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1.发明申请
公开(公告)号：WO2004001102A1
公开(公告)日：2003-12-31
申请号：PCT/CA2003/000397
申请日：2003-03-20
Applicant: INTEGRAN TECHNOLOGIES INC.
Inventor： PALUMBO, Gino , BROOKS, Iain , ROBERTSON, J. , PANAGIOTOPOULOS, Konstantinos , GONZALEZ, Francisco , TOMANTSCHGER, Klaus
IPC: C25D5/02
Abstract: A process for in situ electroforming a structural reinforcing layer of selected metallic material for repairing an external surface area of a degraded section of metallic workpieces, especially of tubes and tube sections, is described. Preferably, the metal layer coatings are made of fine-grained metals, metal alloys or metal matrix composites. The plating system can be used on straight tubes, tube joints to different diameter tubes or face plates, tube elbows and other complex shapes encountered in piping systems. A suitable apparatus is assembled on or near the degraded site and is sealed in place to form the plating cell. Also described is a process for plating "patches" onto degraded areas by selective plating including brush plating.
Abstract translation: 描述了一种用于原位电铸选择的金属材料的结构增强层的方法，用于修复金属工件的退化部分，特别是管和管部分的退化部分的外表面区域。 优选地，金属层涂层由细粒金属，金属合金或金属基质复合材料制成。 电镀系统可用于直管，管接头到不同直径的管或面板，管弯头和管道系统中遇到的其他复杂形状。 将合适的装置组装在退化位置上或附近，并将其密封在适当位置以形成电镀槽。 还描述了通过包括刷镀的选择性电镀将“贴剂”电镀到降解区域上的方法。
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公开(公告)号：WO2009079745A1
公开(公告)日：2009-07-02
申请号：PCT/CA2008/001695
申请日：2008-09-25
Applicant: INTEGRAN TECHNOLOGIES INC. , TOMANTSCHGER, Klaus , HIBBARD, Glenn , PALUMBO, Gino , BROOKS, Iain , MCCREA, Johnathan , SMITH, Fred
Inventor： TOMANTSCHGER, Klaus , HIBBARD, Glenn , PALUMBO, Gino , BROOKS, Iain , MCCREA, Johnathan , SMITH, Fred
CPC classification number: C25D15/02 , C23C14/3414 , C25D1/00 , C25D1/02 , C25D1/04 , C25D5/00 , C25D5/022 , C25D5/08 , C25D5/10 , C25D5/14 , C25D5/16 , C25D5/18 , C25D7/00 , C25D15/00 , C25D17/008 , C25D21/10 , C25D21/12 , C25D21/14 , Y10T428/24612
Abstract: Variable property deposit, at least partially of fine-grained metallic material, optionally containing solid particulates dispersed therein, is disclosed. The electrodeposition conditions in a single plating cell are suitably adjusted to once or repeatedly vary at least one property in the deposit direction. In one embodiment denoted multidimension grading, property variation along the length and/or width of the deposit is also provided. Variable property metallic material deposits containing at least in part a fine-grained microstructure and variable property in the deposit direction and optionally multidimensionally, provide superior overall mechanical properties compared to monolithic fine-grained (average grain size: >20 micron) or entirely amorphous metallic material deposits.
Abstract translation: 公开了至少部分为细颗粒金属材料，任选地含有分散在其中的固体颗粒的可变性质沉积物。 适当地调整单个电镀槽中的电沉积条件一次或重复地改变沉积方向上的至少一种性质。 在一个被称为多维分级的实施例中，还提供沿着沉积物的长度和/或宽度的性质变化。 可变性金属材料沉积物至少部分地含有细晶粒微观结构和沉积方向上的可变性质，并且任选地多维地提供了与单片细粒度（平均晶粒尺寸：> 20微米）或完全非晶金属 物料存款
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3.发明申请PROCESS FOR ELECTROPLATING METALLIC AND METALL MATRIX COMPOSITE FOILS, COATINGS AND MICROCOMPONENTS 审中-公开电镀金属和金属基复合材料，涂料和微生物的方法
公开(公告)号：WO2004001100A1
公开(公告)日：2003-12-31
申请号：PCT/EP2002/007023
申请日：2002-06-25
Applicant: INTEGRAN TECHNOLOGIES, INC. , PALUMBO, Gino , BROOKS, Iain , MCCREA, Jonathan , HIBBARD, Glenn, D. , GONZALEZ, Francisco , TOMANTSCHGER, Klaus , ERB, Uwe
Inventor： PALUMBO, Gino , BROOKS, Iain , MCCREA, Jonathan , HIBBARD, Glenn, D. , GONZALEZ, Francisco , TOMANTSCHGER, Klaus , ERB, Uwe
IPC: C25D1/04
CPC classification number: C25D1/04 , C25D5/02 , C25D5/06 , C25D5/08 , C25D5/18 , C25D5/20 , C25D7/04 , C25D15/00 , C25D15/02
Abstract: The invention relates to a process for forming coatings or free-standing deposits of nano-crystalline metals, metal alloys or metal matrix composites. The process employs drum plating or selective plating processes involving pulse electrode-position and a non-stationary anode or cathode. Novel nano-crystalline metal matrix composites and micro components are disclosed as well. Also described is a process for forming micro-components with grain sizes below 1,000nm.
Abstract translation: 本发明涉及一种用于形成纳米结晶金属，金属合金或金属基质复合材料的涂层或独立沉积物的方法。 该方法采用包括脉冲电极位置和非固定阳极或阴极的鼓电镀或选择性电镀工艺。 还公开了新颖的纳米晶体金属基复合材料和微型组件。 还描述了一种用于形成粒度小于1000nm的微组件的方法。
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公开(公告)号：WO2014001401A1
公开(公告)日：2014-01-03
申请号：PCT/EP2013/063418
申请日：2013-06-26
Applicant: INTEGRAN TECHNOLOGIES INC. , BROOKS, Iain
Inventor： BROOKS, Iain , MCCREA, Jonathan , KATUGAHA, Herath , PALUMBO, Gino , PANAGIOTOPOULOS, Konstantinos , NAGARAJAN, Nandakumar , HIRMER, Gerhard
CPC classification number: C25D5/50 , B05D2201/06 , B32B15/06 , B32B15/18 , B32B15/20 , B32B25/08 , B32B27/20 , B32B2255/10 , B32B2255/205 , B32B2255/26 , B32B2262/106 , B32B2307/202 , B32B2307/702 , B32B2307/704 , B32B2307/714 , B32B2457/00 , B32B2605/00 , B32B2605/18 , C23C18/1653 , C23C18/2086 , C23C24/04 , H05K3/387 , Y10T428/31522 , Y10T428/31678
Abstract: An article of manufacture includes a substrate having an outer surface clad with a metal construct including one or more continuous metal layers, at least one of which is an amorphous layer or a microcrystalline layer having a grain size below 5000 nm. A bonding layer is provided between the substrate and the layered metallic construct so that the bonding layer is in direct contact with the substrate and with the layered metallic construct. The bonding layer is made of a substantially fully cured resin including at least 10% of a rubber. The layered metallic construct has peel strength greater than 10N/cm. Also provided is a process for making the article including coating an article outer surface with a bonding layer and a layered metallic construct. The bonding layer is substantially fully cured before the layered metal construct is bonded to the article. The coated article is annealed.
Abstract translation: 一种制品包括具有外表面的基材，该外表面包括金属构件，该金属构件包括一个或多个连续金属层，其中至少一个是非晶层或具有低于5000nm的晶粒尺寸的微晶层。 在基板和层状金属构造体之间设置粘合层，使得粘结层与基底和层状金属构件直接接触。 粘合层由包括至少10％的橡胶的基本完全固化的树脂制成。 层状金属构造物的剥离强度大于10N / cm。 还提供了一种用于制造制品的方法，包括用粘结层和层状金属构造物涂覆制品外表面。 在层状金属构造物结合到制品之前，粘合层基本上完全固化。 涂层制品退火。
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5.发明申请METHOD FOR PREPARING POLYCRYSTALLINE STRUCTURES HAVING IMPROVED MECHANICAL AND PHYSICAL PROPERTIES 审中-公开制备具有改进的机械和物理性能的多晶结构的方法
公开(公告)号：WO2009076777A1
公开(公告)日：2009-06-25
申请号：PCT/CA2008/002265
申请日：2008-12-18
Applicant: INTEGRAN TECHNOLOGIES INC. , PALUMBO, Gino , BROOKS, Iain , TOMANTSCHGER, Klaus , LIN, Peter , AUST, Karl , NAGARAJAN, Nandakumar , GONZALEZ, Francisco
Inventor： PALUMBO, Gino , BROOKS, Iain , TOMANTSCHGER, Klaus , LIN, Peter , AUST, Karl , NAGARAJAN, Nandakumar , GONZALEZ, Francisco
IPC: C25D5/50
Abstract: Polycrystalline materials are prepared by electrodeposition of a precursor material that is subsequently heat-treated to induce at least a threefold increase in the grain size of the material to yield a relatively high fraction of 'special' low Σ grain boundaries and a randomized crystallographic texture. The precursor metallic material has sufficient purity and a fine-grained microstructure (e.g., an average grain size of 4 nm to 5 µm). The resulting metallic material is suited to the fabrication of articles requiring high mechanical or physical isotropy and/or resistance to grain boundary-mediated deformation or degradation mechanisms.
Abstract translation: 通过电沉积前体材料来制备多晶材料，该前体材料随后进行热处理以诱导材料的晶粒尺寸至少增加三倍，从而产生相对较高的“特殊”低S晶界和随机晶体织构。 前体金属材料具有足够的纯度和细粒度的微观结构（例如，平均粒度为4nm至5μm）。 所得到的金属材料适于制造需要高机械或物理各向同性的物品和/或对晶界介导的变形或降解机理的抵抗力。
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Patent Agency Ranking6.发明申请
公开(公告)号：WO2006063469A1
公开(公告)日：2006-06-22
申请号：PCT/CA2005/001925
申请日：2005-12-16
Applicant: INTEGRAN TECHNOLOGIES, INC.
Inventor： PALUMBO, Gino , MCCREA, Jonathan , TOMANTSCHGER, Klaus , BROOKS, Iain , JEONG, Daehyun , LIMOGES, Dave , PANAGIOTOPOULOS, Konstantinos , ERB, Uwe
CPC classification number: C25D7/00 , A01K87/00 , A45B9/00 , A63B49/02 , A63B49/10 , A63B49/12 , A63B53/04 , A63B53/0466 , A63B53/047 , A63B53/10 , A63B53/12 , A63B59/00 , A63B59/50 , A63B60/54 , A63B2053/0416 , A63B2209/00 , A63B2209/023 , B82Y30/00 , C23C26/00 , C25D5/00 , C25D15/02 , F42B5/30 , Y10T428/12049 , Y10T428/12201 , Y10T428/12569 , Y10T428/1321 , Y10T428/24612 , Y10T428/249941 , Y10T428/31507 , Y10T428/31511 , Y10T428/31681 , Y10T428/31685 , Y10T428/31692
Abstract: Lightweight articles comprising a polymeric material at least partially coated with a fine-grained metallic material are disclosed. The fine-grained metallic material has an average grain size of 2nm to 5,000nm, a thickness between 25 micron and 5cm, and a hardness between 200VHN and 3,000 VHN. The lightweight articles are strong and ductile and exhibit high coefficients of restitution and a high stiffness and are particularly suitable for a variety of applications including aerospace and automotive parts, sporting goods, and the like.
Abstract translation: 公开了包含至少部分涂覆有细粒金属材料的聚合材料的轻质制品。 细晶金属材料的平均晶粒尺寸为2nm至5,000nm，厚度为25微米至5cm，硬度为200VHN至3,000VHN。 轻型制品是坚固的和延展性的并且表现出高的恢复系数和高刚度，并且特别适用于各种应用，包括航空航天和汽车零件，运动用品等。
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7.发明申请
公开(公告)号：WO2006063468A1
公开(公告)日：2006-06-22
申请号：PCT/CA2005/001923
申请日：2005-12-16
Applicant: INTEGRAN TECHNOLOGIES, INC.
Inventor： PALUMBO, Gino , MCCREA, Jonathan , TOMANTSCHGER, Klaus , BROOKS, Iain , JEONG, Daehyun , LIMOGES, Dave , PANAGIOTOPOULOS, Konstantinos , ERB, Uwe
CPC classification number: C25D7/00 , A01K87/00 , A45B9/00 , A63B49/02 , A63B49/10 , A63B49/12 , A63B53/04 , A63B53/10 , A63B53/12 , A63B59/00 , A63B59/50 , A63B59/70 , A63B60/54 , A63B2053/0416 , A63B2209/00 , A63B2209/02 , A63B2209/023 , B82Y30/00 , C23C24/04 , C23C28/021 , C23C28/027 , C25D5/00 , C25D7/0607 , C25D15/02 , F41H5/0457 , F42B5/30 , F42B6/04 , F42B12/80 , Y10T428/12028 , Y10T428/12063 , Y10T428/12146 , Y10T428/12292 , Y10T428/12493 , Y10T428/12535 , Y10T428/12597 , Y10T428/12674 , Y10T428/12701 , Y10T428/12708 , Y10T428/12736 , Y10T428/12743 , Y10T428/1275 , Y10T428/12757 , Y10T428/12764 , Y10T428/12778 , Y10T428/12937 , Y10T428/12972 , Y10T428/13 , Y10T428/24942 , Y10T428/256 , Y10T428/26 , Y10T428/2918 , Y10T428/2956 , Y10T428/2958 , Y10T428/2964 , Y10T428/30 , Y10T428/31678
Abstract: Fine-grained (average grain size 1nm to 1,000nm) metallic coatings optionally containing solid particulates dispersed therein are disclosed. The fine-grained metallic materials are significantly harder and stronger than conventional coatings of the same chemical composition due to Hall-Petch strengthening and have low linear coefficients of thermal expansion (CTEs). The invention provides means for matching the CTE of the fine-grained metallic coating to the one of the substrate by adjusting the composition of the alloy and/or by varying the chemistry and volume fraction of particulates embedded in the coating. The fine-grained metallic coatings are particularly suited for strong and lightweight articles, precision molds, sporting goods, automotive parts and components exposed to thermal cycling. The low CTEs and the ability to match the CTEs of the fine-grained metallic coatings with the CTEs of the substrate minimize dimensional changes during thermal cycling and prevent premature failure.
Abstract translation: 公开了细颗粒（平均晶粒尺寸1nm至1,000nm）金属涂层，其任选地含有分散在其中的固体颗粒。 由于Hall-Petch强化，细粒金属材料比同一化学成分的常规涂层显着更硬和更强，并且具有低线性热膨胀系数（CTE）。 本发明提供了通过调节合金的组成和/或通过改变嵌入涂层中的微粒的化学和体积分数来匹配细粒金属涂层的CTE与基体之一的方法。 细粒金属涂层特别适用于强而轻的制品，精密模具，运动用品，汽车零件和暴露于热循环的部件。 低CTE和将细粒金属涂层的CTE与衬底的CTE匹配的能力使热循环期间的尺寸变化最小化并防止过早失效。
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公开(公告)号：WO2006063431A1
公开(公告)日：2006-06-22
申请号：PCT/CA2005/001429
申请日：2005-09-20
Applicant: INTEGRAN TECHNOLOGIES INC.
Inventor： PALUMBO, Gino , BROOKS, Iain , PANAGIOTOPOULOS, Konstantinos , TOMANTSCHGER, Klaus , MCCREA, Jonathan , LIMOGES, David , UWE, Erb
IPC: C25D3/00
CPC classification number: C25D15/00 , A01K87/00 , A45B9/00 , A63B49/02 , A63B49/10 , A63B53/04 , A63B53/0466 , A63B53/10 , A63B53/12 , A63B59/00 , A63B59/50 , A63B59/70 , A63B60/54 , A63B2053/0416 , A63B2209/00 , A63B2209/023 , B82Y30/00 , C25D1/00 , C25D7/00 , Y02P20/582 , Y10T428/12028 , Y10T428/12493 , Y10T428/12708 , Y10T428/12778 , Y10T428/13 , Y10T428/24405 , Y10T428/24413 , Y10T428/26 , Y10T428/265 , Y10T428/31678
Abstract: Articles for automotive, aerospace, manufacturing and defence industry applications including shafts or tubes used, for example, as golf club shafts, ski and hiking poles, fishing rods or bicycle frames, skate blades and snowboards are at least partially coated with an electrodeposited metal, metal alloy or metal matrix composite coating layer. The coating layer having a quasi-isotropic microstructure, a thickness of higher than 30µm and an average grain size between 0.004µm and 10µm. The coating layer provides articles of high resilience, high yield strength, scratch and wear resistance and hardness, and appealing appearance.
Abstract translation: 用于汽车，航空航天，制造和国防工业应用的物品，包括例如用作高尔夫球杆杆，滑雪和徒步旅行杆，钓鱼竿或自行车车架，滑板和滑雪板的轴或管至少部分地涂有电沉积金属， 金属合金或金属基复合涂层。 该涂层具有准各向同性微观结构，厚度大于30μm，平均粒径在0.004μm至10μm之间。 涂层提供具有高回弹性，高屈服强度，耐划伤性，耐磨性和硬度以及吸引人的外观的制品。
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公开(公告)号：EP2220270A1
公开(公告)日：2010-08-25
申请号：EP08800385.0
申请日：2008-09-25
Applicant: Integran Technologies Inc.
Inventor： TOMANTSCHGER, Klaus , HIBBARD, Glenn , PALUMBO, Gino , BROOKS, Iain , MCCREA, Johnathan , SMITH, Fred
CPC classification number: C25D15/02 , C23C14/3414 , C25D1/00 , C25D1/02 , C25D1/04 , C25D5/00 , C25D5/022 , C25D5/08 , C25D5/10 , C25D5/14 , C25D5/16 , C25D5/18 , C25D7/00 , C25D15/00 , C25D17/008 , C25D21/10 , C25D21/12 , C25D21/14 , Y10T428/24612
Abstract: Variable property deposit, at least partially of fine-grained metallic material, optionally containing solid particulates dispersed therein, is disclosed. The electrodeposition conditions in a single plating cell are suitably adjusted to once or repeatedly vary at least one property in the deposit direction. In one embodiment denoted multidimension grading, property variation along the length and/or width of the deposit is also provided. Variable property metallic material deposits containing at least in part a fine-grained microstructure and variable property in the deposit direction and optionally multidimensionally, provide superior overall mechanical properties compared to monolithic fine-grained (average grain size: >20 micron) or entirely amorphous metallic material deposits.
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10.发明授权PROCESS FOR ELECTROPLATING METALLIC AND METALL MATRIX COMPOSITE FOILS, COATINGS AND MICROCOMPONENTS 有权电镀法金属和金属基复合薄膜，涂层和微型元件
公开(公告)号：EP1516076B1
公开(公告)日：2008-02-27
申请号：EP02754753.8
申请日：2002-06-25
Applicant: Integran Technologies Inc.
Inventor： PALUMBO, Gino , BROOKS, Iain , MCCREA, Jonathan , HIBBARD, Glenn, D. , GONZALEZ, Francisco , TOMANTSCHGER, Klaus , ERB, Uwe
CPC classification number: C25D1/04 , C25D5/02 , C25D5/06 , C25D5/08 , C25D5/18 , C25D5/20 , C25D7/04 , C25D15/00 , C25D15/02
Abstract: The invention relates to a process for forming coatings or free-standing deposits of nanocrystalline metals, metal alloys or metal matrix composites. The process employs drum plating or selective plating processes involving pulse electrodeposition and a non-stationary anode or cathode. Novel nanocrystalline metal matrix composites and micro components are disclosed as well. Also described is a process for forming micro components with grain sizes below 1,000nm.
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