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公开(公告)号:DE50111991D1
公开(公告)日:2007-03-22
申请号:DE50111991
申请日:2001-05-16
Applicant: BASF AG
Inventor: BADER JOACHIM , BECHTOLSHEIMER HANS-HEINRICH , BRUCKER ARMIN , DOCKNER TONI , IFFLAND GABRIELE , KLINK HANS , MARTIN STEFAN , MOHR JUERGEN , MUGRAUER HANS-MARTIN
Abstract: Alkali metal ions are separated off from alkoxylates containing alkali metal ions by a process comprising:a) dilution of the alkali metal-containing alkoxylate with an inert solvent,b) treatment of the alkali metal-containing solution of the alkoxylate with a cationic exchanger in order to obtain a substantially alkali metal-free solution of the alkoxylate, andc) removal of the solvent from the substantially alkali metal-free solution of the alkoxylate in order to obtain a substantially alkali metal-free and substantially solvent-free alkoxylate.
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公开(公告)号:AU6229301A
公开(公告)日:2001-11-26
申请号:AU6229301
申请日:2001-05-16
Applicant: BASF AG
Inventor: BADER JOACHIM , BECHTOLSHEIMER HANS-HEINRICH , BRUCKER ARMIN , DOCKNER TONI , IFFLAND GABRIELE , KLINK HANS , MARTIN STEFAN , MOHR JURGEN , MUGRAUER HANS-MARTIN
Abstract: Alkali metal ions are separated off from alkoxylates containing alkali metal ions by a process comprising:a) dilution of the alkali metal-containing alkoxylate with an inert solvent,b) treatment of the alkali metal-containing solution of the alkoxylate with a cationic exchanger in order to obtain a substantially alkali metal-free solution of the alkoxylate, andc) removal of the solvent from the substantially alkali metal-free solution of the alkoxylate in order to obtain a substantially alkali metal-free and substantially solvent-free alkoxylate.
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公开(公告)号:DE10024313A1
公开(公告)日:2001-11-22
申请号:DE10024313
申请日:2000-05-17
Applicant: BASF AG
Inventor: BADER JOACHIM , BECHTOLSHEIMER HANS-HEINRICH , BRUCKER ARMIN , DOCKNER TONI , IFFLAND GABRIELE , KLINK HANS , MARTIN STEFAN , MOHR JUERGEN , MUGRAUER HANS-MARTIN
Abstract: Removal of alkali metal ions from alkoxylates. Removal of alkali metal ions from alkoxylates involves: (i) diluting the alkoxylate with an inert solvent; (ii) contacting the solution with an cation-exchanger; and (iii) removing the solvent.
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公开(公告)号:DE10054462B4
公开(公告)日:2005-02-17
申请号:DE10054462
申请日:2000-11-03
Applicant: BASF AG
Inventor: KAMMEL ULRICH , BENFER REGINA , LENZ WALTER , MUGRAUER HANS-MARTIN , SPIEGLER WOLFGANG , ZEHNER PETER , ZIPPLIES MATTHIAS , FLORY KLAUS
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公开(公告)号:DE10054462A1
公开(公告)日:2002-06-06
申请号:DE10054462
申请日:2000-11-03
Applicant: BASF AG
Inventor: KAMMEL ULRICH , BENFER REGINA , LENZ WALTER , MUGRAUER HANS-MARTIN , SPIEGLER WOLFGANG , ZEHNER PETER , ZIPPLIES MATTHIAS , FLORY KLAUS
Abstract: Preparation of polyalcoholates involves the steps: (a) reaction of alcohols with bases with formation of an alcoholate containing mixture, (b) preparation of the mixture in a water-free form, (1c) feeding of the mixture into a rotary reactor, (d) feeding of alkylene oxide into the reactor in a number of sites, (e) reaction of the alcoholate and/or products of reaction. Preparation of polyalcoholates involves the steps: (a) reaction of alcohols with bases with formation of an alcoholate containing mixture; (b) preparation of the mixture in a water-free form; (c) feeding of the mixture into a rotary reactor; (d) feeding of alkylene oxide into the reactor in a number of sites; (e) reaction of the alcoholate and/or products of reaction between the alcoholate and alkylene oxide into the reactor. The steps (a) to (e) are continuous, the reactor is cooled externally, and the reactor is in the form of a plate-type heat exchanger, a plate-type heat exchanger system in a container with vapor cooling, a single way tube type heat exchanger, or a multi-way tube heat exchanger.
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公开(公告)号:AT353087T
公开(公告)日:2007-02-15
申请号:AT01936367
申请日:2001-05-16
Applicant: BASF AG
Inventor: BADER JOACHIM , BECHTOLSHEIMER HANS-HEINRICH , BRUCKER ARMIN , DOCKNER TONI , IFFLAND GABRIELE , KLINK HANS , MARTIN STEFAN , MOHR JUERGEN , MUGRAUER HANS-MARTIN
Abstract: Alkali metal ions are separated off from alkoxylates containing alkali metal ions by a process comprising:a) dilution of the alkali metal-containing alkoxylate with an inert solvent,b) treatment of the alkali metal-containing solution of the alkoxylate with a cationic exchanger in order to obtain a substantially alkali metal-free solution of the alkoxylate, andc) removal of the solvent from the substantially alkali metal-free solution of the alkoxylate in order to obtain a substantially alkali metal-free and substantially solvent-free alkoxylate.
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