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    METHOD FOR PRODUCING ALKALI METHYLATES
    21.
    发明专利
    METHOD FOR PRODUCING ALKALI METHYLATES 未知

    公开(公告)号：HU0301074A2

    公开(公告)日：2003-08-28

    申请号：HU0301074

    申请日：2000-12-08

    Applicant: BASF AG

    Inventor： BURKART KIRSTEN ,  FRIEDRICH HOLGER ,  GUTH JOSEF ,  HOFFMANN ELKE ,  KAIBEL GERD ,  STERZEL HANS-JOSEF DR

    IPC: B01D1/28 ,  C07C29/70 ,  C07C29/80 ,  C07C31/30

    Abstract: Alkali metal methoxides are prepared from aqueous alkali metal hydroxide, which may have been admixed with methanol, and methanol in a reaction column having at least 5, preferably from 15 to 30, theoretical plates between the feed point for the aqueous alkali metal hydroxide and the feed point for the methanol. The gaseous methanol/water mixture formed in the reaction is fractionated in a rectification column. In one variant of the invention, the trays chosen for the reaction column configured as a bubble cap tray, valve tray or sieve tray column are trays in which not more than 5%, preferably

    25.
    发明专利
    未知

    公开(公告)号：PT947493E

    公开(公告)日：2003-03-31

    申请号：PT99105126

    申请日：1999-03-26

    Applicant: BASF AG

    Inventor： STROEZEL MANFRED ,  KAIBEL GERD ,  AQUILA WERNER ,  BROCKER FRANZ JOSEF ,  FUCHS HARTWIG ,  WEGNER GUNTER

    IPC: B01J23/44 ,  B01J8/20 ,  B01J8/22 ,  B01J19/24 ,  B01J23/46 ,  C07B61/00 ,  C07C45/62 ,  C07C47/21 ,  C07C49/04

    Abstract: Production of saturated carbonyl compounds (I) by selective liquid-phase hydrogenation of alpha , beta -unsaturated carbonyl compounds (II) is carried out in a packed bubble column with the product recycled and by circulating hydrogen gas. Production of saturated carbonyl compounds of formula R1-CH(R2)-CH(R3)-C(R4)=O (I) by selective liquid-phase hydrogenation of alpha , beta -unsaturated carbonyl compounds of formula R1-C(R2)=C(R3)-C(R4)=O (II) in the presence of a particulate palladium and/or rhodium catalyst and a base is carried out in a packed bubble column with the product recycled and by circulating hydrogen gas. R1 = H or an organic group; R2-R4 = H or 1-4C alkyl.

    26.
    发明专利
    未知

    公开(公告)号：ES2183469T3

    公开(公告)日：2003-03-16

    申请号：ES99122636

    申请日：1999-11-13

    Applicant: BASF AG

    Inventor： OOST CARSTEN ,  STROEZEL MANFRED ,  ETZRODT HEINZ ,  WELLER DIETMAR ,  RHEUDE UDO ,  KAIBEL GERD

    IPC: B01J31/14 ,  C07B61/00 ,  C07C45/67 ,  C07C45/74 ,  C07C49/203

    Abstract: Preparation of unsaturated ketones by reaction of the corresponding alpha , beta -unsaturated alcohol with an alkyl acetoacetate compound in the presence an organo-aluminum catalyst at constant temperature, with separation and continuous removal of CO2 and alcohol formed. Preparation of unsaturated ketones of formula (I) by reaction of the corresponding alpha , beta -unsaturated alcohol of formula (II) with an alkyl acetoacetate compound of formula (III) in the presence of 0.1-5 mole% (based on (III)) of an organo-aluminum catalyst with separation and continuous distillative removal of CO2 and alcohol of formula R3OH formed during reaction, in a reactor containing a fractionation column, where: (A) (II) is added to the reaction mixture together with the organic catalyst without additional solvent and (III) is then added to this mixture; (B) the reaction temperature is kept constant between 175-220 degrees C; (C) the content of (III) is kept at a constant level between 0.1-10 wt.% during the reaction. R1, R3 = 1-4C alkyl; R2 = 4-30C aliphatic, cycloaliphatic or cycloaliphatic-aliphatic; a, b = optional additional bonds.

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