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公开(公告)号:US6350906B2
公开(公告)日:2002-02-26
申请号:US36291299
申请日:1999-07-29
Applicant: BASF AG
Inventor: MACHHAMMER OTTO , ZEHNER PETER , DEBERDT FILIP
Abstract: A process for the continuous recovery of (meth)acrylic acid from the reaction gases of a catalytic gas-phase oxidation by (I) absorption in a high-boiling solvent, (II) isolation of the (meth)acrylic acid from the mixture with the solvent and, if required, further purification of the (meth)acrylic acid isolated, (III) purification of the solvent and (IV) recycling of the purified solvent to absorption stage (I) is proposed, the temperature in each process stage not exceeding 155° C., in particular 140° C., preferably 120° C.
Abstract translation: (I)在高沸点溶剂中的吸收从催化气相氧化的反应气体中连续回收(甲基)丙烯酸的方法,(II)从(甲基)丙烯酸与混合物的分离 溶剂,并且如果需要,进一步纯化分离的(甲基)丙烯酸,(III)溶剂的纯化和(IV)将纯化溶剂再循环至吸收级(I),每个过程阶段的温度不是 超过155℃,特别是140℃,优选120℃。
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公开(公告)号:WO2004014845A8
公开(公告)日:2005-03-03
申请号:PCT/EP0308430
申请日:2003-07-30
Applicant: BASF AG , WALSDORFF CHRISTIAN , FIENE MARTIN , STROEFER ECKHARD , HARTH KLAUS , JACOBS JAN D , DEBERDT FILIP
Inventor: WALSDORFF CHRISTIAN , FIENE MARTIN , STROEFER ECKHARD , HARTH KLAUS , JACOBS JAN D , DEBERDT FILIP
IPC: B01J23/46 , C01B7/04 , C07C263/10 , C07C263/20 , C25B1/26
CPC classification number: C01B7/04 , B01J23/462 , C07C263/10 , C07C263/20 , Y02P20/125 , C07C265/14
Abstract: The invention relates to a method for producing organic isocyanates, said method consisting of the following steps: (a) a first partial quantity of chlorine containing
Abstract translation: 一种用于包括(a)提供氯的第一部分量的步骤有机异氰酸酯的制备过程中,第一部分量的氯具有游离和结合溴和<400ppm的碘的含量; (B)提供氯的第二部分量; (C)氯的第一和第二部分的量与一氧化碳以形成光气反应; (D)从步骤(c)光气与一种或多种伯胺,以形成相应的异氰酸酯和氯化氢反应; (E)中分离和任选地在步骤(d)异氰酸酯形成清洁的; 氯化氢形成(F)中分离和任选地在步骤(d)清洁的; (G)催化氧化至少步骤(e)将分离的氯化氢与氧氯的一部分; (H)分离出形成在步骤(g)中的氯和使用至少分离的氯的子集,如步骤氯的第二部分量(b)中。
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公开(公告)号:AT382600T
公开(公告)日:2008-01-15
申请号:AT04740321
申请日:2004-06-25
Applicant: BASF AG
Inventor: STEINBRENNER ULRICH , STROEFER ECKHARD , SOHN MARTIN , QUASCHNING VERONIKA , MOEHWALD HELMUT , THIELE KAI , DEBERDT FILIP , JACOBS JAN , PINKOS ROLF
IPC: C07C209/78 , C07C209/86 , C07C211/50
Abstract: A process is described for preparing diaminodiarylmethanes comprising the steps a) reacting an aromatic amine with a methylene-donating agent in the presence of homogeneous acid catalysts, b) removing the homogeneous acid catalyst from the reaction product, c) working up and purifying the reaction product, which comprises removing the homogeneous acid catalyst from the reaction mixture by adsorption to a solid adsorbent.
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公开(公告)号:DE102004026095A1
公开(公告)日:2005-12-15
申请号:DE102004026095
申请日:2004-05-25
Applicant: BASF AG
Inventor: WOELFERT ANDREAS , PALLASCH HANS-JUERGEN , STROEFER ECKHARD , PENZEL ULRICH , DEBERDT FILIP
IPC: C07C263/10 , C07C265/12 , C07C265/14
Abstract: A process for the preparation of isocyanates by reacting amines with phosgene, the phosgene-containing stream of starting materials (i) being substantially free of isocyanates and (ii) having a mass content of hydrogen chloride (referred to below as HCl) of less than 0.4% by mass, and a production plant for carrying out the process according to the invention.
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公开(公告)号:PT1575908E
公开(公告)日:2006-12-29
申请号:PT03785813
申请日:2003-12-13
Applicant: BASF AG
Inventor: PENZEL ULRICH , MARTIN SOHN DR , ABEEL PETER VAN DEN , JACOBS JAN D , STROEFER ECKHARD , NEVEJANS FILIP , PALLASCH HANS-JUERGEN , DEBERDT FILIP , MACKENROTH WOLFGANG
IPC: C07C263/20
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公开(公告)号:AT335721T
公开(公告)日:2006-09-15
申请号:AT03785813
申请日:2003-12-13
Applicant: BASF AG
Inventor: SOHN MARTIN , STROEFER ECKHARD , NEVEJANS FILIP , PENZEL ULRICH , PALLASCH HANS-JUERGEN , VAN DEN ABEEL PETER , DEBERDT FILIP , JACOBS JAN D , MACKENROTH WOLFGANG
IPC: C07C263/20
Abstract: The invention relates to a process for preparing isocyanates by reaction of amines with phosgene in the presence of inert organic solvents in a reactor and subsequent work-up of the reaction mixture leaving the reactor, wherein the solvent is separated off in a two-stage or multistage, preferably two-stage, distillation process in which the solvent is separated off at a pressure of 0.1-15 bar in a first apparatus and at 1-900 mbar in a second apparatus or further apparatuses, with the heat of condensation of the solvent vapor from the first apparatus being used for partial or complete vaporization of solvent in the second apparatus.
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公开(公告)号:AU2003294849A1
公开(公告)日:2004-07-14
申请号:AU2003294849
申请日:2003-12-13
Applicant: BASF AG
Inventor: SOHN MARTIN , STROEFER ECKHARD , NEVEJANS FILIP , PENZEL ULRICH , PALLASCH HANS-JURGEN , ABEEL PETER VAN DEN , DEBERDT FILIP , JACOBS JAN D , MACKENROTH WOLFGANG
IPC: C07C263/20
Abstract: The invention relates to a process for preparing isocyanates by reaction of amines with phosgene in the presence of inert organic solvents in a reactor and subsequent work-up of the reaction mixture leaving the reactor, wherein the solvent is separated off in a two-stage or multistage, preferably two-stage, distillation process in which the solvent is separated off at a pressure of 0.1-15 bar in a first apparatus and at 1-900 mbar in a second apparatus or further apparatuses, with the heat of condensation of the solvent vapor from the first apparatus being used for partial or complete vaporization of solvent in the second apparatus.
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公开(公告)号:BRPI0511449B1
公开(公告)日:2015-06-09
申请号:BRPI0511449
申请日:2005-05-21
Applicant: BASF AG
Inventor: WÖLFERT ANDREAS , PALLASCH HANS-JÜRGEN , STROEFER ECKHARD , PENZEL ULRICH , DEBERDT FILIP
IPC: C07C263/10 , C07C265/12 , C07C265/14
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公开(公告)号:PT1646604E
公开(公告)日:2008-02-11
申请号:PT04740321
申请日:2004-06-25
Applicant: BASF AG
Inventor: PINKOS ROLF , STROEFER ECKHARD , DEBERDT FILIP , STEINBRENNER ULRICH , SOHN MARTIN , QUASCHNING VERONIKA , MOEHWALD HELMUT , THIELE KAI , JACOBS JAN D
IPC: C07C209/78 , C07C209/86 , C07C211/50
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公开(公告)号:BRPI0511449A
公开(公告)日:2007-12-26
申请号:BRPI0511449
申请日:2005-05-21
Applicant: BASF AG
Inventor: WOELFERT ANDREAS , PALLASCH HANS-JUERGEN , STROEFER ECKHARD , PENZEL ULRICH , DEBERDT FILIP
IPC: C07C263/10 , C07C265/12 , C07C265/14
Abstract: A process for the preparation of isocyanates by reacting amines with phosgene, the phosgene-containing stream of starting materials (i) being substantially free of isocyanates and (ii) having a mass content of hydrogen chloride (referred to below as HCl) of less than 0.4% by mass, and a production plant for carrying out the process according to the invention.
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