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    2.
    发明专利
    未知

    公开(公告)号：AT359989T

    公开(公告)日：2007-05-15

    申请号：AT02027069

    申请日：2002-12-03

    Applicant: BASF AG

    Inventor： GOEBBEL HANS-GEORG DR ,  GERLACH TILL DR ,  FUNKE FRANK DR ,  EBEL KLAUS DR ,  UNVERRICHT SIGNE DR ,  KAIBEL GERD DR

    IPC: C07B61/00 ,  C07C29/141 ,  C07C33/03

    Abstract: Selective hydrogenation of alpha , beta -ethylenically unsaturated aldehydes (II) to corresponding unsaturated alcohols (I) comprises performing reaction in a reactor containing a liquid phase, suspended catalyst and optionally a gas phase, The liquid phase and gas phase (if present) are supplied to the reactor through a device (A) with openings or channels having a hydraulic diameter of 0.5-2 mm. Selective hydrogenation of unsaturated aldehydes of formula R R C=CR -CHO (II) to corresponding alcohols of formula R R C=CR -CH2OH (I) comprises performing the reaction in a reactor containing a liquid phase, suspended catalyst and optionally a gas phase. The liquid phase and optionally the gas phase are supplied to the reactor through a device (A) with openings or channels having a hydraulic diameter of 0.5-2 mm. R , R = H, optionally substituted mono- or polyunsaturated 1-20C alkyl (sic; some of the groups exemplified in the disclosure are saturated), optionally substituted aryl or optionally substituted heterocyclyl; R = H or 1-4C alkyl.

    3.
    发明专利
    未知

    公开(公告)号：DE50208766D1

    公开(公告)日：2007-01-04

    申请号：DE50208766

    申请日：2002-12-03

    Applicant: BASF AG

    Inventor： HAAKE MATHIAS DR ,  GERLACH TILL DR ,  FUNKE FRANK DR

    IPC: C07C29/141 ,  C07C29/145 ,  C07B61/00 ,  C07C33/02 ,  C07C33/025

    Abstract: Selective liquid hydrogenation of carbonyl compounds to the corresponding alcohols is effected using a platinum/zinc oxide catalyst. Selective liquid hydrogenation of carbonyl compounds of formula R C(O)R (I) to the corresponding alcohols of formula R C(OH)R (II) is effected using a platinum/zinc oxide catalyst. R and R = H, optionally mono- or poly-unsaturated, optionally substituted 1-20C alkyl, optionally substituted aryl or optionally substituted heterocyclic group.

    PROCEDIMIENTO PARA LA HIDROGENACION SELECTIVA DE COMPUESTOS CARBONILADOS, OLEFINICAMENTE INSATURADOS.
    4.
    发明专利
    PROCEDIMIENTO PARA LA HIDROGENACION SELECTIVA DE COMPUESTOS CARBONILADOS, OLEFINICAMENTE INSATURADOS. 未知

    公开(公告)号：ES2283501T3

    公开(公告)日：2007-11-01

    申请号：ES02027069

    申请日：2002-12-03

    Applicant: BASF AG

    Inventor： GOBBEL HANS-GEORG DR ,  GERLACH TILL DR ,  FUNKE FRANK DR ,  EBEL KLAUS DR ,  UNVERRICHT SIGNE DR ,  KAIBEL GERD DR

    IPC: C07C29/141 ,  C07B61/00 ,  C07C33/03

    Abstract: Procedimiento para la hidrogenación selectiva de compuestos carbonilados a, a-insaturados de la fórmula general I, en la que R1, R2 pueden ser respectivamente iguales o diferentes, independientemente entre sí y significan hidrógeno o un resto alquilo con 1 hasta 20 átomos de carbono mono o poliinsaturado, de cadena lineal o de cadena ramificada, en caso dado substituido, un resto arilo substituido en caso dado o un grupo heterocíclico substituido en caso dado, significando los restos, en tanto en cuanto estén presentes, restos metilo, etilo, propilo, i-propilo, butilo, t-butilo, flúor, cloro, bromo, yodo, nitro o amino, y R3 significa hidrógeno o un resto alquilo con 1 hasta 4 átomos de carbono, para dar los correspondientes alcoholes insaturados de la fórmula general II en la que R1, R2 y R3 tienen el significado anteriormente indicado, en un reactor, que contiene una fase líquida, en la que está suspendido, al menos, un catalizador y que puede contener, en caso dado, una fase gaseosa adicional, caracterizado porque la fase líquida y, en caso dado, la fase gaseosa se conducen en el reactor por medio de un dispositivo con orificios o con canales, cuyo diámetro hidráulico está comprendido entre 0, 5 y 20 mm, y porque se emplean partículas suspendidas del catalizador con un tamaño medio de grano desde 0, 0001 hasta 2 mm.

    7.
    发明专利
    未知

    公开(公告)号：AT359992T

    公开(公告)日：2007-05-15

    申请号：AT01130515

    申请日：2001-12-21

    Applicant: BASF AG

    Inventor： PFEFFINGER JOACHIM ,  HUELLMANN MICHAEL DR ,  HOEHN ARTHUR DR ,  FUNKE FRANK DR ,  OHLBACH FRANK DR ,  GERLACH TILL DR

    IPC: C07B61/00 ,  C07C209/48 ,  C07C211/05 ,  C07C211/11 ,  C07C211/14

    Abstract: Secondary amines of the formula (II)whereX is a C1-20-alkyl, C2-20-alkenyl or C3-8-cycloalkyl group which may be unsubstituted or substituted by C1-20-alkyl, C3-8-cycloalkyl, C4-20-alkylcycloalkyl, C4-20-cycoalkylalkyl, C2-20-alkoxyalkyl, C6-14-aryl, C7-20-alkylaryl, C7-20-aralkyl, C1-20-alkoxy, hydroxy, C1-20-hydroxyalkyl, amino, C1-20-alkylamino, C2-20-dialkylamino, C2-12-alkenylamino, C3-8-cycloalkylamino, arylamino, diarylamino, aryl-C1-8-alkylamino, halogen, mercapto, C2-20-alkenyloxy, C3-8-cycloalkoxy, aryloxy and/or C2-8-alkoxycarbonyl,are prepared by reacting nitriles of the formula (III)with hydrogen at from 20 to 250° C. and pressures of from 60 to 350 bar in the presence of an Rh-containing catalyst comprising from 0.1 to 5% by weight, based on the total weight of the catalyst, of Rh on a support to give mixtures of primary amines of the formula (I)and secondary amines of the formula (II)and returning at least part of the primary amines separated from the mixtures obtained to the reaction.

    8.
    发明专利
    未知

    公开(公告)号：AT346030T

    公开(公告)日：2006-12-15

    申请号：AT02027071

    申请日：2002-12-03

    Applicant: BASF AG

    Inventor： HAAKE MATHIAS DR ,  GERLACH TILL DR ,  FUNKE FRANK DR

    IPC: C07C29/145 ,  C07B61/00 ,  C07C29/141 ,  C07C33/02 ,  C07C33/025

    Abstract: Selective liquid hydrogenation of carbonyl compounds to the corresponding alcohols is effected using a platinum/zinc oxide catalyst. Selective liquid hydrogenation of carbonyl compounds of formula R C(O)R (I) to the corresponding alcohols of formula R C(OH)R (II) is effected using a platinum/zinc oxide catalyst. R and R = H, optionally mono- or poly-unsaturated, optionally substituted 1-20C alkyl, optionally substituted aryl or optionally substituted heterocyclic group.

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