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    11.
    发明专利
    未知

    公开(公告)号：DE19523151A1

    公开(公告)日：1996-08-14

    申请号：DE19523151

    申请日：1995-06-29

    Applicant: BASF AG

    Inventor： BALKENHOHL FRIEDHELM DR ,  NUEBLING CHRISTOPH DR ,  DITRICH KLAUS DR

    IPC: C12P13/02 ,  C12P41/00 ,  C07C215/44 ,  C07C215/08 ,  C07C217/52 ,  C07C217/10 ,  C07C217/08 ,  C07C231/20 ,  C07C213/08 ,  C07C235/14 ,  C07C235/08 ,  C07B57/00

    Abstract: A process for preparing optically active primary and secondary heteroatom-substituted amines from the corresponding racemates is characterised in that (a) a racemic heteroatom-substituted amine is enantioselectively acylated in the presence of a hydrolase with an ester whose acid component bear a fluorine, nitrogen, phosphorus, oxygen or sulphur atom next to the carbonyl carbon atom; (b) the mixture of optically active heteroatom-substituted amine and optically active acylated heteroatom-substituted amine is separated in order to produce an enantiomer of the heteroatom-substituted amine; (c) the other enantiomer of the heteroatom-substituted amine is optionally extracted from the acylated heteroatom-substituted amine by amide cleavage.

    12.
    发明专利
    未知

    公开(公告)号：DE4426561A1

    公开(公告)日：1996-02-01

    申请号：DE4426561

    申请日：1994-07-27

    Applicant: BASF AG

    Inventor： DITRICH KLAUS DR ,  KRAUSE WOLFGANG DR

    IPC: B01J27/08 ,  C07B61/00 ,  C07F9/40 ,  C07F9/655

    Abstract: Prodn. of phosphonate esters of formula ACH2PO(OR1)2 (I) comprises rearrangement of phosphite esters of formula ACH2OP(OR1)2 (II) in the presence of a catalytic amt. of a halide ion source (III): A = aryl or an alpha, beta-olefinically unsatd. gp.; R1 = 1-4C alkyl or phenyl. Also claimed are phosphonate esters of formula (Ia) and (Ib).

    13.
    发明专利
    未知

    公开(公告)号：DE4419517A1

    公开(公告)日：1995-12-07

    申请号：DE4419517

    申请日：1994-06-03

    Applicant: BASF AG

    Inventor： BUSSCHE-HUENNEFELD CHRISTOPH D ,  KLINTZ RALF DR ,  HAMPRECHT GERHARD DR ,  HEISTRACHER ELISABETH DR ,  SCHAEFER PETER DR ,  DITRICH KLAUS DR ,  WESTPHALEN KARL-OTTO DR ,  GERBER MATTHIAS DR ,  WALTER HELMUT DR

    IPC: C07D231/18 ,  A01N43/56 ,  A01N47/12 ,  A01N47/34 ,  A01N47/40 ,  C07D231/20 ,  C07D231/22 ,  C07D401/06 ,  C07D401/10 ,  C07D403/06 ,  C07D403/10 ,  C07D405/06 ,  C07D405/10 ,  C07D409/06 ,  C07D231/14

    Abstract: Substituted 3-phenylpyrazoles (I) in which: R represents -C(R )=C(R ,R ), (a), -C(R ,R )-C(R ,R ,R ), (b), (c), -C(R )=C(R )-phenyl or -C(R ,R )-C(R ,R )-phenyl; R represents CN, CF3, halogen; R represents H, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy-C1-C4-alkyl; R represents C1-C4-alkoxy, C1-C4-haloalkoxy, C1-C4-alkylthio, C1-C4-haloalkylthio, C1-C4-alkylsulfinyl, C1-C4-haloalkylsulfinyl, C1-C4-alkylsulfonyl, C1-C4-haloalkylsulfonyl; R represents H, NO2, halogen, carboxylic acid/ester radical, substituted or unsubstituted aminocarbonyl; R represents H, halogen; Y represents -O-, -S-, -CH2-; Z represents 2- to 5-membered chain; R represents CN, halogen, C1-C4-alkyl, C1-C4-haloalkyl, C2-C4-alkenyl, carboxylic acid/ester radical, substituted or unsubstituted aminocarbonyl; R , R , R , R represent H, CN, halogen, C1-C4-alkyl, C1-C4-haloalkyl, C2-C4-alkenyl, carboxylic acid/ester radical, substituted or unsubstituted -N(H)-CO-R , amino or aminocarbonyl: R represents CN, halogen, carboxylic acid/ester radical, substituted or unsubstituted amino or aminocarbonyl, azido, OH, (halo)alkoxy, alkenyloxy, alkylcarbonyloxy; R represents isoxazolidinylcarbonyl, carboxylic acid/ester radical, acid amide group, -CO-O-N=C(R )-(C1-C6-alkyl), -CO-O-N=C(R )-CO-O-(C1-C6-alkyl), -CO-O-N=C(R31)-(C1-C4-alkyl)-CO-O-(C1-C4-alkyl)-CO-O-CH2-R , -CO-O-C(R )-(C1-C4-alkyl), substituted or unsubstituted aminocarbonyl or aminothiocarbonyl, -CO-NH-SO2-(C1-C4-alkyl), -CO-R , -CO-O-(C1-C4-alkyl)-C(R )=N-O-(C1-C4-alkyl), substituted or unsubstituted -CO-NH-CH(R )-(COOH/ester) substituted or unsubstituted cyclopentyliminooxy- or cyclohexyliminooxycarbonyl; R represents H, C1-C4-alkyl, phenyl, benzyl; R , R represents H, C1-C6-alkyl, C1-C6-haloalkyl, C1-C4-alkoxy-C1-C4-alkyl, substituted or unsubstituted C3-C7-cycloalkyl, phenyl or phenyl-C1-C6-alkyl; R represents C1-C6-alkyl, C1-C4-haloalkyl, C1-C6-alkoxy-C1-C4-alkyl, C1-C6-alkoxycarbonyl-C1-C4-alkyl, di-[C1-C6-alkoxycarbonyl]-C1-C4-alkyl, C3-C6-cycloalkyl, C1-C6-alkoxy, C1-C6-alkoxycarbonyl, 2-furyl, substituted or unsubstituted phenyl; R represents H, halogen, C1-C4-alkyl, C2-C4-alkenyl, C1-C4-haloalkyl, C1-C4-alkoxy-C1-C4-alkyl, C1-C4-alkylthio-C1-C4-alkyl, are used as herbicides.

    14.
    发明专利
    未知

    公开(公告)号：DE59400025D1

    公开(公告)日：1995-11-09

    申请号：DE59400025

    申请日：1994-01-05

    Applicant: BASF AG

    Inventor： EICKEN KARL DR ,  DITRICH KLAUS DR ,  MUELLER THOMAS DR ,  WAGNER OLIVER DR

    IPC: C07D277/20 ,  C07D277/34 ,  C07D277/56

    Abstract: Process for the preparation of alkyl 2-alkyl-4-fluoromethylthiazolecarboxylates of the formula I in which R is alkyl, R is difluoromethyl or trifluoromethyl and R is alkyl, by reacting thiocarboxamides of the formula II in which R has the abovementioned meaning with alkyl 2-chloro-4-fluoroacetoacetates of the formula III in which R and R have the abovementioned meanings, in an aprotic solvent at temperatures of below 100@C and reacting the product with a dehydrating agent at temperatures of below 80@C, if appropriate in the presence of bases.

    16.
    发明专利
    未知

    公开(公告)号：DE4301356A1

    公开(公告)日：1994-07-21

    申请号：DE4301356

    申请日：1993-01-20

    Applicant: BASF AG

    Inventor： EICKEN KARL DR ,  DITRICH KLAUS DR ,  MUELLER THOMAS DR ,  WAGNER OLIVER DR

    IPC: C07D277/20 ,  C07D277/34 ,  C07D277/56 ,  C07D277/36

    Abstract: Process for the preparation of alkyl 2-alkyl-4-fluoromethylthiazolecarboxylates of the formula I in which R is alkyl, R is difluoromethyl or trifluoromethyl and R is alkyl, by reacting thiocarboxamides of the formula II in which R has the abovementioned meaning with alkyl 2-chloro-4-fluoroacetoacetates of the formula III in which R and R have the abovementioned meanings, in an aprotic solvent at temperatures of below 100@C and reacting the product with a dehydrating agent at temperatures of below 80@C, if appropriate in the presence of bases.

    17.
    发明专利
    未知

    公开(公告)号：DE3931786A1

    公开(公告)日：1991-04-04

    申请号：DE3931786

    申请日：1989-09-23

    Applicant: BASF AG

    Inventor： DITRICH KLAUS DR ,  HAMPRECHT GERHARD DR ,  PLATH PETER DR ,  WUERZER BRUNO DR ,  WESTPHALEN KARL-OTTO DR

    IPC: A01N43/56 ,  C07D231/14 ,  C07D401/02 ,  C07D401/04 ,  C07D401/12 ,  C07D401/14 ,  C07D403/12 ,  C07D405/02 ,  C07D405/04 ,  C07D405/12 ,  C07D405/14 ,  C07D409/02 ,  C07D409/04 ,  C07D409/12 ,  C07D409/14 ,  C07D413/04 ,  C07D417/12 ,  C07D417/14

    Abstract: Pyrazole-3-carboxamides of the general formula I in which the substituents have the following meanings: R represents hydrogen or optionally substituted C3-C8-cycloalkyl or C1-C4-alkyl, R represents hydroxyl; amino; C1-C4-alkylamino; di-C1-C4-alkylamino, aminocarbonyl-C1-C6-alkyl, optionally substituted C1-C4-alkoxy, C3-C6-alkenyl, C3-C6-alkynyl, phenyl or naphthyl, optionally substituted 5- to 6-membered heterocycle; one of the groups mentioned under R or R and R together form a 4- to 7-membered chain which can contain as ring member one of the following groups in addition to methylene groups: oxygen, sulphur, N-methyl or carbonyl; R represents optionally substituted 5- to 6-membered heterocycle, optionally substituted C3-C6-alkenyl, C3-C6-alkynyl, 5,6,7,8-tetrahydronaphthyl or phenyl, or one of the groups mentioned under R ; R represents nitro; cyano; carboxyl; halogen; optionally substituted C1-C4-alkoxy or C1-C4-alkylthio, or one of the groups mentioned under R ; R represents 4,5-dihydrooxazol-2-yl or a group COYR ; Y represents oxygen or sulphur; R represents hydrogen; C3-C8-cycloalkyl, optionally substituted C1-C6-alkyl, C3-C6-alkenyl, C3-C6-alkynyl, C5-C7-cycloalkenyl or phenyl, optionally substituted 5- to 6-membered heterocycle; phthalimido; tetrahydrophthalimido; succinimido; maleimido; benzotriazolyl or a group -N=CR R where R is hydrogen or C1-C6-alkyl and R is C3-C6-cycloalkyl, phenyl, furyl or a radical R , or R and R together form a 4- to 7-membered alkylene chain, and their agriculturally useful salts, where Y is not oxygen and R is not hydrogen when R is hydrogen and R is nitro, trifluoromethyl, halogen or C1-C4-alkoxy, and -YR is not ethoxy when R is hydrogen, R is methyl and R is phenyl or substituted phenyl.

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