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1.发明申请METHOD FOR PRODUCING IPDA WITH A HIGH CIS/TRANS ISOMER RATIO BY DISTILLATION 审中-公开蒸馏工艺用于生产IPDA具有高顺/反式异构体
公开(公告)号：WO2004024668A3
公开(公告)日：2004-10-14
申请号：PCT/EP0308831
申请日：2003-08-08
Applicant: BASF AG , FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUEDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED
Inventor： FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUEDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED
IPC: C07C209/86 , B01D3/14 , C07C209/84 , C07C211/36
CPC classification number: B01D3/141 , B01D3/146 , C07C209/84 , Y10S203/20 , C07C211/36
Abstract: The invention relates to a method for obtaining 3-aminomethyl-3,5,5-trimethyl cyclohexylamine (isophorone diamine, IPDA) with a cis/trans isomer ratio of at least 73/27 by fractional distillation. Said method comprises the following steps: a) preparation of IPDA with a cis/trans isomer ratio /=73/27 and iv) an IPDA fraction with a cis/trans isomer ratio
Abstract translation: 本发明涉及一种用于具有顺式/反式异构体中的至少73/27通过分馏，其包括以下步骤比率回收3-氨基甲基-3,5,5-三甲基环己胺（异佛尔酮二胺，IPDA）：a）提供 具有IPDA顺/反异构体比率<73/27; b）将IPDA送入蒸馏塔的中间区域具有内部和在一定温度下在该蒸馏塔中蒸馏IPDA。 为5〜300℃，为10〜2000毫巴的压力; c）任选地进一步纯化由步骤b）通过在至少一个另外的塔中蒸馏得到IPDA; 其中，所述步骤b）和c）需要在步骤a中使用的IPDA的分离）放置到至少五个级分IA）至iv）：IA）erunreinigungen低于一小部分的有机比例反式IPDA沸腾V，IB）的含水部分 一小部分比反式IPDA沸点杂质下，ii）除了顺式IPDA沸点杂质更高的馏分，iii）具有> = 73/27的顺/反异构体比率的IPDA馏分和iv）具有顺式的IPDA馏分 式/反式异构体比率<= 66/34。
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公开(公告)号：AT343561T
公开(公告)日：2006-11-15
申请号：AT03794858
申请日：2003-08-08
Applicant: BASF AG
Inventor： FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUEDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED
IPC: C07C209/86 , B01D3/14 , C07C209/84 , C07C211/36
Abstract: Recovery of isophoronediamine (IPDA) comprises preparation of IPDA having a cis/trans isomer ratio of less than 73/27 and separation into at least 5 fractions by distillation including an IPDA fraction having a cis/trans ratio of greater than 73/27 and a fraction having a cis/trans ratio of less than 66/34. A process for the recovery of 3-aminomethyl-3,5,5-trimethylcyclohexylamine (isophoronediamine, IPDA) comprises; (a) preparation of IPDA having a cis/trans isomer ratio of less than 73/27; (b) introduction of IPDA to the middle region of a distillation column having inserts and distillation of IPDA at 5-300 degreesC and 10-2000 mbar; (c) optionally further purification of the IPDA from (b) by distillation in at least one further column whereby the IPDA from step (b) and (c) are separated into at least 5 fractions comprising an organic fraction (1a) containing impurities having a lower b. pt. than trans-IPDA, an aqueous fraction (1b) containing impurities having a lower b. pt. than trans-IPDA, a fraction (2) containing impurities having a higher b. pt. than cis-IPDA, an IPDA fraction (3) having a cis/trans ratio of greater than 73/27 and an IPDA fraction (4) having a cis/trans ratio of less than 66/34.
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公开(公告)号：AT217860T
公开(公告)日：2002-06-15
申请号：AT98906939
申请日：1998-02-09
Applicant: BASF AG
Inventor： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
Abstract: PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.
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公开(公告)号：AU744848B2
公开(公告)日：2002-03-07
申请号：AU6296298
申请日：1998-02-09
Applicant: BASF AG
Inventor： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
Abstract: PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.
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公开(公告)号：NO992550A
公开(公告)日：1999-11-29
申请号：NO992550
申请日：1999-05-27
Applicant: BASF AG
Inventor： MATTMANN WOLFGANG , KOENIG JOSEF , JONES SIMON A , EDINGER CHRISTINE , EDINGER MICHAEL , HEMMER GERD
CPC classification number: F23G5/006 , B01D53/34 , B01D53/75 , B01D53/77 , F23G2209/14
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Patent Agency Ranking
公开(公告)号：AU6296298A
公开(公告)日：1998-09-09
申请号：AU6296298
申请日：1998-02-09
Applicant: BASF AG
Inventor： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
Abstract: PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.
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公开(公告)号：ES2290546T3
公开(公告)日：2008-02-16
申请号：ES03790870
申请日：2003-08-06
Applicant: BASF AG
Inventor： FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD
IPC: C07C209/54 , C07C209/84 , C07B61/00 , C07C29/68 , C07C209/82 , C07C209/86 , C07C211/36
Abstract: Un proceso para preparar 3-aminometil-3, 5, 5-trimetilciclohexilamina (isoforonodiamina, IPDA) sustancialmente pura que tiene una proporción de isómeros cis/trans de por lo menos 73/27, y comprende la siguientes etapas: a) suministrar IPDA crudo que tenga una proporción de isómeros cis/trans de
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公开(公告)号：AU2003258591A1
公开(公告)日：2004-04-30
申请号：AU2003258591
申请日：2003-08-08
Applicant: BASF AG
Inventor： HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED , FUNKE FRANK , HILL THOMAS , WATZDORF JOBST RUDIGER VON , MATTMANN WOLFGANG , HARDER WOLFGANG
IPC: C07C209/86 , B01D3/14 , C07C209/84 , C07C211/36 , C07C209/00
Abstract: Recovery of isophoronediamine (IPDA) comprises preparation of IPDA having a cis/trans isomer ratio of less than 73/27 and separation into at least 5 fractions by distillation including an IPDA fraction having a cis/trans ratio of greater than 73/27 and a fraction having a cis/trans ratio of less than 66/34. A process for the recovery of 3-aminomethyl-3,5,5-trimethylcyclohexylamine (isophoronediamine, IPDA) comprises; (a) preparation of IPDA having a cis/trans isomer ratio of less than 73/27; (b) introduction of IPDA to the middle region of a distillation column having inserts and distillation of IPDA at 5-300 degreesC and 10-2000 mbar; (c) optionally further purification of the IPDA from (b) by distillation in at least one further column whereby the IPDA from step (b) and (c) are separated into at least 5 fractions comprising an organic fraction (1a) containing impurities having a lower b. pt. than trans-IPDA, an aqueous fraction (1b) containing impurities having a lower b. pt. than trans-IPDA, a fraction (2) containing impurities having a higher b. pt. than cis-IPDA, an IPDA fraction (3) having a cis/trans ratio of greater than 73/27 and an IPDA fraction (4) having a cis/trans ratio of less than 66/34.
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公开(公告)号：BR9807583A
公开(公告)日：2000-03-21
申请号：BR9807583
申请日：1998-02-09
Applicant: BASF AG
Inventor： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
Abstract: PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.
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公开(公告)号：DE19823899A1
公开(公告)日：1999-12-02
申请号：DE19823899
申请日：1998-05-28
Applicant: BASF AG
Inventor： MATTMANN WOLFGANG , KOENIG JOSEF , JONES SIMON A , EDINGER CHRISTINE , HEMMER GERD
Abstract: A tanker (I) is washed with high pressure water (1) with the effluent liquid passing to storage/disposal (II), and any displaced vapors being pumped away by a pump (III) via a water disentrainment device (IV) and fed into a combustion chamber (V) from where combustion products are cooled through a heat recovery unit (VI) before being washed with alkaline solution in a scrubber (VII) and discharged to the atmosphere via a stack (VIII). A tanker (I), in a cleaning station, is washed with high pressure water (1), optionally containing detergents, with the effluent liquid passing to storage/disposal (II), and any displaced vapors, etc. being pumped away by a pump (III) via a water disentrainment device (IV) and fed into a combustion chamber (V) maintained at 800-1200 deg C. The combustion products from the furnace (V) are cooled through a heat recovery unit (VI) before being washed with alkaline solution in a scrubber (VII) and discharged to atmosphere via a stack (VIII). The vapor pump may be a liquid ring pump or a fan, etc.
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