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    COPOLYMERIZABLE ETHYLENIC UNSATURATED-GROUP CONTAINING COMPOUND FOR AQUEOUS DISPERSANT AND ITS STABILIZER
    1.
    发明专利
    COPOLYMERIZABLE ETHYLENIC UNSATURATED-GROUP CONTAINING COMPOUND FOR AQUEOUS DISPERSANT AND ITS STABILIZER 失效

    公开(公告)号：JPH1060223A

    公开(公告)日：1998-03-03

    申请号：JP9039197

    申请日：1997-04-09

    Applicant: BASF AG

    Inventor： HAEUSLING LUKAS DR ,  KOCH ANDREAS DR ,  LEBKUECHER WERNER

    IPC: C07D211/94 ,  C08F2/40 ,  C08J3/03 ,  C08K5/3432 ,  C08K5/3435 ,  C08K5/353 ,  C08L57/00 ,  C08L75/16 ,  C09D7/45 ,  C09D175/14

    Abstract: PROBLEM TO BE SOLVED: To obtain a dispersion of a copolymerizable ethylenic unsaturated- group containing compound that if prepared to have an excellent storage stability of polymer particles without coagulation of the dispersion by containing a specific stabilizer and useful for production of coatings, etc. SOLUTION: This copolymerizable ethylenic unsaturated-group containing compound contains, out of stabilizers of formula I [(m) is 1-100; R and R are each a 1-4C alkyl, phenyl, etc.; R3 is H, hydroxyl, a primary amino, etc,; R is H, a 1-12C alkyl, etc.)] that have one or more piperidine-N-oxide groups tetra-substituted in their 2, 2, 6, and 6 sites, a stabilizer of formula II, etc., preferably in a quantity of 0,.001-0.5wt.% based on the above copolymerizable ethylenic unsaturated-group containing compound, which is preferably polyurethane, the content of ethylenic unsaturated groups of which is preferably 0.005-0.4mol based on 100g of the polyurethane.

    HARDENABLE POLYURETHANE POLYMER, DISPERSION AND COATING MATERIAL COMPRISING THE SAME, PRODUCTION OF POLYMER AND USE OF DISPERSION
    2.
    发明专利
    HARDENABLE POLYURETHANE POLYMER, DISPERSION AND COATING MATERIAL COMPRISING THE SAME, PRODUCTION OF POLYMER AND USE OF DISPERSION 失效

    公开(公告)号：JPH11315130A

    公开(公告)日：1999-11-16

    申请号：JP6701599

    申请日：1999-03-12

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  KOENIGER RAINER ,  REICH WOLFGANG ,  MENZEL KLAUS

    IPC: C08L75/04 ,  C08G18/08 ,  C08G18/32 ,  C08G18/67 ,  C08G18/68 ,  C09D175/04 ,  C09D175/14

    Abstract: PROBLEM TO BE SOLVED: To obtain a hardenable polyurethane polymer capable of providing an unhardened and dried coating film hardenable by radiation and having a good pendulum hardness, a high hardness and scratch resistance, and further capable of providing a hardened film having a high hardness and good flexibility by including a specific hydroxy-containing prepolymer in a specified proportion in a copolymerized state. SOLUTION: This hardenable polyurethane polymer comprises (A) 40-80 wt.% one or more kinds of OH group-containing prepolymers having one or more radically or photochemically polymerizable α,β-ethylenically unsaturated double bonds (based on the whole weight), (B) 0.1-20 wt.% one or more kinds of compounds having one or more isocyanate-reactive OH groups and/or primary or secondary amino groups, and further one or more polar functional groups, (C) 0.1-10 wt.% compound selected from a diamine, a polyamine and a mixture thereof, and (D) 10-50 wt.% one or more kinds of polyisocyanates in a copolymerized state. The OH value of the components A to C is 121-300 mg- KOH/g.

    Radiation-hardenable aqueous polyurethane dispersion, useful as coating mass, comprises: compounds e.g. with free isocyanides-, reactive isocyanides- and acid groups; basic compounds; polyisocyanates; additives; water; and di-/polyamines
    7.
    发明专利
    Radiation-hardenable aqueous polyurethane dispersion, useful as coating mass, comprises: compounds e.g. with free isocyanides-, reactive isocyanides- and acid groups; basic compounds; polyisocyanates; additives; water; and di-/polyamines 未知

    公开(公告)号：DE102005008932A1

    公开(公告)日：2006-08-31

    申请号：DE102005008932

    申请日：2005-02-24

    Applicant: BASF AG

    Inventor： HEISCHKEL YVONNE ,  LARBIG HARALD ,  LEBKUECHER WERNER ,  SCHWALM REINHOLD ,  GRUBER NICK

    IPC: C08G83/00 ,  C08G18/80 ,  C08G18/81 ,  C08G85/00 ,  C09D175/04

    Abstract: Radiation-hardenable aqueous polyurethane dispersion (A) comprises: a compound with two free isocyanate-, allophanate (bonded) group, radical polymerized C=C double bond; compound with isocyanate reactive group and radical polymerized C=C double bond; optionally compound with at least two isocyanate reactive groups; compound with isocyanate reactive- and acid group; basic compound; optionally a different compound that has isocyanate reactive group; water; optionally: different polyisocyanate; additives and di- and/or polyamine (where (A) does not contain thermal initiators). Radiation-hardenable aqueous polyurethane dispersion (A) comprises: (a) at least one compound with at least two free isocyanate group, at least one (bound) allophanate group, and radical polymerized C=C double bond, which is directly bounded to double bond of a carbonyl group or oxygen atom in bound ether group; (b) at least one compound with at least one isocyanate reactive group and at least one radical polymerized C=C double bond; (c) optionally at least one compound with at least two isocyanate reactive group of hydroxyl-, mercapto-, primary- and/or secondary amino groups; (d) at least one compound with at least one isocyanate reactive group and at least one acid group; (e) at least one basic compound of partially neutralized acid groups of (d); (f) optionally compound of (b), (d) and/or (e) that has only one isocyanate reactive group; (g) optionally at least one different polyisocyanate of (a); (h) optionally further additives such as reactive solvents, photo initiators or lacquer additives; (i) water; and (j) optionally at least one di- and/or polyamine (where (A) does not contain thermal initiators). Independent claims are included for: (1) a coated substrate comprising (A); and (2) a method for coating substrates comprising applying (A) on the substrate, drying and radiation hardening.

    8.
    发明专利
    未知

    公开(公告)号：AT297423T

    公开(公告)日：2005-06-15

    申请号：AT00115226

    申请日：2000-07-13

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  MENZEL KLAUS ,  REICH WOLFGANG

    IPC: C08G18/08 ,  C08G18/67 ,  C08G18/72 ,  C09D175/04 ,  C09D175/14

    Abstract: A curable polyurethane polymer comprises a hydroxyl group containing prepolymer, a compound having a hydroxyl group and/or prim. or sec. amine group and a compound having at least 2 isocyanate groups and/or their salts whereby the ratio of isocyanate group equivalents to isocyanate reactive groups is 0.4:1-0.9:1. A curable polyurethane polymer (I) comprises: (A) 10-60 wt.% of a hydroxyl group containing prepolymer having at least a thermally or photochemically polymerizable alpha , beta -ethylenically unsaturated double bond (B) 0.1-30 wt.% of a compound having a hydroxyl group and/or prim. or sec. amine group that is reactive towards an isocyanate group and having at least one polar functional group per molecule; (C) 0.1-30 wt.% of a diamine and/or polyamine; (D) 0-10 wt.% of a compound, different to (A), (B), (C) and (E) having at least 2 isocyanate reactive groups and containing hydroxyl and/or prim. and/or sec. amine groups; (E) 0-20 wt.% of a compound having one isocyanate reactive group; (F) 10-65 wt.% of a compound having at least 2 isocyanate groups and/or their salts whereby the ratio of isocyanate group equivalents in (F) to isocyanate reactive groups is (A)-(E) is 0.4:1-0.9:1. Independent claims are included for: (i) a polymer dispersion containing (I); and (ii) a coating agent containing (I).

    9.
    发明专利
    未知

    公开(公告)号：DE59909876D1

    公开(公告)日：2004-08-12

    申请号：DE59909876

    申请日：1999-03-11

    Applicant: BASF AG

    Inventor： PAULUS WOLFGANG ,  LEBKUECHER WERNER ,  KOENIGER RAINER ,  REICH WOLFGANG ,  MENZEL KLAUS

    IPC: C08L75/04 ,  C08G18/08 ,  C08G18/32 ,  C08G18/67 ,  C08G18/68 ,  C09D175/04 ,  C09D175/14 ,  C09D175/16

    Abstract: Curable polyurethane polymers (I) and their salts are novel in that the sum of the OH numbers of a component comprising a prepolymer(s) containing hydroxyl groups with ethylenically unsaturated double bond(s) capable of free radical photochemical polymerization, and a component containing isocyanate-reactive hydroxy groups or hydroxy groups and/or amino groups, is 121-300 mg KOH/g. Curable polyurethane polymers (I) and their salts comprise (A) 40-80 wt.% prepolymer(s) containing hydroxyl (OH) groups with alpha , beta -ethylenically unsaturated double bond(s) capable of free radical photochemical polymerization; (B) 0.1-20 wt.% compound(s) containing OH and/or primary or secondary amino group(s) reacting with isocyanate (NCO) groups and also polar functional group(s); (C) 0.1-10 wt.% diamine(s) and/or polyamine(s); (D) 0-20 wt.% other compound(s) with NOTLESS 2 NCO-reactive OH groups or OH and/or primary or secondary amino groups; (E) 0-20 wt.% other compound(s) with an NCO-reactive group; and (F) 10-50 wt.% polyisocyanate(s). The novelty is that the sum of the OH numbers of components (A) and (D) is 121-300 mg KOH/g. Independent claims are also included for (a) (I) dispersions; and (b) the production of (I) in which the polymers are prepared by (1) reacting components (A), (B), (F) and optionally (D) and/or (E) with an NCO polyurethane prepolymer; (2) optionally ionizing the ionogenic polar functional groups by neutralization and/or quaternization; (3) reacting the NCO prepolymer with (C) and optionally (E) to give a product free from NCO groups and optionally dispersing the product in water; and optionally (4) drying the reaction product, preferably by spray drying.

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