuierlichen Herstellung von Adipodinitril 审中-公开
    一种用于连续生产己二腈的过程

    公开(公告)号：EP2998290A1

    公开(公告)日：2016-03-23

    申请号：EP14184965.3

    申请日：2014-09-16

    Applicant: BASF SE

    Inventor： FISCHER, Rolf-Hartmuth ,  BAUMANN, Robert ,  WLOKA, Veronika ,  LUYKEN, Hermann

    IPC: C07C253/10 ,  C07C253/30 ,  C07C255/04 ,  C07C255/07

    CPC classification number: C07C253/30 ,  C07C253/10 ,  Y02P20/127 ,  C07C255/04 ,  C07C255/07

    Abstract: Beschrieben wird ein Verfahren zur kontinuierlichen Herstellung von Adipodinitril durch Hydrocyanierung von 3-Pentennnitril, bei dem man
    a) 3-Pentennitril hydrocyaniert unter Erhalt eines Reaktionsaustrags, der Adipodinitril enthält,
    b) in einer Aufarbeitung 1 aus dem Reaktionsaustrag des Reaktors R1 in einer ersten Destillationsvorrichtung als Kopfprodukt ein Gemisch enthaltend cis-2-Methyl-2-butennitril und cis-2-Pentennitril abtrennt,
    c) das Gemisch enthaltend cis-2-Methyl-2-butennitril und cis-2-Pentennitril aus Schritt b) in einem Reaktor R2 in Gegenwart von Aluminiumoxid als Katalysator kontinuierlich zu einem 3-Pentennitril enthaltenden Produktgemisch isomerisiert,
    d) aus dem Reaktionsaustrag des Reaktors R2 in einer Aufarbeitung 2 in einer Destillationsvorrichtung cis-2-Methyl-2-butennitril als Kopfprodukt abtrennt und ausschleust.

    Abstract translation: 公开了一种用于通过3-戊烯腈的氢氰化连续制备己二腈的方法，其中a）3-戊烯腈氢氰化，得到含有反应产物混合物己二腈，b）以在第一蒸馏装置的工作器1从反应器R1的反应流出物 作为塔顶产物含有分离的混合物顺式-2-甲基-2-丁烯腈和顺式-2-戊烯腈，c）含顺式-2-甲基-2-丁烯腈和来自步骤b顺式-2-戊烯腈）在反应器R2中的混合物 异构化在氧化铝的存在下连续地导入催化剂的产物混合物，d）从所述反应器R2的反应流出物中的后处理2在蒸馏设备中顺式-2-甲基-2-丁烯腈作为顶部产物和ausschleust分离含有3-戊烯腈 - 。

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