Continuous recovery of (meth)acrylic acid
    1.
    发明授权
    Continuous recovery of (meth)acrylic acid 失效
    连续回收(甲基)丙烯酸

    公开(公告)号:US6350906B2

    公开(公告)日:2002-02-26

    申请号:US36291299

    申请日:1999-07-29

    Applicant: BASF AG

    CPC classification number: C07C51/42 C07C57/04

    Abstract: A process for the continuous recovery of (meth)acrylic acid from the reaction gases of a catalytic gas-phase oxidation by (I) absorption in a high-boiling solvent, (II) isolation of the (meth)acrylic acid from the mixture with the solvent and, if required, further purification of the (meth)acrylic acid isolated, (III) purification of the solvent and (IV) recycling of the purified solvent to absorption stage (I) is proposed, the temperature in each process stage not exceeding 155° C., in particular 140° C., preferably 120° C.

    Abstract translation: (I)在高沸点溶剂中的吸收从催化气相氧化的反应气体中连续回收(甲基)丙烯酸的方法,(II)从(甲基)丙烯酸与混合物的分离 溶剂,并且如果需要,进一步纯化分离的(甲基)丙烯酸,(III)溶剂的纯化和(IV)将纯化溶剂再循环至吸收级(I),每个过程阶段的温度不是 超过155℃,特别是140℃,优选120℃。

    4.
    发明专利
    未知

    公开(公告)号:DE102004026095A1

    公开(公告)日:2005-12-15

    申请号:DE102004026095

    申请日:2004-05-25

    Applicant: BASF AG

    Abstract: A process for the preparation of isocyanates by reacting amines with phosgene, the phosgene-containing stream of starting materials (i) being substantially free of isocyanates and (ii) having a mass content of hydrogen chloride (referred to below as HCl) of less than 0.4% by mass, and a production plant for carrying out the process according to the invention.

    6.
    发明专利
    未知

    公开(公告)号:AT335721T

    公开(公告)日:2006-09-15

    申请号:AT03785813

    申请日:2003-12-13

    Applicant: BASF AG

    Abstract: The invention relates to a process for preparing isocyanates by reaction of amines with phosgene in the presence of inert organic solvents in a reactor and subsequent work-up of the reaction mixture leaving the reactor, wherein the solvent is separated off in a two-stage or multistage, preferably two-stage, distillation process in which the solvent is separated off at a pressure of 0.1-15 bar in a first apparatus and at 1-900 mbar in a second apparatus or further apparatuses, with the heat of condensation of the solvent vapor from the first apparatus being used for partial or complete vaporization of solvent in the second apparatus.

    10.
    发明专利
    未知

    公开(公告)号:BRPI0511449A

    公开(公告)日:2007-12-26

    申请号:BRPI0511449

    申请日:2005-05-21

    Applicant: BASF AG

    Abstract: A process for the preparation of isocyanates by reacting amines with phosgene, the phosgene-containing stream of starting materials (i) being substantially free of isocyanates and (ii) having a mass content of hydrogen chloride (referred to below as HCl) of less than 0.4% by mass, and a production plant for carrying out the process according to the invention.

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