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    Vaccum deposition of cationic polymer systems
    32.
    发明授权
    Vaccum deposition of cationic polymer systems 有权

    公开(公告)号：US06468595B1

    公开(公告)日：2002-10-22

    申请号：US09783926

    申请日：2001-02-13

    Applicant: Michael G. Mikhael ,  Angelo Yializis

    Inventor： Michael G. Mikhael ,  Angelo Yializis

    IPC: C23C1600

    CPC classification number: C23C14/12 ,  B05D3/068 ,  B05D3/144 ,  B05D7/04

    Abstract: A thermally-stable cationic photoinitiator capable of flash vaporization under vacuum and temperature conditions of an available flash-evaporation chamber is selected. The photoinitiator is mixed with a cation-polymerizable monomer and/or oligomer of interest and the mixture is flash evaporated and condensed in conventional manner as a film on a cold substrate. The resulting vacuum-deposited, homogeneous layer is cured with a high-energy radiation source that causes the cationic photoinitiator to liberate acidic species that catalyze the crosslinking of the monomer/oligomer compounds in its deposited film form. As a result of the homogeneous, pinhole-free nature of the vacuum deposition process, the thin-film polymer product does not suffer from the disadvantages attendant to prior-art atmospheric processes for cationically-cured polymers. In addition, because of the versatility afforded by vacuum deposition, hybrid films of such polymers with inorganic materials are also easily manufactured in-line during the same process.

    High energy density capacitor
    34.
    发明授权
    High energy density capacitor 失效
    高能量密度电容器

    公开(公告)号：US6092269A

    公开(公告)日：2000-07-25

    申请号：US45266

    申请日：1998-03-20

    Applicant: Angelo Yializis ,  Theodore A. Miller

    Inventor： Angelo Yializis ,  Theodore A. Miller

    IPC: H01G4/18 ,  H01G4/30 ,  H01G7/00

    CPC classification number: H01G4/30 ,  H01G4/18 ,  Y10T29/435

    Abstract: A high energy density, high power density capacitor having an energy density of at least about 0.5 J/cm.sup.3 is provided. The capacitor comprises a plurality of interleaved metal electrode layers separated by a polymer layer. The interleaved metal electrode layers terminate at opposite ends in a solder termination strip. The high energy density aspect of the capacitors of the invention is achieved by at least one of the following features: (a) the dielectric thickness between the interleaved metal electrode layers is a maximum of about 5 .mu.m; (b) the polymer is designed with a high dielectric constant .kappa. of at least about 3.5; (c) the metal electrode layers within the polymer layer are recessed along edges orthogonal to the solder termination strips to prevent arcing between the metal electrode layers at the edges; and (d) the resistivity of the metal electrode layers is within the range of about 10 to 500 ohms per square, or a corresponding thickness of about 200 to 30 .ANG..

    Abstract translation: 提供了具有至少约0.5J / cm 3的能量密度的高能量密度高功率密度电容器。 电容器包括由聚合物层隔开的多个交错的金属电极层。 交错的金属电极层在焊接端接条中的相对端终止。 本发明的电容器的高能量密度方面通过以下特征中的至少一个来实现：（a）交错的金属电极层之间的电介质厚度最大为约5μm; （b）聚合物被设计成具有至少约3.5的高介电常数κ; （c）聚合物层内的金属电极层沿垂直于焊料端接条的边缘凹陷，以防止金属电极层在边缘处产生电弧; 和（d）金属电极层的电阻率在约10至500欧姆/平方的范围内，或对应的厚度为约200至30纳米。

    Metal nanolaminate composite
    35.
    发明授权
    Metal nanolaminate composite 失效
    金属纳米复合材料

    公开(公告)号：US5912069A

    公开(公告)日：1999-06-15

    申请号：US769422

    申请日：1996-12-19

    Applicant: Angelo Yializis ,  Richard E. Ellwanger

    Inventor： Angelo Yializis ,  Richard E. Ellwanger

    IPC: B32B15/08 ,  B32B7/02

    CPC classification number: B32B15/08 ,  Y10T428/24942 ,  Y10T428/2495 ,  Y10T428/2982 ,  Y10T428/31504 ,  Y10T428/31678

    Abstract: Metal-polymer nanolaminate products are fabricated from a bulk nanolaminate material composed of thousands of alternating metal and polymer layers. The nanolaminate material is produced by a prior art ultra high speed vacuum nanotechnology process that forms metal layers separated by radiation cross linked multifunctional acrylate polymer materials. The polymer to metal ratio in the nanolaminate composite can be successfully controlled. The polymer chemistry in the nanolaminate can be varied to incorporate a broad range of functional groups. The nanolaminate products are safe to handle and are environmentally and chemically stable at least up to 250.degree. C. A change in polymer chemistry can be used to lower or enhance the thermal degradation point of the polymer material.

    Abstract translation: 金属聚合物纳米酸盐产品由由数千个交替的金属和聚合物层组成的体积的Naminaminate材料制成。 纳米材料通过现有技术的超高速真空纳米技术制造，其形成由辐射交联的多官能丙烯酸酯聚合物材料分离的金属层。 可以成功控制纳米复合材料中的聚合物与金属的比例。 可以改变纳米级氨基甲酸酯中的聚合物化学以掺入宽范围的官能团。 Nanolaminate产品可以安全处理，并且在至少250℃下是环境和化学稳定性的。聚合物化学的变化可用于降低或增强聚合物材料的热降解点。

    NANO-STRUCTURED DIELECTRIC COMPOSITE
    37.
    发明申请
    NANO-STRUCTURED DIELECTRIC COMPOSITE 有权
    纳米结构电介质复合材料

    公开(公告)号：US20120003449A1

    公开(公告)日：2012-01-05

    申请号：US12828146

    申请日：2010-06-30

    Applicant: Angelo Yializis ,  Gordon Goodyear

    Inventor： Angelo Yializis ,  Gordon Goodyear

    IPC: B32B5/16 ,  B05D3/06 ,  C23C16/513 ,  B32B7/02

    CPC classification number: B05D1/60 ,  B05D1/62 ,  B05D3/067 ,  B05D2201/02 ,  B32B5/16 ,  B32B7/02 ,  B32B27/16 ,  B32B27/36 ,  B32B2307/204 ,  B32B2307/418 ,  B32B2307/546 ,  B32B2307/732 ,  B32B2457/00 ,  B32B2551/00 ,  B82Y20/00 ,  G02B5/008 ,  G02B2207/101 ,  H01G4/206 ,  Y10T428/2495

    Abstract: A multilayer dielectric structure is formed by vacuum depositing two-dimensional matrices of nanoparticles embedded in polymer dielectric layers that are thicker than the effective diameter of the nanoparticles, so as to produce a void-free, structured, three-dimensional lattice of nanoparticles in a polymeric dielectric material. As a result of the continuous, repeated, and controlled deposition process, each two-dimensional matrix of nanoparticles consists of a layer of uniformly distributed particles embedded in polymer and separated from adjacent matrix layers by continuous polymer dielectric layers, thus forming a precise three-dimensional nanoparticle matrix defined by the size and density of the nanoparticles in each matrix layer and by the thickness of the polymer layers between them. The resulting structured nanodielectric exhibits very high values of dielectric constant as well as high dielectric strength.

    Abstract translation: 通过真空沉积嵌入在聚合物电介质层中的纳米颗粒的有效直径的纳米颗粒的二维矩阵形成多层介电结构，以便产生纳米颗粒的无空隙结构的三维晶格 聚合物介电材料。 作为连续，重复和控制的沉积过程的结果，纳米颗粒的每个二维矩阵由均匀分布的颗粒层嵌入聚合物中并且通过连续的聚合物介电层与相邻的基质层分离，从而形成精确的三维结构， 由每个基质层中的纳米颗粒的尺寸和密度以及它们之间的聚合物层的厚度限定的三维纳米颗粒基质。 所得到的结构化纳米介电材料具有非常高的介电常数以及高介电强度。

    COMPOSITE REFLECTIVE BARRIER
    39.
    发明申请
    COMPOSITE REFLECTIVE BARRIER 审中-公开
    复合反射障碍

    公开(公告)号：US20090041936A1

    公开(公告)日：2009-02-12

    申请号：US12250083

    申请日：2008-10-13

    Applicant: Angelo Yializis ,  James DiBattista ,  Gordon Goodyear

    Inventor： Angelo Yializis ,  James DiBattista ,  Gordon Goodyear

    IPC: C23C16/00

    CPC classification number: C23C14/022 ,  C23C14/20 ,  C23C14/562 ,  C23C14/5826 ,  C23C14/5853

    Abstract: A coated, low-emissivity aluminum film is manufactured entirely in vacuum by depositing an aluminum layer over a substrate and then immediately coating the metal layer with a very thin protective polymeric layer. The thickness of this coating is selected to minimize absorption in the 3-15 micron wavelength. In vacuum, the metal layer is coated substantially in the absence of moisture, thereby preventing the formation of hydrated oxides that promote corrosion. The aluminum layer is preferably also passivated by in-line exposure to a plasma gas containing an oxygen-bearing component. A leveling polymeric layer may also be deposited between relatively rough substrates and the aluminum layer in order to improve the reflectivity of the resulting structures.

    Abstract translation: 通过在衬底上沉积铝层，然后立即用非常薄的保护性聚合物层涂覆金属层，完全在真空中制造涂覆的低发射率铝膜。 选择该涂层的厚度以使在3-15微米波长的吸收最小化。 在真空中，基本上没有水分地涂覆金属层，从而防止形成促进腐蚀的水合氧化物。 铝层优选通过在线暴露于含有含氧组分的等离子体气体而被钝化。 为了提高所得结构的反射率，也可以在相对粗糙的基底和铝层之间沉积出均匀的聚合物层。

    Inline passivation of vacuum-deposited aluminum on web substrate
    40.
    发明申请
    Inline passivation of vacuum-deposited aluminum on web substrate 有权
    真空沉积的铝在网状基材上的在线钝化

    公开(公告)号：US20070166556A1

    公开(公告)日：2007-07-19

    申请号：US11586478

    申请日：2006-10-25

    Applicant: Angelo Yializis ,  Michael G. Mikhael

    Inventor： Angelo Yializis ,  Michael G. Mikhael

    IPC: C23C16/00 ,  H05H1/00 ,  B32B15/04 ,  B32B15/20

    CPC classification number: C23C14/022 ,  C23C14/20 ,  C23C14/562 ,  C23C14/5826 ,  C23C14/5853 ,  Y10T428/31678

    Abstract: In a continuous in-vacuum process for the manufacture of a film metallized with aluminum, the aluminum layer is exposed to a passivating agent, inline, immediately after deposition and prior to rewinding of the film onto a take-up roller. Passivation is carried out by plasma treatment in an oxidizing atmosphere (oxygen, nitrogen or others). The resulting product exhibits no peel-off problems during unwinding of the take-up roller and greatly improved corrosion resistance.

    Abstract translation: 在用于制造用铝金属化的膜的连续真空过程中，铝层在沉积之后并且在将膜重新卷绕到卷取辊上之前立即暴露于钝化剂。 钝化通过在氧化气氛（氧气，氮气或其它）中等离子体处理进行。 所得产品在卷取辊的卷绕过程中不会出现剥离问题，并且极大地改善了耐腐蚀性。

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