Abstract:
The invention relates to a method for distillative separation of triethanolamin from a substance mixture consisting of mono- di-, and triethanolamin, ethanolamin-ether and water obtainable by an ammonia and ethylene oxide reaction in a liquid phase at a high pressure and temperature consisting in distilling the substance mixture in two stages. In the first stage, a low-boiling fraction and a high-boiling fraction are withdrawn and discharged, and in the second stage, a medium-boiling fractions is distilled at a triethanolamin content >99.4 % by weight and a diethanolamin content
Abstract:
PCT No. PCT/EP97/03303 Sec. 371 Date Jan. 7, 1999 Sec. 102(e) Date Jan. 7, 1999 PCT Filed Jun. 24, 1997 PCT Pub. No. WO98/01438 PCT Pub. Date Jan. 15, 1998The disclosure is a process for preparing a phthalide of the general formula I where R1, R2, R3 and R4 are each independently of the others hydrogen, C1-C4-alkyl or C1-C4-alkoxy, by hydrogenation of a phthalic anhydride of the general formula II where R1, R2, R3 and R4 are each as defined above, with the aid of a hydrogenation catalyst, which comprises performing the hydrogenation with the aid of a nickel catalyst doped with metals of subgroup 1, subgroup 6 and/or subgroup 7 of the Periodic Table.
Abstract:
Described is the use of terminal group capped fatty acid amide alkoxylates of the formula (I): R1-CO-NH-(CH2)n-O-(AO)x-R2 in which R1 is a C5-C21 alkyl or akenyl group, R2 is a C1-C4 alkyl group, A is C2-C4 alkylene, n is 2 or 3 and x is a number from 1 to 6, as non ionic surfactants or emulsifiers in washing, cleaning or bodycare agents, as surface-active substances for applications in the electroplating field, in the photographic industry, in the transport of crude oil, in the pharmaceutical industry, in plant nutrition and in plantprotection formulations, as well as surface-active substances for use in the manufacture of emulsions, pigments and synthetic-polymer dispersions.
Abstract:
Procedimiento para la separación por destilación, continua, de trietanolamina a partir de una mezcla de productos, constituida por monoetanolamina, por dietanolamina y por trietanolamina así como por etanolamina-éter y agua, obtenida mediante la reacción, en fase líquida, de amoníaco con óxido de etileno bajo presión y a elevada temperatura, caracterizado porque la mezcla de productos se destila en dos etapas, retirándose y purgándose en la primera etapa la fracción de punto de ebullición bajo y la fracción de punto de ebullición elevado, destilándose en la segunda etapa la fracción de punto de ebullición medio con un contenido en trietanolamina > 99, 4 % en peso y con un contenido en dietanolamina
Abstract:
PCT No. PCT/EP96/02928 Sec. 371 Date Jan. 13, 1998 Sec. 102(e) Date Jan. 13, 1998 PCT Filed Jul. 4, 1996 PCT Pub. No. WO97/03946 PCT Pub. Date Feb. 6, 1997The invention relates to the preparation of organic nitrogen compounds, in particular of aminoalkanes, alkyloximes, alkylnitrones or mixtures thereof, which have only one nitrogen-functional group and no alcoholic hydroxyl groups in the molecule, from nitro-containing reaction products of polymers of C2-C6-olefins with an average degree of polymerization P=5-100 with nitrogen oxides or mixtures of nitrogen oxides and oxygen by hydrogenation of these reaction products. The invention also relates to particular mixtures of such aminoalkanes, alkyloximes and/or alkylnitrones and to individual compounds of these types themselves. The designated products are suitable as additives to fuels and lubricants.
Abstract:
PCT No. PCT/EP97/05186 Sec. 371 Date Apr. 1, 1999 Sec. 102(e) Date Apr. 1, 1999 PCT Filed Sep. 22, 1997 PCT Pub. No. WO98/14441 PCT Pub. Date Apr. 9, 1998A process for preparing phthalides of the general formula I, where R1, R2, R3 and R4 are independently hydrogen, C1-C4-alkyl or C1-C4-alkoxy, by hydrogenating phthalic anhydrides of the general formula II, where R1, R2, R3 and R4 are each as defined above, with hydrogen in the presence of suspended catalysts of the Raney type in a hydrogenation apparatus by using a mixing apparatus to mix a liquid phase, which includes the catalyst and the phthalic anhydride used and resulting phthalide, and a gas phase, which includes the hydrogenating hydrogen, comprises using the mixing apparatus to introduce a mixing intensity of at least 50 W/l into the liquid phase.