公开(公告)号：ZA9007565B

公开(公告)日：1992-05-27

申请号：ZA9007565

申请日：1990-09-21

Applicant: BASF AG

Inventor： MAYWALD VOLKER ,  VOLKER MAYWALD ,  FREUND WOLFGANG ,  WOLFGANG FREUND ,  HAMPRECHT GERHARD ,  GERHARD HAMPRECHT ,  KUEKENHOEHNER THOMAS ,  THOMAS KUEKENHOEHNER ,  PLATH PETER ,  PETER PLATH ,  WUERZER BRUNO ,  BRUNO WUERZER ,  WESTPHALEN KARL-OTTO ,  KARL-OTTO WESTPHALEN

IPC: A01N43/80 ,  C07D261/18 ,  C07D275/02 ,  C07D275/03 ,  C07D ,  A01N

CPC classification number: C07D275/03 ,  A01N43/80 ,  C07D261/18

公开(公告)号：BR9004803A

公开(公告)日：1991-09-10

申请号：BR9004803

申请日：1990-09-25

Applicant: BASF AG

Inventor： DITRICH KLAUS ,  MAYWALD VOLKER ,  HAMPRECHT GERHARD ,  HARREUS ALBRECHT ,  WUERZER BRUNO ,  WESTPHALEN KARL-OTTO

IPC: C07D277/20 ,  A01N43/74 ,  A01N43/76 ,  A01N43/78 ,  C07D263/34 ,  C07D263/36 ,  C07D263/46 ,  C07D277/56 ,  C07D413/04 ,  C07D413/12 ,  C07D413/14 ,  C07D417/04 ,  C07D417/12 ,  C07D417/14 ,  C07D413/02 ,  C07D417/02

Abstract: Oxazole- or thiazolecarboxamides of the formulae Ia and Ib in which the substituents have the following meanings: X is oxygen or sulphur; R is hydrogen; halogen; optionally substituted C1-C6-alkyl, benzyl, cycloalkyl, alkenyl, alkynyl, phenyl, phenoxy or phenylthio; alkoxy; alkylthio; haloalkoxy; haloalkylthio; or an optionally substituted 5- or 6-membered heterocyclic radical; R is formyl, 4,5-dihydrooxazol-2-yl or the radical -COYR ; Y is oxygen or sulphur; R is hydrogen; cycloalkyl; optionally substituted alkyl, phenyl, benzyl, alkenyl, cycloalkenyl or alkynyl; an optionally substituted 5- or 6-membered heterocyclic radical; phthalimido; tetrahydrophthalimido; succinimido; maleimido; a cation equivalent; or a radical -N=CR R ; R and R are hydrogen; alkyl; cycloalkyl; phenyl; furyl or together are a methylene chain having 4 to 7 chain members; R is hydrogen or optionally substituted alkyl or cycloalkyl; R is hydroxyl or alkoxy; optionally substituted alkyl, cycloalkyl, alkenyl, alkynyl, phenyl or naphthyl; an optionally substituted 5- or 6-membered heterocyclic radical; or R and R together are a radical of the structure -(CH2)n-Yp-(CH2)q-, where n and q are 1, 2 or 3, p is 0 or 1 and Y is oxygen, sulphur or N-methyl, or form the radical of the formula -(CH2)3-CO-, and their environmentally compatible salts, where in the formula Ib X does not represent sulphur when R represents 3-pyridyl, R represents CO2CH2CH3 or R represents hydrogen, and where in the formula Ia X does not represent sulphur or R does not represent thien-2-yl when YR represents OH and R represents hydrogen and R represents methyl, processes for their preparation, and herbicidal agents containing the compounds of the formula Ia or Ib as active substances.

公开(公告)号：HUT55371A

公开(公告)日：1991-05-28

申请号：HU630690

申请日：1990-10-02

Applicant: BASF AG

Inventor： KUEKENHOEHNER THOMAS ,  FREUND WOLFGANG ,  MAYWALD VOLKER ,  GOETZ NORBERT

IPC: C07D261/18 ,  C07D413/04

公开(公告)号：BRPI0316844B1

公开(公告)日：2016-03-08

申请号：BR0316844

申请日：2003-12-01

Applicant: BASF AG

Inventor： WEVERS JAN HENDRIK ,  KEIL MICHAEL ,  HOFFMANN NICO ,  VOGELBACHER UWE JOSEF ,  MAYWALD VOLKER

IPC: C07C45/81 ,  C07C45/46 ,  C07C49/84 ,  C07C51/363 ,  C07C51/60

Abstract: "processo para preparar benzofenonas". um processo para preparar benzofenonas de fórmula i, em que x pode ser cloro, hidroxila, metoxi ou c~ 1~-c~ 6~-alquilcarbonilóxi, e y pode ser cloro ou bromo, reagindo um cloreto ácido de fórmula ii em que x e y são como definidos acima com 3,4,5-trimetoxitolueno, que compreende efetuar a reação na presença de a) um hidrocarboneto aromático como um diluente e b) de 0,0 1 a 0,2 % molar de um catalisador contendo ferro, com base no cloreto ácido, c) em temperatura entre 60 c e o ponto de ebulição do diluente usado.

公开(公告)号：CA2508714C

公开(公告)日：2011-04-05

申请号：CA2508714

申请日：2003-12-01

Applicant: BASF AG

Inventor： MAYWALD VOLKER ,  HOFFMANN NICO ,  KEIL MICHAEL ,  VOGELBACHER UWE JOSEF ,  WEVERS JAN HENDRIK

IPC: C07C45/46 ,  C07C45/81 ,  C07C49/84 ,  C07C51/363 ,  C07C51/60

Abstract: Disclosed is a method for producing benzophenones of formula I, wherein X can represent chlorine, hydroxy, methoxy, or C1-C6 alkylcarbonyloxy while Y represents chlorine or bromine, by reacting an acid chloride of formula II, wherein X and Y have the meaning mentioned above, with 3,4,5-trimethoxytoluene. The inventive method is characterized by the fact that the reaction is carried out in the presence of a) an aromatic hydrocarbon as a thinner, and b) 0.01 to 0.2 mole percent of an iron catalyst, the percentage being in relation to the acid chloride, c) at a temperature ranging between 60oC and the boiling point of the respective thinner.

公开(公告)号：BRPI0608712A2

公开(公告)日：2010-12-07

申请号：BRPI0608712

申请日：2006-03-16

Applicant: BASF AG

Inventor： SMIDT SEBASTIAN PEER ,  BUDICH MANUEL ,  MAYWALD VOLKER ,  KEIL MICHAEL ,  WOLF BERND ,  RACK MICHAEL

IPC: C07C51/08 ,  C07C17/23 ,  C07C17/363 ,  C07C25/13 ,  C07C63/70

Abstract: The invention relates to a method for producing 5-halo-2,4,6-tifluoroisophthalic acid of formula (I), wherein X represents F, Cl, Br, or I, by hydrolysis of 5-halo-2,4,6-trifluoroisophthalodinitrile of formula (II). Said invention is characterised in that in a first step, isophthalodinitrile (II) or a solution containing isophthalodinitrile (II) is reacted with a concentrated sulphuric acid at room temperature in order to form a 5-halo-2,4,6-trifluoroisophthalodiamide of general formula (III), and is, subsequently, heated and in a second step, isophthalic acid (I) is produced after additional heating and addition of water.

公开(公告)号：AU2003294750B2

公开(公告)日：2010-04-01

申请号：AU2003294750

申请日：2003-12-01

Applicant: BASF AG

Inventor： KEIL MICHAEL ,  WEVERS JAN HENDRIK ,  HOFFMANN NICO ,  VOGELBACHER UWE JOSEF ,  MAYWALD VOLKER

IPC: C07C45/46 ,  C07C45/81 ,  C07C51/363 ,  C07C51/60

Abstract: A process for preparing benzophenones of the formula I, where X may be chlorine, hydroxyl, methoxy or C 1 -C 6 -alkylcarbonyloxy, and Y may be chlorine or bromine, by reacting an acid chloride of the formula II where X and Y are as defined above with 3,4,5-trimethoxytoluene, which comprises carrying out the reaction in the presence of a) an aromatic hydrocarbon as a diluent and b) from 0.01 to 0.2 mol % of an iron catalyst, based on the acid chloride, c) at a temperature between 60° C. and the boiling point of the particular diluent.

公开(公告)号：SK286367B6

公开(公告)日：2008-08-05

申请号：SK6792001

申请日：1999-11-06

Applicant: BASF AG

Inventor： MAYWALD VOLKER ,  STEINMETZ ADRIAN ,  RACK MICHAEL ,  GOTZ NORBERT ,  GOTZ ROLAND ,  HENKELMANN JOCHEM ,  BECKER HEIKE ,  AISCAR BAYETO JUAN JOSE

IPC: C07D231/00 ,  C07D231/20

Abstract: It is described a method for producing 1-substituted 5- and/or 3-hydroxypyrazoles of formulas (I) and (II), wherein R1 represents C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkinyl, C3-C6-cycloalkyl or C1-C4-alkoxy, whereby these groups can be substituted by halogen, C1-C4-alkoxy, phenoxy, C1-C6-alkoxycarbonyl, C1-C6-alkylthiocarbonyl or a cyclic ring system with 3-14 ring atoms, by reacting a 3-alkoxyacrylic acid alkyl ester of formula (III), wherein R2, R3 independently mean C1-C6-alkyl or C3-C6-cycloalky, with a hydrazine of formula (IV), wherein R1 has the above cited meaning, a) at a pH value of 6-11 to form 5-hydroxypyrazoles of formula (I), or b) at a pH value of 11-14 to form 3-hydroxypyrazoles of formula (II).

公开(公告)号：DE50106537D1

公开(公告)日：2005-07-21

申请号：DE50106537

申请日：2001-09-12

Applicant: BASF AG

Inventor： MAYWALD VOLKER ,  KOBER REINER ,  HEIMANN FRANK ,  OBERDORF KLAUS ,  HARREUS ALBRECHT ,  GOETZ NORBERT ,  VOSSEN MARCUS

IPC: A01N43/14 ,  A01N43/18 ,  C07D335/02

Abstract: A process for preparing 2-{1-[2-(4-chlorophenoxy)propoxyimino]-butyl}-3-hydroxy-5-(tetrahydrothiopyran-3-yl)cyclohex-2-enone lithium salt by reacting the corresponding acid 2-{1-[2-(4-chlorophenoxy)-propoxyimino]butyl}-3-hydroxy-5-(tetrahydrothiopyran-3-yl)-cyclohex-2-enone and lithium hydroxide and the isolation of the lithium salt are described. Here, it is advantageous to use a solvent mixture which comprises methanol and at least one aromatic hydrocarbon and to remove at least some of the solvent prior to the isolation. It is particularly preferred to dissolve the acid in an aromatic hydrocarbon, preferably toluene, and to use a methanolic lithium hydroxide solution. The product, which can be obtained in a more efficient manner by this process, furthermore has considerable advantages with respect to formulation.

公开(公告)号：CA2508714A1

公开(公告)日：2004-07-01

申请号：CA2508714

申请日：2003-12-01

Applicant: BASF AG

Inventor： VOGELBACHER UWE JOSEF ,  MAYWALD VOLKER ,  HOFFMANN NICO ,  KEIL MICHAEL ,  WEVERS JAN HENDRIK

IPC: C07C45/46 ,  C07C45/81 ,  C07C51/363 ,  C07C51/60 ,  C07C49/84

Abstract: Disclosed is a method for producing benzophenones of formula I, wherein X ca n represent chlorine, hydroxy, methoxy, or C1-C6 alkylcarbonyloxy while Y represents chlorine or bromine, by reacting an acid chloride of formula II, wherein X and Y have the meaning mentioned above, with 3,4,5- trimethoxytoluene. The inventive method is characterized by the fact that th e reaction is carried out in the presence of a) an aromatic hydrocarbon as a thinner, and b) 0.01 to 0.2 mole percent of an iron catalyst, the percentage being in relation to the acid chloride, c) at a temperature ranging between 60oC and the boiling point of the respective thinner.