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    少なくとも１つの（メタ）アクリルモノマーを含む液体混合物に熱を伝達するための方法
    1.
    发明专利
    少なくとも１つの（メタ）アクリルモノマーを含む液体混合物に熱を伝達するための方法 审中-公开
    用于发送液体混合物的方法，包括至少一种（甲基）丙烯酸单体

    公开(公告)号：JP2014198717A

    公开(公告)日：2014-10-23

    申请号：JP2014109260

    申请日：2014-05-27

    Applicant: ビーエーエスエフ ソシエタス・ヨーロピアBasf Se ,  Basf Se ,  ビーエーエスエフ ソシエタス・ヨーロピアBasf Se

    Inventor： LIPOWSKY GUNTER ,  SCHLIEPHAKE VOLKER DR ,  RISSEL STEFFEN ,  JAEGER ULRICH ,  HOEFER FRANK ,  HAREMZA SYLKE ,  ZUROWSKI PETER ,  MULLER-ENGEL KLAUS JOACHIM

    IPC: C07C51/44 ,  C07C51/50 ,  C07C57/04

    CPC classification number: C09K5/08 ,  C07C51/252 ,  C07C51/412 ,  C07C51/42 ,  C08F220/00 ,  C09K5/10 ,  F28D7/00 ,  C07C57/04 ,  C08K5/17

    Abstract: 【課題】間接式熱交換器を利用した、少なくとも1つの(メタ)アクリルモノマーを含む液体混合物に熱を伝達するための向上した方法の提供。【解決手段】少なくとも1つの(メタ)アクリルモノマーを含む液体混合物は、三級アミン、三級アミンとブレンステッド酸から形成された塩、および四級アンモニウム化合物からなる群からの(メタ)アクリルモノマー以外の少なくとも1つの添加作用化合物を含むが、少なくとも1つの作用化合物における三級および四級窒素原子がいずれもフェニル基を有さず、少なくとも一部分量が少なくとも1つのアルキル基を有することを条件とする、流体熱媒体がその一次側を流れ、少なくとも1つの(メタ)アクリルモノマーを含む液体混合物がその二次側を同時に流れる間接式熱交換器を利用した、少なくとも1つの(メタ)アクリルモノマーを含む液体混合物に熱を伝達するための方法。【選択図】なし

    Abstract translation: 要解决的问题：提供一种通过使用间接热交换器将热传递到包含至少一种（甲基）丙烯酸类单体的液体混合物的改进方法。解决方案：在所提供的将热传递到包括至少一种 （甲基）丙烯酸类单体，其中流体热介质流过其初级侧，并且包含至少一种（甲基）丙烯酸单体的液体混合物同时流过其二次侧，所述液体混合物包括至少一种 （甲基）丙烯酸单体包括除了（叔）胺，由叔胺和布朗斯台德酸形成的盐和季铵化合物以外的（甲基）丙烯酸单体以外的至少一种添加剂， 所述至少一种添加剂的季氮原子具有苯基，但至少其部分部分具有至少一个烷基。

    Separating column
    2.
    发明专利
    Separating column 有权
    分隔柱

    公开(公告)号：JP2010058122A

    公开(公告)日：2010-03-18

    申请号：JP2009284104

    申请日：2009-12-15

    Applicant: Basf Se ,  ビーエーエスエフ ソシエタス・ヨーロピアBasf Se

    Inventor： DIEHL VOLKER ,  JAEGER ULRICH ,  HAMMON ULRICH DR ,  SCHROEDER JUERGEN DR ,  RISSEL STEFFEN

    IPC: B01J10/00 ,  B01D3/16 ,  B01D3/32 ,  B01D5/00 ,  C07B61/00 ,  C07C51/44 ,  C07C57/07

    CPC classification number: B01D3/326 ,  B01D3/324 ,  C07C51/44 ,  Y10S203/11 ,  Y10S203/22 ,  C07C57/04

    Abstract: PROBLEM TO BE SOLVED: To remove a part of a face which is in the shadow region of a reflux sprayed and inhibited in polymerization of the internal structure included in a separating column suitable for a thermal separation method from the shadow region by using a method as simple as possible without a high cost, and also without a spraying nozzle to be used.
    SOLUTION: The problem is solved by the separating column which includes a continuity of a substance exchanging tray in which a covered double-T support and/or a covered U-shaped support are incorporated as a supporting element.
    COPYRIGHT: (C)2010,JPO&INPIT

    Abstract translation: 要解决的问题：为了通过使用以下方式除去在适合于热分离方法的分离塔中包含的内部结构的聚合反应中所喷射的反射区域的阴影区域的一部分与阴影区域 尽可能简单的方法，而不需要高成本，也不需要使用喷嘴。 解决方案：通过分离柱解决问题，该分离柱包括物质交换盘的连续性，其中结合有覆盖的双T支撑和/或覆盖的U形支撑作为支撑元件。 版权所有（C）2010，JPO＆INPIT

    8.
    发明专利
    未知

    公开(公告)号：BRPI0721107A2

    公开(公告)日：2014-03-04

    申请号：BRPI0721107

    申请日：2007-12-11

    Applicant: BASF SE

    Inventor： LIPOWSKY GUNTER ,  SCHLIEPHAKE VOLKER ,  RISSEL STEFFEN ,  JAEGER ULRICH ,  HOEFER FRANK ,  HAREMZA SYLKE ,  ZUROWSKI PETER ,  MUELLER-ENGEL KLAUS JOACHIM

    IPC: C08K5/17 ,  C08F220/00 ,  F28D1/00

    Abstract: Process for transferring heat to a liquid mixture comprising at least one (meth)acrylic monomer with the aid of an indirect heat exchanger comprises introducing the liquid mixture simultaneously into the primary side of the heat exchanger by a liquid heat carrier and secondary side of the heat exchanger, where: the liquid mixture comprising at least one (meth)acrylic monomer contains at least one added active compound other than (meth)acrylic monomers from tertiary amine or salts formed from a tertiary amine and Bronsted acid, and quaternary ammonium compounds. Process for transferring heat to a liquid mixture comprising at least one (meth)acrylic monomer with the aid of an indirect heat exchanger comprises introducing the liquid mixture simultaneously into the primary side of the heat exchanger by a liquid heat carrier and secondary side of the heat exchanger, where: the liquid mixture comprising at least one (meth)acrylic monomer contains at least one added active compound other than (meth)acrylic monomers from tertiary amine or salts formed from a tertiary amine and Bronsted acid, and quaternary ammonium compounds, with proviso that none of the tertiary and quaternary nitrogen atoms in the active compound bears a phenyl group, but at least partly contains an alkyl group.

    Separating acrylic acid comprises cooling product gas mixture of partial gas phase oxidation of three carbon precursor compound in cooler and providing cooled product gas mixture with (non)evaporated cooling liquid into absorption column
    10.
    发明专利
    Separating acrylic acid comprises cooling product gas mixture of partial gas phase oxidation of three carbon precursor compound in cooler and providing cooled product gas mixture with (non)evaporated cooling liquid into absorption column 未知

    公开(公告)号：DE102009027401A1

    公开(公告)日：2010-02-18

    申请号：DE102009027401

    申请日：2009-07-01

    Applicant: BASF SE

    Inventor： BLUM TILL ,  ZUROWSKI PETER ,  RISSEL STEFFEN ,  HAREMZA SYLKE ,  FRIESE THORSTEN ,  JAEGER ULRICH ,  SCHLIEPHAKE VOLKER ,  MUELLER-ENGEL KLAUS JOACHIM ,  HAMMON ULRICH ,  HOEFER FRANK

    IPC: C07C57/07

    Abstract: Separating acrylic acid from the product gas mixture of a heterogeneously catalyzed partial gas phase oxidation of at least one 3C-precursor compound to acrylic acid comprises: (a) cooling the product gas mixture in a direct cooler by directly cooling with a finely sprayed cooling liquid, where a portion of the cooling liquid is evaporated and (b) providing the cooled product gas mixture together with evaporated and non-evaporated cooling liquid into an absorption column of a sump region. Method for separating acrylic acid from the product gas mixture of a heterogeneously catalyzed partial gas phase oxidation of at least a 3C-precursor compound to acrylic acid, where the mixture, in addition to acrylic acid, comprises water vapor, glyoxal, low boiling, average boiling, high boiling and highly condensable compounds that are different from the above, as by-products, comprises: (a) cooling the product gas mixture in a direct cooler by directly cooling with a finely sprayed cooling liquid, where a portion of the cooling liquid is evaporated; (b) providing the cooled product gas mixture together with evaporated and non-evaporated cooling liquid into an absorption column of a sump region, where between the absorption room of the absorption column a chimney plate having at least one chimney, is present and connected; (c) providing the cooled product gas mixture and evaporated cooling liquid into the soil absorption column through the chimney of the chimney plate, which forms descending high-boiling absorption medium, where the chimney plate contains a absorbate, which absorbs acrylic acid; (d) removing the acrylic acid from the absorbate; (e) contacting one portion of absorbate filled in the absorption column to the sump room of the absorption column for forming a sump fluid in the sump region, optionally cooling another portion of the absorbate and recycling the chimney plate into the absorption column; (f) contacting the residual quantity in the absorbate or the absorbate in a rectification column with reinforcing and stripping section; (g) enriching the stripping section of the rectification column with the absorbate and feeding out the stripping section of absorption agent with an acrylic acid weight portion of >= 1 wt.%; (h) enriching the rectification section of the rectification column with acrylic acid and feeding out the reinforcing section of a raw acrylic acid, where the weight portion of the acrylic acid is = 90 wt.%; (i) extracting the obtained sump liquid from the sump region of the absorption column, feeding one portion of the obtained sump liquid, as cooling liquid, into the direct cooler and feeding the remaining portion of the liquid into the bottom of a distillation unit comprising a distillation column and a circulating heat exchangers; (j) separating the sump liquid in the distillation column of the distillation unit in exhaust vapors, whose weight portion in the absorption agent is greater than the weight portion of the sump fluid at absorption agent, and into liquid concentrate, whose weight portion is high, when the absorption agent of the boiling components is greater than the high boiling components of the sump liquid; (k) recycling water vapor, possibly its cooling and/or condensation in an indirect heat exchanger and above the chimney plate in the absorption column; (l) leading out a mass flow from the bottom of the distillation column in the standing height of the liquid concentrate with the temperature T 1>from the distillation column; (m) discharging a partial stream of the mass flow from the procedure of the separation of acrylic acid from the product gas mixture; and (n) recycling the residual stream of the mass flow over the circulation heat exchanger with a temperature (T 2>>= T 1>) of absorbed mass flow from the distillation column, into the distillation column; where the average retention time of the components of the partial stream in the distillation unit is = 40 hours.

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