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    41.
    发明专利
    未知

    公开(公告)号：AT255609T

    公开(公告)日：2003-12-15

    申请号：AT99964568

    申请日：1999-12-14

    Applicant: BASF AG

    Inventor： BRUCHMANN BERND ,  BECK ERICH ,  RENZ HANS ,  KOENIGER RAINER ,  SCHWALM REINHOLD ,  LOKAI MATTHIAS ,  REICH WOLFGANG

    IPC: G03F7/027 ,  A61K6/893 ,  C07C265/14 ,  C07C275/60 ,  C08G18/67 ,  C08G18/78 ,  C08G18/81 ,  C09D4/00 ,  C09D5/00 ,  C09D175/04 ,  C09D175/14 ,  C09D175/16 ,  C09D201/02

    Abstract: Compounds having isocyanate groups with or without blocking, allophanate groups and free-radically polymerizable C-C double bonds, the C-C double bonds being in activated form by virtue of a carbonyl group attached directly to them or by virtue of an oxygen atom in ether function (activated double bonds), derived from polyisocyanates and alcohols A which in addition to the alcohol group also carry an activated double bond (compounds I). The invention additionally relates to radiation-curable formulations and coating compositions comprising the compounds I, to methods for coating using these substances, and to coated articles produced using these methods. Furthermore, the invention relates to the use of the compounds I in radiation-curable compositions such as in casting compositions, dental compounds, composite materials, sealing compounds, adhesives, troweling compounds, printing inks, in photostructurable compositions such as solder resists, photoresists, photopolymeric printing plates, and stereolithography resins.

    42.
    发明专利
    未知

    公开(公告)号：DE59800994D1

    公开(公告)日：2001-08-16

    申请号：DE59800994

    申请日：1998-04-02

    Applicant: BASF AG

    Inventor： KOKEL NICOLAS ,  MENZEL KLAUS ,  REICH WOLFGANG

    IPC: C09D175/04 ,  C09D175/16

    Abstract: Aqueous dispersions which are essentially free from protective colloids or emulsifiers, comprise, in dispersed form,A. a polyurethane (A) comprising hydrophilic groups, which bring about the water-dispersibility of the polyurethane, this polyurethane (A) being essentially free from C-C double bonds, andB. a prepolymer having a content of from 0.1 to 1 mol of free-radically polymerizable C-C double bonds per 100 g of prepolymer.

    43.
    发明专利
    未知

    公开(公告)号：DE59606463D1

    公开(公告)日：2001-03-29

    申请号：DE59606463

    申请日：1996-11-12

    Applicant: BASF AG

    Inventor： HAEUSSLING LUKAS ,  BERNHARD LUDWIG ,  REICH WOLFGANG ,  SCHWALM REINHOLD ,  BECK ERICH

    IPC: C07C67/08 ,  C07C67/62 ,  C07C69/54 ,  C08G65/332 ,  C09D4/02

    Abstract: A process for the production of (meth)acrylate esters (I) by esterification of (meth)acrylic acid (II) with mono- or poly- hydric alcohols (III) is claimed. The reaction mixture, still containing (II) in amounts equivalent to an acid number of at least 5 mg KOH/g, is treated with amino compound(s) (IV) containing at least one prim., sec. or tert. amino group. Also claimed are: (1) esters (I) obtained by this process; and (2) radiation-curable materials (RCM) containing (I).

    44.
    发明专利
    未知

    公开(公告)号：DE19933012A1

    公开(公告)日：2001-01-18

    申请号：DE19933012

    申请日：1999-07-14

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  MENZEL KLAUS ,  REICH WOLFGANG

    IPC: C08G18/08 ,  C08G18/67 ,  C08G18/72 ,  C09D175/04 ,  C09D175/14 ,  C08L75/14

    Abstract: A curable polyurethane polymer comprises a hydroxyl group containing prepolymer, a compound having a hydroxyl group and/or prim. or sec. amine group and a compound having at least 2 isocyanate groups and/or their salts whereby the ratio of isocyanate group equivalents to isocyanate reactive groups is 0.4:1-0.9:1. A curable polyurethane polymer (I) comprises: (A) 10-60 wt.% of a hydroxyl group containing prepolymer having at least a thermally or photochemically polymerizable alpha , beta -ethylenically unsaturated double bond (B) 0.1-30 wt.% of a compound having a hydroxyl group and/or prim. or sec. amine group that is reactive towards an isocyanate group and having at least one polar functional group per molecule; (C) 0.1-30 wt.% of a diamine and/or polyamine; (D) 0-10 wt.% of a compound, different to (A), (B), (C) and (E) having at least 2 isocyanate reactive groups and containing hydroxyl and/or prim. and/or sec. amine groups; (E) 0-20 wt.% of a compound having one isocyanate reactive group; (F) 10-65 wt.% of a compound having at least 2 isocyanate groups and/or their salts whereby the ratio of isocyanate group equivalents in (F) to isocyanate reactive groups is (A)-(E) is 0.4:1-0.9:1. Independent claims are included for: (i) a polymer dispersion containing (I); and (ii) a coating agent containing (I).

    45.
    发明专利
    未知

    公开(公告)号：DE19929258A1

    公开(公告)日：2000-12-28

    申请号：DE19929258

    申请日：1999-06-25

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  REICH WOLFGANG ,  BECK ERICH ,  JAWOREK THOMAS ,  KOENIGER RAINER

    IPC: B01J31/30 ,  C07B61/00 ,  C07C67/08 ,  C07C67/60 ,  C07C67/62 ,  C07C69/54

    Abstract: (Meth)acrylate compound is prepared by esterification with an alcoholic hydroxyl-containing compound using a copper salt as polymerization inhibitor and neutralizing the product with a basic inorganic compound(s). Preparation of (meth)acrylate comprises: (i) esterifying acrylic and/or methacrylic acids with a compound(s) with at least one alcoholic hydroxyl group at 90-150 degrees C in the presence of an acid esterification catalyst, a polymerization inhibitor, comprising a copper(II) salt optionally mixed with a copper (I) salt, the copper sulfide obtained being precipitated and separated after reaction, and a hydrocarbon of b.pt. 60-140 degrees C as water drawing agent; (ii) distilling off excess (meth)acrylic acid at 90-150 degrees C under normal pressure: and (iii) optionally neutralizing the product with a basic inorganic compound(s).

    46.
    发明专利
    未知

    公开(公告)号：DE19810793A1

    公开(公告)日：1999-09-16

    申请号：DE19810793

    申请日：1998-03-12

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  KOENIGER RAINER ,  REICH WOLFGANG ,  MENZEL KLAUS

    IPC: C08L75/04 ,  C08G18/08 ,  C08G18/32 ,  C08G18/67 ,  C08G18/68 ,  C09D175/04 ,  C09D175/14 ,  C08G18/42 ,  C08G18/48 ,  C08G18/64 ,  C08G18/58 ,  C08G18/10

    Abstract: Curable polyurethane polymers (I) and their salts are novel in that the sum of the OH numbers of a component comprising a prepolymer(s) containing hydroxyl groups with ethylenically unsaturated double bond(s) capable of free radical photochemical polymerization, and a component containing isocyanate-reactive hydroxy groups or hydroxy groups and/or amino groups, is 121-300 mg KOH/g. Curable polyurethane polymers (I) and their salts comprise (A) 40-80 wt.% prepolymer(s) containing hydroxyl (OH) groups with alpha , beta -ethylenically unsaturated double bond(s) capable of free radical photochemical polymerization; (B) 0.1-20 wt.% compound(s) containing OH and/or primary or secondary amino group(s) reacting with isocyanate (NCO) groups and also polar functional group(s); (C) 0.1-10 wt.% diamine(s) and/or polyamine(s); (D) 0-20 wt.% other compound(s) with NOTLESS 2 NCO-reactive OH groups or OH and/or primary or secondary amino groups; (E) 0-20 wt.% other compound(s) with an NCO-reactive group; and (F) 10-50 wt.% polyisocyanate(s). The novelty is that the sum of the OH numbers of components (A) and (D) is 121-300 mg KOH/g. Independent claims are also included for (a) (I) dispersions; and (b) the production of (I) in which the polymers are prepared by (1) reacting components (A), (B), (F) and optionally (D) and/or (E) with an NCO polyurethane prepolymer; (2) optionally ionizing the ionogenic polar functional groups by neutralization and/or quaternization; (3) reacting the NCO prepolymer with (C) and optionally (E) to give a product free from NCO groups and optionally dispersing the product in water; and optionally (4) drying the reaction product, preferably by spray drying.

    49.
    发明专利
    未知

    公开(公告)号：DE50010494D1

    公开(公告)日：2005-07-14

    申请号：DE50010494

    申请日：2000-07-13

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  MENZEL KLAUS ,  REICH WOLFGANG

    IPC: C08G18/08 ,  C08G18/67 ,  C08G18/72 ,  C09D175/04 ,  C09D175/14

    Abstract: A curable polyurethane polymer comprises a hydroxyl group containing prepolymer, a compound having a hydroxyl group and/or prim. or sec. amine group and a compound having at least 2 isocyanate groups and/or their salts whereby the ratio of isocyanate group equivalents to isocyanate reactive groups is 0.4:1-0.9:1. A curable polyurethane polymer (I) comprises: (A) 10-60 wt.% of a hydroxyl group containing prepolymer having at least a thermally or photochemically polymerizable alpha , beta -ethylenically unsaturated double bond (B) 0.1-30 wt.% of a compound having a hydroxyl group and/or prim. or sec. amine group that is reactive towards an isocyanate group and having at least one polar functional group per molecule; (C) 0.1-30 wt.% of a diamine and/or polyamine; (D) 0-10 wt.% of a compound, different to (A), (B), (C) and (E) having at least 2 isocyanate reactive groups and containing hydroxyl and/or prim. and/or sec. amine groups; (E) 0-20 wt.% of a compound having one isocyanate reactive group; (F) 10-65 wt.% of a compound having at least 2 isocyanate groups and/or their salts whereby the ratio of isocyanate group equivalents in (F) to isocyanate reactive groups is (A)-(E) is 0.4:1-0.9:1. Independent claims are included for: (i) a polymer dispersion containing (I); and (ii) a coating agent containing (I).

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