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公开(公告)号：KR1020000059735A
公开(公告)日：2000-10-05
申请号：KR1019990007558
申请日：1999-03-08
Applicant: 한국화학연구원
IPC: C07D413/12
Abstract: PURPOSE: A N-(5-isoxazolinylmethyloxyphenyl)-dimethylmaleimide derivative is provided which has excellent stability against a rice plant and shows good herbicidal activity on weeds in a paddy like echor, scpju, moova, cypse, sagpy or so on. CONSTITUTION: The N-(5-isoxazolinylmethyloxyphenyl)-dimethylmaleimide derivative is shown in a chemical formula 1 wherein R is alkyl radical with 1-5 carbon number, phenyl radical or substituted phenyl radical, cyano radical, carboxylic acid or carboxylic ester, heterocyclic or substituted heterocyclic radical. The substituted phenyl radical or substituted heterocyclic radical is simply or mixedly substituted from 1-3 radicals among alkyl radical with 1-3 carbon number, alkoxy radial with 1-3 carbon number, halogen atom, cyano radical, nitro radical, carboxyl radical and carboxylic ester.
Abstract translation: 目的：提供一种对水稻植株具有优异稳定性的N-（5-异恶唑啉基甲氧基苯基） - 二甲基马来酰亚胺衍生物，对水稻，scpju，moova，cypse，sagpy等中的杂草具有良好的除草活性。 组成：N-（5-异恶唑啉基甲氧基苯基） - 二甲基马来酰亚胺衍生物以化学式1表示，其中R是具有1-5个碳数的烷基，苯基或取代的苯基，氰基，羧酸或羧酸酯，杂环或 取代的杂环基。 取代的苯基或取代的杂环基团在具有1-3个碳原子的烷基，具有1-3个碳数的烷氧基，卤素原子，氰基，硝基，羧基和羧基的烷基中简单或混合取代1-3个基团 酯。
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公开(公告)号：KR100250838B1
公开(公告)日：2000-05-01
申请号：KR1019970065411
申请日：1997-12-02
Applicant: 한국화학연구원
IPC: C07D307/08
Abstract: PURPOSE: Provided is a preparation method of 3(-(hydroxymethyl)tetrahydrofuran) represented by the formula (1) which is used as an intermediate raw material of drugs and insecticide. Thereby the compound is simply and easily prepared compared to the conventional methods. CONSTITUTION: (3-(hydroxymethyl)tetrahydrofuran) of the formula (1) is prepared by cyclization reaction of 2-hydroxymethyl-4-alkene-1-ol derivative of the formula (2) in the presence of I2 catalyst in organic solvent, wherein R1, R2 and R3 are C1-C4 alkyl or phenyl selected from the group consisting of hydrogen, methyl, ethyl, n-propyl, i-propyl, n-butyl, i-butyl and t-butyl, respectively.
Abstract translation: 目的：提供用作药物和杀虫剂的中间体原料的由式（1）表示的3（ - （羟甲基）四氢呋喃）的制备方法。 因此，与常规方法相比，化合物简单且容易地制备。 组成：通式（2）的2-羟甲基-4-烯-1-醇衍生物在有机溶剂中存在的I2催化剂的环化反应制备式（1）的（3-（羟甲基）四氢呋喃） 其中R1，R2和R3分别是C1-C4烷基或选自氢，甲基，乙基，正丙基，异丙基，正丁基，异丁基和叔丁基的苯基。
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公开(公告)号：KR100128544B1
公开(公告)日：1998-04-04
申请号：KR1019940016984
申请日：1994-07-14
Applicant: 한국화학연구원
IPC: C07D209/32 , C07D209/42
Abstract: Title derivatives(I; R1, R2= same or not, H, fluro, chlorro, bromo, C1-3 alkyl, C1-3 alkoxy; R1 and R2 are formed a fused ring such as -CH=CH-CH=CH-; R3= H, C1-4 alkyl, C3-6 alkenyl, etc.), useful as herbicides were prepared. Thus, 3.03 g 4-fluorophenol was reacted with 1.9 ml ethyl chloride, followed by addition of 4.0 g anhydrous aluminium chloride at 180 deg.C for 30 minutes to give 2.71 g 2-hydroxy-5-fluoroacetophenone(III). III and 1.05 g ethyl carbamate were refluxed for 20- 30 hours in 50 ml n-propanol to give ethoxycarbonylhydrazone derivatives IV. 2.41 g IV was dissolved in 100 ml tetrahydrofuran, adding 4.44 g (CH3COO)4Pb as an oxidation agent at room temperature for 3- 5 hours to give ethyl 0-acetylarylcarboxylate derivatives(V). 2.1 g V and 0.83 g 4-chloro-2-fluoro-5-hydroxyaniline were refluxed for 20- 30 hours in a mixed solvent of 50 ml o-dichlorobenzene and acetic acid to give 2,3-dihydro-3-methylene- 2-(4-chloro-2-fluoro-3-hydroxyphenyl)-1H-isoindol-1-one(VII). VII was refluxed for 20 hours to give 2,3-dihydro-3-methylene-2- (3-propagyloxy-4-chloro-2-fluorophenyl)-1H-isoindol-1-one(I).
Abstract translation: 标题衍生物（I; R1，R2 =相同或不同，H，氟，氯，溴，C1-3烷基，C1-3烷氧基; R1和R2形成稠环，例如-CH = CH-CH = CH- ; R3 = H，C1-4烷基，C3-6烯基等），可用作除草剂。 因此，将3.03g 4-氟苯酚与1.9ml氯乙烷反应，然后在180℃下加入4.0g无水氯化铝30分钟，得到2.71g 2-羟基-5-氟苯乙酮（III）。 III和1.05g氨基甲酸乙酯在50ml正丙醇中回流20-30小时，得到乙氧基羰基腙衍生物IV。 将2.41g IV溶解在100ml四氢呋喃中，在室温下加入4.44g（CH3COO）4Pb作为氧化剂，持续3-5小时，得到O-乙酰基芳基羧酸乙酯衍生物（V）。 将2.1g V和0.83g 4-氯-2-氟-5-羟基苯胺在50ml邻二氯苯和乙酸的混合溶剂中回流20-30小时，得到2,3-二氢-3-亚甲基-2 - （4-氯-2-氟-3-羟基苯基）-1H-异吲哚-1-酮（VII）。 VII的混合物回流20小时，得到2,3-二氢-3-亚甲基-2-（3-羰基氧基-4-氯-2-氟苯基）-1H-异吲哚-1-酮（I）。
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公开(公告)号：KR1019960022496A
公开(公告)日：1996-07-18
申请号：KR1019940037131
申请日：1994-12-27
Applicant: 한국화학연구원
IPC: C07D307/79
Abstract: 본 발명은 농약 및 의약의 중간체로 유용한 다음 구조식(Ⅰ)로 표시되는 2,3-디히드로-2-메틸-2-알킬 벤조퓨란 유도체의 제조방법에 관한 것이다.
상기 식에서, X는 수소원자, 할로겐원자, 히드록시기, 알데히드기 또는 C
1 ∼C
6 의 알킬기이고, R은 C
1 ∼C
6 의 알킬이다.-
公开(公告)号：KR1019960007549A
公开(公告)日：1996-03-22
申请号：KR1019940020420
申请日：1994-08-18
Applicant: 한국화학연구원
IPC: C07C251/44 , A01N35/10 , C07C47/546 , C07C49/723 , C07C251/42
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Patent Agency Ranking
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公开(公告)号：KR101190716B1
公开(公告)日：2012-10-12
申请号：KR1020100042020
申请日：2010-05-04
Applicant: 한국화학연구원
Abstract: 본 발명은 탄소나노볼에 팔라듐을 담지한 불균일 촉매 및 상기 촉매하에서 아세틸렌 가스와 다양한 아릴 할라이드(aryl halide)를 반응시켜 단 한 단계에 산업적으로 유용성이 높은 디아릴아세틸렌 화합물들을 높은 수율로 제조하는 방법에 관한 것으로, 본 발명에 따른 팔라듐을 담지한 탄소나노볼 불균일 촉매는 회수하여 반복 사용할 수 있어 디아릴아세틸렌 화합물의 대량생산이 가능하며, 반응을 한 단계만으로 끝낼 수 있어 기존의 수율 감소 문제를 해결할 수 있다.
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公开(公告)号：KR101184292B1
公开(公告)日：2012-09-21
申请号：KR1020100054444
申请日：2010-06-09
Applicant: 한국화학연구원
Abstract: 본 발명은 하기 화학식 2로 표시되는 3관능성 [1,1';3',1'']Terphenyl-4,5',4''-triol 화합물을 에폭시화한 저융점의 에폭시 수지 및 상기 에폭시 수지에 경화제 등을 더 포함하여 이루어지는 에폭시 수지 조성물과 이 조성물로부터 얻어지는 에폭시 수지 경화물에 관한 것이다. 본 발명의 따른 에폭시 수지 경화물은 할로겐계 화합물이나 인계 난연제를 사용하지 않고도 높은 난연성을 나타내고 내충격성, 내흡수성, 내열성이 우수하여 반도체 밀봉재, 인쇄 회로 기판, 도료, 접착, 주형 용도 등에 적합하게 사용할 수 있다.
[화학식 2]
상기식에서 R 은 C
1
-12 의 알킬, 페닐, p 는 0~2의 정수이다.-
公开(公告)号：KR101174668B1
公开(公告)日：2012-08-17
申请号：KR1020100103556
申请日：2010-10-22
Applicant: 충남대학교산학협력단 , 한국화학연구원
IPC: C09J133/04 , C09J11/06 , C09J133/14 , C08L33/04
Abstract: 본발명은 a) C1~C14의알킬기를갖는 (메타)아크릴레이트계단량체; 히드록시기를갖는 (메타)아크릴레이트계단량체, 카복실기를갖는 (메타)아크릴레이트계단량체또는이들의혼합물;을중합하는단계; 및 b) 상기중합체에 C8~C12의알킬글리시딜에테르를투입하여그라프트(부가반응)하여중합하는단계;를포함하는점착제조성물의제조방법및 이의제조방법으로부터제조된점착제조성물에관한것이다.본발명에따른점착제조성물은젖음성및 재박리성이우수하다.
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公开(公告)号：KR1020120046618A
公开(公告)日：2012-05-10
申请号：KR1020100108364
申请日：2010-11-02
Applicant: 한국화학연구원
CPC classification number: C07F9/09 , C08K5/521 , C08L2201/02 , C08L2666/84 , C09K21/12
Abstract: PURPOSE: A flame retardant composition using biguanide phosphate compounds is provided to ensure excellent thermal resistance. CONSTITUTION: A biguanide phosphate compound is denoted by chemical formula 1. The compound is prepared by reacting dicyandiamide and ammonium phosphate and is neutral. A flame retardant composition contains the compound of chemical formula 1. A thermoplastic resin composition with excellent flame retardancy contains 100 weight parts of thermoplastic resin and 1-50 weight parts of the compound of chemical formula 1. The thermoplastic resin composition further contains organic phosphate ester compounds, magnesium, aluminum, fluorinated polyolefin, organic metal compounds, zinc borate, tetrafluoro ethylene or fluorinated vinylidene polymers or copolymers.
Abstract translation: 目的：提供使用双胍磷酸酯化合物的阻燃剂组合物，以确保优异的耐热性。 构成：化学式1表示双胍磷酸酯化合物。该化合物通过双氰胺和磷酸铵反应制备，为中性。 阻燃剂组合物含有化学式1的化合物。具有优异阻燃性的热塑性树脂组合物含有100重量份热塑性树脂和1-50重量份化学式1化合物。热塑性树脂组合物还含有有机磷酸酯 化合物，镁，铝，氟化聚烯烃，有机金属化合物，硼酸锌，四氟乙烯或氟化亚乙烯基聚合物或共聚物。
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