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    PRODUCTION OF (METH)ACRYLIC ESTER
    3.
    发明专利
    PRODUCTION OF (METH)ACRYLIC ESTER 失效

    公开(公告)号：JP2001026569A

    公开(公告)日：2001-01-30

    申请号：JP2000187845

    申请日：2000-06-22

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  REICH WOLFGANG DR ,  BECK ERICH ,  JAWOREK THOMAS ,  KOENIGER RAINER DR

    IPC: B01J31/30 ,  C07B61/00 ,  C07C67/08 ,  C07C67/60 ,  C07C67/62 ,  C07C69/54

    Abstract: PROBLEM TO BE SOLVED: To provide a method for easily producing a (meth)acrylic ester by which a light color esterification product is obtained in high yield. SOLUTION: This method for producing a (meth)acrylic ester comprises esterifying acrylic acid and/or methacrylic acid with at least one compound having at least one alcoholic hydroxyl group while adding to the reaction system a hydrocarbon with a boiling point of 60-140 deg.C as a water azeotropic agent at 90-150 deg.C in the presence of an acidic esterification catalyst and a polymerization inhibitor, and after esterification, distilling the water azeotropic agent and excess (meth)acrylic acid off at 90-150 deg.C under a normal or reduced pressure, and if necessary, neutralizing the product obtained after distillation with at least one basic inorganic compound, wherein a copper (II) salt or a mixture composed of the copper (II) salt and a copper (I) salt to be deposited after esterification as a copper sulfide and separated is used as the polymerization inhibitor.

    HARDENABLE POLYURETHANE POLYMER, DISPERSION AND COATING MATERIAL COMPRISING THE SAME, PRODUCTION OF POLYMER AND USE OF DISPERSION
    4.
    发明专利
    HARDENABLE POLYURETHANE POLYMER, DISPERSION AND COATING MATERIAL COMPRISING THE SAME, PRODUCTION OF POLYMER AND USE OF DISPERSION 失效

    公开(公告)号：JPH11315130A

    公开(公告)日：1999-11-16

    申请号：JP6701599

    申请日：1999-03-12

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  KOENIGER RAINER ,  REICH WOLFGANG ,  MENZEL KLAUS

    IPC: C08L75/04 ,  C08G18/08 ,  C08G18/32 ,  C08G18/67 ,  C08G18/68 ,  C09D175/04 ,  C09D175/14

    Abstract: PROBLEM TO BE SOLVED: To obtain a hardenable polyurethane polymer capable of providing an unhardened and dried coating film hardenable by radiation and having a good pendulum hardness, a high hardness and scratch resistance, and further capable of providing a hardened film having a high hardness and good flexibility by including a specific hydroxy-containing prepolymer in a specified proportion in a copolymerized state. SOLUTION: This hardenable polyurethane polymer comprises (A) 40-80 wt.% one or more kinds of OH group-containing prepolymers having one or more radically or photochemically polymerizable α,β-ethylenically unsaturated double bonds (based on the whole weight), (B) 0.1-20 wt.% one or more kinds of compounds having one or more isocyanate-reactive OH groups and/or primary or secondary amino groups, and further one or more polar functional groups, (C) 0.1-10 wt.% compound selected from a diamine, a polyamine and a mixture thereof, and (D) 10-50 wt.% one or more kinds of polyisocyanates in a copolymerized state. The OH value of the components A to C is 121-300 mg- KOH/g.

    PHASE SEPARATION OF ORGANIC-WATER SYSTEM
    6.
    发明专利
    PHASE SEPARATION OF ORGANIC-WATER SYSTEM 失效

    公开(公告)号：JPH11269127A

    公开(公告)日：1999-10-05

    申请号：JP1868099

    申请日：1999-01-27

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  GEISENDOERFER MATTHIAS

    IPC: C07C67/08 ,  C07C67/52 ,  C07C67/58 ,  C07C67/62 ,  C07C69/54

    Abstract: PROBLEM TO BE SOLVED: To provide a method for separating an organic phase and an aqueous phase produced by an esterification. SOLUTION: At least one organic polymeric, anionic and water-soluble flocculant is used in a method for the phase separation of an organic-aqueous system containing unreacted residues of a carboxylic acid anhydride, a carboxylic acid or an alcohol used for producing an acrylate, a diacrylate, a (poly)ester acrylate or a (poly)ether acrylate and an acrylate which are substantially monomers. The flocculant is selected from a functional high-molecular weight polymer containing a carboxylic acid, a sulfonic acid, a phosphoric acid and/or a phosphonic acid functional groups and an anionic-modified polyacrylamide is preferred. The anionic flocculant has 4-22 Mda molecular weight.

    METHOD FOR THE PRODUCTION OF COATINGS, ADHESIVE LAYERS OR SEALS FOR PRIMED OR UNPRIMED SUBSTRATES
    7.
    发明申请
    METHOD FOR THE PRODUCTION OF COATINGS, ADHESIVE LAYERS OR SEALS FOR PRIMED OR UNPRIMED SUBSTRATES 审中-公开
    用于生产涂料，粘合剂膜或密封件涂底漆或未涂底漆的基材

    公开(公告)号：WO0156431A3

    公开(公告)日：2002-03-14

    申请号：PCT/EP0101085

    申请日：2001-02-01

    Applicant: BASF AG ,  BLUM RAINER ,  PAULUS WOLFGANG ,  SCHWALM REINHOLD

    Inventor： BLUM RAINER ,  PAULUS WOLFGANG ,  SCHWALM REINHOLD

    IPC: B05D3/02

    CPC classification number: C09J133/08 ,  B05D3/0209 ,  B05D3/0263 ,  C09D133/08

    Abstract: The invention concerns a method for the production of coatings, adhesive layers or seals for primed or unprimed substrates, wherein (1) at least one coating material that can be hardened thermally and/or with actinic radiation and/or an adhesive and/or at least one sealant that can be hardened thermally and/or with actinic radiation in the form of a powder slurry is applied on and/or to the primed or unprimed substrate; (2) the resulting powder slurry layer is dried; (3) the resulting solid layer (2) is molten by heating and (4) the resulting molten layer obtained in step (3) of the method is hardened with near infrared radiation (NIR) in its molten state during and/or after solidification.

    Abstract translation: 一种用于生产涂料，粘合剂膜或密封件涂底漆或未涂底漆的基材，它包括：（1）至少一种热和/或光化辐射涂层和/或粘合剂和/或至少一个热和/或可固化的光化辐射密封剂härbaren过程 在上和/或在grundiete或未涂底漆的基材施加，（2）干燥得到的粉末淤浆层的粉末浆料的形式，（3）熔化所得固体膜（2）通过加热，并在处理步骤（4）（3） 所得和/或近红外辐射（NIR辐射）固化固化后在熔融状态下熔融层，在凝固过程中。

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