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公开(公告)号：DE102014103692A1
公开(公告)日：2015-09-24
申请号：DE102014103692
申请日：2014-03-18
Applicant: BASF SE
Inventor： HAMMON ULRICH , WALTER THOMAS
IPC: B01J4/00
Abstract: Die vorliegende Erfindung beschreibt ein System (1) zum Rückgewinnen von flüssigen oder fließfähigen Chemikalien in einer chemischen Anlage (3), das – zumindest zwei Anlagenteile (3a, 3b) der Anlage (3), – je Anlagenteil (3a, 3b) zumindest eine Anschlusseinrichtung (5a, 5b), die jeweils am tiefsten Punkt des jeweiligen Anlagenteils (3a, 3b) angeordnet ist, – zumindest eine gemeinsame Sammelleitung (7), welche unterhalb der Anschlusseinrichtungen (5a, 5b) verläuft und diese miteinander verbindet, – zumindest einen Sammelbehälter (9), der im Wesentlichen auf der gleichen Höhe wie oder höher als die zumindest zwei Anlagenteile (3a, 3b) und oberhalb der Sammelleitung (7) angeordnet ist, – zumindest eine Pumpe (11), die zwischen den Anschlusseinrichtungen (5a, 5b) und dem Sammelbehälter (9) in der Sammelleitung (7) vorgesehen ist, zum Abziehen der in der Sammelleitung (7) zusammengeführten zumindest einen flüssigen oder fließfähigen Chemikalie und Einleiten in den Sammelbehälter (9) umfasst. Die vorliegende Erfindung bezieht sich ferner auf ein Verfahren zum Rückgewinnen von flüssigen oder fließfähigen Chemikalien in einer chemischen Anlage (3) mittels des erfindungsgemäßen Systems (1) sowie auf die Verwendung des Systems (1).
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12.发明专利
公开(公告)号：DE102014103691A1
公开(公告)日：2015-09-24
申请号：DE102014103691
申请日：2014-03-18
Applicant: BASF SE
Inventor： HAMMON ULRICH , WALTER THOMAS , SCHRAUT ARMIN
Abstract: Die vorliegende Erfindung bezieht sich auf einen Wärmetauscher (1), der – ein Bündel von zumindest zwei Wärmetauscherrohren (3), wobei das Bündel von Wärmetauscherrohren (3) vertikal ausgerichtet ist und nach unten von einem Wärmetauscherrohrboden (31) abgeschlossen wird, – ein das Bündel von Wärmetauscherrohren (3) umgebendes Wärmetauschergehäuse (5), wobei das Bündel von Wärmetauscherrohren (3) in dem Wärmetauschergehäuse (5) von einem flüssigen Wärmeträger (7) umspült wird, – eine das Wärmetauschergehäuse (5) nach oben abschließende Wärmetauscherhaube (9), – einen das Wärmetauschergehäuse (5) nach unten abschließenden Wärmetauscherboden (11), – einen am Wärmetauschergehäuse (5) vorgesehenen Zulauf (13) für den Wärmeträger (7) in den Wärmetauscher (1), – einen am Wärmetauschergehäuse (5) vorgesehenen Ablauf (15) für den Wärmeträger (7) aus dem Wärmetauscher (1) und – ein Notentlastungsstutzen (17), der in der Nähe der Wärmetauscherhaube (9) angeordnet ist, umfasst. Der Wärmetauscher (1) ist dadurch gekennzeichnet, dass der Wärmetauscher (1) eine Sicherheitseinrichtung (19) aufweist, die in der Nähe des Wärmetauscherbodens (11) angeordnet ist. Die vorliegende Erfindung stellt ferner eine Reaktoranordnung (101) dar, die – einen Reaktor (27) – einen mit dem Reaktor (27) verbundenen Wärmetauscher (1) gemäß der vorliegenden Erfindung, und – eine mit dem Reaktor (27) und/oder dem Wärmetauscher (1) verbundene Pumpe (29) zum Umwälzen zumindest eines Teils des flüssigen Wärmeträgers (7). umfasst. Schließlich werden ein Verfahren zum Temperieren eines Reaktors (27) und die Verwendung des Wärmetauschers (1) gemäß der vorliegenden Erfindung beschrieben.
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公开(公告)号：BRPI0810143A2
公开(公告)日：2014-10-29
申请号：BRPI0810143
申请日：2008-04-18
Applicant: BASF SE
Inventor： HAMMON ULRICH , FRIESE THORSTEN , PETZOLDT JOCHEN , MUELLER-ENGEL KLAUS JOACHIM , CREMER ULRICH , RAICHLE ANDREAS
IPC: C07C51/25 , C07C57/055
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公开(公告)号：BRPI0809157A2
公开(公告)日：2014-09-16
申请号：BRPI0809157
申请日：2008-03-20
Applicant: BASF SE
Inventor： FUNK RUEDIGER , HEIDE WILFRIED , WEISMANTEL MATTHIAS , HAMMON ULRICH , BENNET ANDREA KAREN
IPC: C07C57/075 , C07C57/04
Abstract: The invention relates to a method for the transportation of a monomer composition in which a composition comprising an aqueous solution of partially or entirely neutralized acrylic acid or overneutralized acrylic acid is placed in a transport means or sent through a pipe. The method according to the invention is characterized in that it has an increased level of safety during the transportation of acrylic acid monomers, an improved quality of the resulting product, and a high degree of efficiency. The method ensures safe transport of the highly reactive acrylic acid. The amount of polymerization inhibitors added to said acrylic acid may be reduced. An additional advantage is the minimization of the formation of dimeric acrylic acid. Tempering of containers, pipes, and pipelines may be omitted.
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公开(公告)号：DE50313279D1
公开(公告)日：2011-01-05
申请号：DE50313279
申请日：2003-07-02
Applicant: BASF SE
Inventor： HAMMON ULRICH , THIEL JOACHIM , SCHLIEPHAKE VOLKER , SCHROEDER JUERGEN
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Patent Agency Ranking
公开(公告)号：DE50312595D1
公开(公告)日：2010-05-20
申请号：DE50312595
申请日：2003-07-10
Applicant: BASF SE
Inventor： HAMMON ULRICH , PETZOLDT JOCHEN , MUELLER-ENGEL KLAUS JOACHIM , DIETERLE MARTIN
IPC: C07C51/25 , B01J8/00 , B01J8/06 , B01J23/00 , C07C51/215 , C07C57/05 , C07C57/055
Abstract: A process for the heterogeneously catalyzed gas-phase partial oxidation of an organic compound over a fixed catalyst bed present in a fixed-bed reactor having a plurality of catalyst tubes, in which the reduction of the quality of the catalyst load with increasing duration of operation is restored by a partial catalyst change, is described.
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公开(公告)号：DE102008041573A1
公开(公告)日：2010-03-04
申请号：DE102008041573
申请日：2008-08-26
Applicant: BASF SE
Inventor： BLUM TILL , ZUROWSKI PETER , RISSEL STEFFEN , HAREMZA SYLKE , FRIESE THORSTEN , JAEGER ULRICH , SCHLIEPHAKE VOLKER , MUELLER-ENGEL KLAUS JOACHIM , HAMMON ULRICH , HEILEK JOERG , MUELLER IMKE BRITTA
Abstract: Separating acrylic acid, contained as main constituent and glyoxal, contained as by-product from a gaseous product mixture of a partial gas phase oxidation of 3C-precursor compound of acrylic acid comprises producing a liquid phase containing at least 70 wt.% of acrylic acid and at least 200 mol.ppm of glyoxal in relation to the contained molar quantity of acrylic acid and separating glyoxal from the acrylic acid by crystallization from the liquid phase, where the acrylic acid is formed in crystallite form and the glyoxal is enriched in the mother liquor remained after crystallization.
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公开(公告)号：DE102008042009A1
公开(公告)日：2009-04-09
申请号：DE102008042009
申请日：2008-09-12
Applicant: BASF SE
Inventor： HEILEK JOERG , HAMMON ULRICH , MUELLER-ENGEL KLAUS-JOACHIM
Abstract: Target product continuous separating operation includes a heat exchanger having a secondary space and a primary space. The secondary space is separated from the primary space by a separating wall, which serves as a surface to transfer the heat from the secondary space to the primary space, where a current in fluid phase, and component of mass flow is fed to the target product in the secondary space of the heat exchanger. A fluid cooling medium having a temperature is fed to the primary space, such that fine crystals of the target product are formed in the secondary phase from the fluid residual phase of the fluid phase. A fluid cooling medium containing a mass flow is fed from primary space to the target product in a former operating state and in latter operating state. A fluid cooling medium containing another mass flow is fed from the secondary space to the target product. The liquid phase has the target product and different product, whose total mole fraction has a value in a component. The total mole fraction at the component, which is different from the target product, in the fluid phase fed in the secondary space, is bigger in the latter operating state than the former operating state.
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公开(公告)号：DE102007043759A1
公开(公告)日：2008-09-11
申请号：DE102007043759
申请日：2007-09-13
Applicant: BASF SE
Inventor： HEILEK JOERG , HAMMON ULRICH , MUELLER-ENGEL KLAUS JOACHIM , SCHLIEPHAKE VOLKER , BAUMANN DIETER
Abstract: The procedure for continuous separation of target product (X) in the form of fine particle of crystallisate from a liquid phase (P) existing from the target product (X) and/or by the target product of different constituents, comprises indirectly operating a heat exchanger having primary and secondary areas, which are spatially separated with one another through a material divider that serves as an area for transmitting heat from the secondary area to the primary area by passing a stream at the liquid phase (P) in the secondary area of the heat exchanger. The procedure for continuous separation of target product (X) in the form of fine particle of crystallisate from a liquid phase (P) existing from the target product (X) and/or by the target product of different constituents, comprises indirectly operating a heat exchanger having primary and secondary areas, which are spatially separated with one another through a material divider that serves as an area for transmitting heat from the secondary area to the primary area by passing a stream at the liquid phase (P) in the secondary area of the heat exchanger during the primary area flows throughable simultaneously to a liquid cooling medium so that it forms fine particles of crystallisate of the target product in the secondary area under disposition of a liquid residual phase from the liquid phase (P). The total mole fraction of the liquid phase has the value of M b, p ges at the constituent (B i). The liquid residual phase (R) contains ingredients with a total mole fraction of M b, r (ges) greater than M b, p (ges) in comparison with the liquid phase (P). The content of residual phase in the target product is 70 wt.%. The cooling medium is suspended by fine particles of crystallisate of the target product in the liquid residual phase under receiving a suspension (S) having a crystallization grade (Y). The secondary area of the heat exchanger continuously takes the suspension with the temperature T s (aus). The suspension of fine particle crystallisate from the extracted suspension in load of discharge device is introduced with temperature (TS) to a mixing buffer container by a pump and the liquid phase is separated from the suspension contained in the discharge device. The temperature of the suspension in the buffer container is elevated from the way of secondary area in the buffer container and/or pipelines of the buffer container by external energy source at a value of T(pu) above of T s(aus) and/or the total mole fraction of the ingredients is increased in the liquid residual phase of the suspension in the buffer container through external additive in the ingredients at a value of M b, p u (ges) above of M b, r (ges). The T(pu)-T s(aus) is greater than or equal to 0.1 K. The increasing of M b, r ges at M b, r (ges) is greater than or equal to 0.1%. The content of the liquid residual phase at the target product is greater than or equal 90 wt.%. The crystallization grade (Y) is 0.20-0.40.
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公开(公告)号：DE10295578B3
公开(公告)日：2008-05-29
申请号：DE10295578
申请日：2002-12-05
Applicant: BASF SE
Inventor： HAMMON ULRICH , SCHROEDER JUERGEN
Abstract: The base (1) for a column to rectify or absorb thermally unstable materials, which tend to polymerize, has risers (7) with covering hoods (8) supported on struts (9). Collected liquid can also run off the edge of the base through outflows (6) from one or more gutters (5). The gutters are angled downwards towards the edge of the base by 0.2-5.0[deg] and preferably 0.5-2.0[deg], and the base surface is angled down towards the gutters by 0.5-5.0[deg] and preferably 1-3[deg]. The under side (2) of the base is flat and horizontal.
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