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    METHOD FOR PRODUCING LONG-CHAIN GLYCINE-N,N-DIACETIC ACID DERIVATIVES
    1.
    发明申请
    METHOD FOR PRODUCING LONG-CHAIN GLYCINE-N,N-DIACETIC ACID DERIVATIVES 审中-公开
    用于生产长链甘氨酸-N，N-二乙酸衍生物

    公开(公告)号：WO9910314A3

    公开(公告)日：1999-07-01

    申请号：PCT/EP9805220

    申请日：1998-08-17

    Applicant: BASF AG ,  RAHM RAINER ,  GREINDL THOMAS ,  OFTRING ALFRED ,  OETTER GUENTER ,  DETERING JUERGEN ,  BRAUN GEROLD

    Inventor： RAHM RAINER ,  GREINDL THOMAS ,  OFTRING ALFRED ,  OETTER GUENTER ,  DETERING JUERGEN ,  BRAUN GEROLD

    IPC: C07C229/08 ,  C07C229/16 ,  C07C253/00 ,  C07C255/25 ,  C07D233/72 ,  C07D233/74

    CPC classification number: C07C229/08 ,  C07C229/16 ,  C07C253/00 ,  C07C255/25

    Abstract: The invention relates to a method for producing compounds of general formula (IIb), wherein R represents C6-C30 alkyl or C6-C30 alkenyl which can also support up to 5 hydroxyl groups, formyl groups, C1-C4 alkoxy groups, phenoxy groups or C1-C4 alkoxycarbonyl groups as substituents and which can be interrupted by up to 5 non-adjacent oxygen atoms, or alkoxylate groupings of formula -(CH2)k-O-(A O)m-(A O)n - Y, wherein A and A represent 1,2 alkylene groups with 2 to 4 C-atoms, Y represents hydrogen, C1-C12 alkyl, phenyl, or C1-C4 alkoxycarbonyl, k represents the number 1, 2 or 3 and m and n each represent numbers from 0 to 50, the sum of m and n being at least 4, independently of each other. According to the inventive method, iminodiacetonitrile is reacted with aldehydes of general formula R-CHO and HCN or alkali cyanides. The method is carried out a) without using an organic solvent and in the presence of a Lewis or Bronsted acid, or b) with or without an organic solvent and in the presence of an emulsifier, or c) with or without an organic solvent and at a pressure of 1 to 40 bar.

    Abstract translation: 在对通式（IIb）的化合物的制备方法，其中R是C6至C30的烷基或C6至C30链烯基，其还携带作为取代基的最多5个羟基，甲酰基，C1至C4烷氧基，苯氧基或C1 - 承载一个至C4烷氧基羰基和可被最多5个不相邻的氧原子，或下式的烷氧基化物基团被中断 - （CH 2）CO（A <1> O）间 - （甲<2> O）N - ÿ 是，表示其中A <1>和A <2>独立地表示1,2-亚烷基基团的碳原子数为2〜4，Y是氢，C 1至C 12表示烷基，苯基或C1-C4烷氧羰基并且k 数字1，2或3，且m和n各自为从0到50，其中m的+ n之和必须至少是4，亚氨基二乙腈与通式R-CHO的醛和HCN或碱金属氰化物反应，则 方法a），而不使用有机溶剂的和在路易斯存在 或布朗斯台德酸，或者b））的使用或不使用有机溶剂的和在1至40巴，使用或不使用有机溶剂的和在乳化剂，或c的存在的范围内的压力下进行。

    3.
    发明专利
    未知

    公开(公告)号：DE59807982D1

    公开(公告)日：2003-05-22

    申请号：DE59807982

    申请日：1998-07-20

    Applicant: BASF AG

    Inventor： DETERING JUERGEN ,  BAUR RICHARD ,  BERTLEFF WERNER ,  RAHM RAINER ,  OETTER GUENTER

    IPC: C11D1/83 ,  C11D3/06 ,  C11D3/08 ,  C11D3/10 ,  C11D3/12 ,  C11D3/33 ,  C11D3/34 ,  C11D3/39 ,  C11D17/06

    Abstract: A solid textile detergent formulation comprises(A) from 1 to 30% by weight of inorganic builders based on carbonates,(B) from 0 to 12% by weight of inorganic builders based on crystalline or amorphous alumosilicates and/or crystalline or amorphous silicates,(C) from 0 to 5% by weight of inorganic builders based on phosphates,(D) from 1 to 40% by weight of one or more glycine-N,N-diacetic acid derivatives Iwhere R is an organic radical and M is hydrogen or a cation, as organic builder component,(E) from 0 to 40% by weight of anionic surfactants and(F) from 0.5 to 50% by weight of nonionic surfactants.

    5.
    发明专利
    未知

    公开(公告)号：DE19829746A1

    公开(公告)日：2000-01-05

    申请号：DE19829746

    申请日：1998-07-03

    Applicant: BASF AG

    Inventor： DETERING JUERGEN ,  BERTLEFF WERNER ,  OFTRING ALFRED ,  RAHM RAINER

    IPC: C07C229/24 ,  C07C233/47 ,  C11D1/10 ,  C11D3/33 ,  C07C227/14 ,  C07C229/26 ,  C11D1/52

    Abstract: The present invention relates to glycin-N,N-carboxylic acid derivatives of formula (I) in which R is an organic radical comprising from 3 to 30 carbon atoms and containing at least one carbonyl group in its main chain; G and G represent independently C1-C3 alkylene; x and y are 1 or 2; and M is hydrogen, an alkaline metal, an alkaline-earth metal, ammonium or substituted ammonium. The compounds of formula (I) can be used as components having surfactant and complex-building properties in textile detergent formulations.

    Compact solid laundry detergent formulation with low inorganic builder content
    6.
    发明专利
    Compact solid laundry detergent formulation with low inorganic builder content 未知

    公开(公告)号：DE19732688A1

    公开(公告)日：1999-02-04

    申请号：DE19732688

    申请日：1997-07-30

    Applicant: BASF AG

    Inventor： DETERING JUERGEN ,  BAUR RICHARD ,  BERTLEFF WERNER ,  RAHM RAINER ,  OETTER GUENTER

    IPC: C11D1/83 ,  C11D3/06 ,  C11D3/08 ,  C11D3/10 ,  C11D3/12 ,  C11D3/33 ,  C11D17/06 ,  C11D17/00

    Abstract: Solid laundry detergent formulation contains (A) 1-30 wt.% inorganic builder based on carbonate, (B) 0-12 wt.% inorganic builder based on crystalline or amorphous aluminosilicates and/or silicates, (C) 0-5 wt.% inorganic builder based on phosphate, (D) 1-40 wt.% glycine-N,N-diacetic acid derivative(s) of formula MOOC-CH(R)-N(CH2COOM)2 (I) as organic builder, (E) 0-40 wt.% anionic surfactant and (F) 0.5-50 wt.% non-ionic surfactant; in which R = (a) 1-30C alkyl or 2-30C alkenyl (which may have up to 5 hydroxyl, sulfate, sulfonate, formyl, 1-4C alkoxy, phenoxy or 1-4C alkoxycarbonyl substituents and up to 5 non-adjacent oxygen (O) and/or nitrogen (N) atoms in the chain), (b) alkoxylate of the formula -(CH2)k-O-(A O)m-(A O)n-Y, (c) phenyl-(1-20 C)-alkyl, (d) 5-6-membered (un)saturated (benzo)-heterocyclyl with up to 3 hetero-atoms selected from N, O and sulfur (S) in the ring; or (e) -A-CH(COOM)-N(CH2COOM)2; A , A = 2-4C 1,2-alkylene; Y = hydrogen (H), 1-12 C alkyl, phenyl, 1- 4 C alkoxycarbonyl or sulfo; k = 1, 2 or 3; m, n = 0-50; m+n \- 2; A = 1-12 C alkylene or a chemical bond; M = H, alkali(ne earth) metal or optionally substituted ammonium.

    10.
    发明专利
    未知

    公开(公告)号：DE59810854D1

    公开(公告)日：2004-04-01

    申请号：DE59810854

    申请日：1998-07-20

    Applicant: BASF AG

    Inventor： DETERING JUERGEN ,  BAUR RICHARD ,  BERTLEFF WERNER ,  RAHM RAINER ,  OETTER GUENTER ,  EHLE BEATE

    IPC: C11D1/10 ,  C11D1/72 ,  C11D1/83 ,  C11D3/06 ,  C11D3/08 ,  C11D3/10 ,  C11D3/12 ,  C11D3/33 ,  C11D3/39

    Abstract: The invention relates to a solid textile detergent formulation containing (A) 1-60 wt. % inorganic builders based on crystalline or amorphous aluminosilicates, crystalline or amorphous silicates, carbonates and/or phosphates, (B) 1-40 wt. % of one or several glycin-N, N-diacetic acid derivatives of formula (I), wherein R stands for an organic radical and M means hydrogen or a cation, (C) 0-6 wt. % anionic surfactants with one or several sulphate groups, one or several sulphate groups or one or two carboxylate groups and (D) 0.5-50 wt. % non ionic surfactants.

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