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51.发明专利
公开(公告)号：UA87389C2
公开(公告)日：2009-07-10
申请号：UAA200713656
申请日：2006-05-02
Applicant: BASF AG
Inventor： OFTRING ALFRED , BRAUN GEROLD , WIRSING FRIEDRICH , STAMM ARMIN , BALDENIUS KAI-UWE
IPC: C07C227/00 , C07C229/16
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52.发明专利
公开(公告)号：CA2607232A1
公开(公告)日：2006-11-16
申请号：CA2607232
申请日：2006-05-02
Applicant: BASF AG
Inventor： BRAUN GEROLD , OFTRING ALFRED , BALDENIUS KAI-UWE , STAMM ARMIN , WIRSING FRIEDRICH
IPC: C07C227/26 , C07C229/16
Abstract: The invention relates to a process for preparing low-by-product, light-color methylglycine-N,N-diacetic acid tri(alkali metal) salt by alkaline hydrolysis of methylglycinediacetonitrile (MGDN), comprising the steps in the sequence (a) to (f): (a) mixing of MGDN with aqueous alkali at a temperature of ≦̸30° C.; (b) allowing the aqueous alkaline MGDN suspension to react at a temperature in the range from 10 to 30° C. over a period of from 0.1 to 10 h to form a solution; (c) allowing the solution from step (b) to react at a temperature in the range from 30 to 40° C. over a period of from 0.1 to 10 h; (d) optionally allowing the solution from step (c) to react at a temperature in the range from 50 to 80° C. over a period of from 0.5 to 2 h; (e) optionally allowing the solution from step (c) or (d) to react at a temperature in the range from 110 to 200° C. over a period of from 5 to 60 min; (f) hydrolysis and removal of ammonia of the solution obtained in step (c), (d) or (e) by stripping at a temperature of from 90 to 105° C.
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53.发明专利
公开(公告)号：AU2006245816A1
公开(公告)日：2006-11-16
申请号：AU2006245816
申请日：2006-05-02
Applicant: BASF AG
Inventor： BRAUN GEROLD , STAMM ARMIN , WIRSING FRIEDRICH , OFTRING ALFRED , BALDENIUS KAI-UWE
IPC: C07C227/26 , C07C229/16
Abstract: The invention relates to a process for preparing low-by-product, light-color methylglycine-N,N-diacetic acid tri(alkali metal) salt by alkaline hydrolysis of methylglycinediacetonitrile (MGDN), comprising the steps in the sequence (a) to (f): (a) mixing of MGDN with aqueous alkali at a temperature of ≦̸30° C.; (b) allowing the aqueous alkaline MGDN suspension to react at a temperature in the range from 10 to 30° C. over a period of from 0.1 to 10 h to form a solution; (c) allowing the solution from step (b) to react at a temperature in the range from 30 to 40° C. over a period of from 0.1 to 10 h; (d) optionally allowing the solution from step (c) to react at a temperature in the range from 50 to 80° C. over a period of from 0.5 to 2 h; (e) optionally allowing the solution from step (c) or (d) to react at a temperature in the range from 110 to 200° C. over a period of from 5 to 60 min; (f) hydrolysis and removal of ammonia of the solution obtained in step (c), (d) or (e) by stripping at a temperature of from 90 to 105° C.
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公开(公告)号：ES2250371T3
公开(公告)日：2006-04-16
申请号：ES01919355
申请日：2001-02-28
Applicant: BASF AG
Inventor： STAMM ARMIN , KNEUPER HEINZ-JOSEF , HENKELMANN JOCHEM , WEBER THEODOR , BUSCH RALPH
Abstract: Procedimiento para la obtención de cloruros de los ácidos clorocarboxílicos de la fórmula (I) en la que R1 y R2 significan, independientemente entre sí, un átomo de hidrógeno, un resto alifático, aromático o aralifático insubstituido o substituido, con 1 hasta 20 átomos de carbono, un halógeno, un grupo nitro o un grupo ciano, e Y significa una cadena alquileno con 1 hasta 10 átomos de carbono en la cadena, que está insubstituida o que está substituida por restos alifáticos, aromáticos o aralifáticos, insubstituidos o substituidos, con 1 hasta 20 átomos de carbono, por halógeno, por grupos nitros y/o por grupos ciano, pudiendo estar interrumpida la cadena alquileno por un grupo éter, por un grupo tioéter, por un grupo amino terciario o por un grupo ceto, pudiendo estar enlazados entre sí los citados restos alifáticos, aromáticos o aralifáticos, insubstituidos o substituidos, con 1 hasta 20 átomos de carbono de Y y/o de R1 y/o de R2, formando un sistema no aromático, caracterizado porquese hace reaccionar una lactona de la fórmula (II) en la que R1, R2 e Y tienen el significado precedentemente indicado, con cloruro de hidrógeno y fosgeno en presencia de un catalizador, caracterizado porque se alimenta cloruro de hidrógeno antes y/o durante la adición de fosgeno, comenzándose con la introducción de cloruro de hidrógeno solamente a partir de una temperatura de 60ºC, como mínimo, y empleándose como catalizador un compuesto de piridina.
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公开(公告)号：DE50205702D1
公开(公告)日：2006-04-13
申请号：DE50205702
申请日：2002-04-17
Applicant: BASF AG
Inventor： STAMM ARMIN , KNEUPER HEINZ-JOSEF , RITTINGER STEFAN , DRANSFELD PETER , SCHILDBERG HANS-PETER , HEILIG MANFRED , WEBER THEODOR
Abstract: A method is provided for the intrinsically safe handling of 3-chloropropyne in the presence of a diluent with a boiling point ranging from -50° C. (223 K) to 200° C. (473 K) under atmospheric pressure, wherein the concentration of 3-chloropropyne in the liquid phase and in the gas phase is kept below the concentrations capable of deflagration by means of the type and amount of the diluent, the temperature and the total system pressure, together with the use of a 3-chloropropyne prepared, stored or transported in this way in the synthesis of dyestuffs, pharmaceutical and agricultural active ingredients, electroplating auxiliaries, disinfectants, steroids and growth hormones.
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Patent Agency Ranking
公开(公告)号：PL357602A1
公开(公告)日：2004-07-26
申请号：PL35760200
申请日：2000-11-27
Applicant: BASF AG
Inventor： STAMM ARMIN , GOTZ ROLAND , GOTZ NORBERT , HENKELMANN JOCHEM , KNEUPER HEINZ-JOSEF , WOLF BERND
Abstract: The invention relates to a method for producing o-choromethyl benzenecarbonyl chlorides of formula (I), wherein R -R can be the same or different and stand for hydrogen, C1-C4-alkyl, halogen or trifluoromnethyl, by converting benzocondensed lactones of formula (II), wherein R -R have the aforementioned meaning, with gaseous or liquid phosgene and the dimers or trimers thereof. The inventive method is characterized in that the conversion is carried out in the presence of catalytical amounts of a Lewis acid and catalytical amounts of a phosgenation catalyst
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公开(公告)号：CZ20032891A3
公开(公告)日：2004-04-14
申请号：CZ20032891
申请日：2002-04-17
Applicant: BASF AG
Inventor： STAMM ARMIN , KNEUPER HEINZ JOSEF , RITTINGER STEFAN , DRANSFELD PETER , SCHILDBERG HANS PETER , HEILIG MANFRED , WEBER THEODOR
Abstract: A method is provided for the intrinsically safe handling of 3-chloropropyne in the presence of a diluent with a boiling point ranging from -50° C. (223 K) to 200° C. (473 K) under atmospheric pressure, wherein the concentration of 3-chloropropyne in the liquid phase and in the gas phase is kept below the concentrations capable of deflagration by means of the type and amount of the diluent, the temperature and the total system pressure, together with the use of a 3-chloropropyne prepared, stored or transported in this way in the synthesis of dyestuffs, pharmaceutical and agricultural active ingredients, electroplating auxiliaries, disinfectants, steroids and growth hormones.
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公开(公告)号：DE50005355D1
公开(公告)日：2004-03-25
申请号：DE50005355
申请日：2000-11-27
Applicant: BASF AG
Inventor： GOETZ ROLAND , GOETZ NORBERT , KEIL MICHAEL , WOLF BERND , STEINMETZ ADRIAN , STAMM ARMIN , HENKELMANN JOCHEM
Abstract: A process for preparing o-chloromethylbenzoyl chlorides of the formula I,in which R to R can be identical or different and are hydrogen, C1-C4-alkyl, halogen or trifluoromethyl, by reacting benzo-fused lactones of the formula II,in which R to R are as defined above, with thionyl chloride, which comprises carrying out the reaction in the presence of catalytic amounts of boric acid, boric anhydride, borate, boronic acid or boronic acid esters and catalytic amounts of a quaternary ammonium salt is described.
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公开(公告)号：ES2201685T3
公开(公告)日：2004-03-16
申请号：ES99911747
申请日：1999-03-08
Applicant: BASF AG
Inventor： STAMM ARMIN , HENKELMANN JOCHEM , WEYER HANS-JURGEN
Abstract: The invention relates to a continuous method for producing propargyl chloride by reacting propargyl alcohol with a chlorinating agent in the presence of a catalyst. According to the invention, the chlorinating agent, propargyl alcohol and 0.1 to 10 mol.% of the catalyst with regard to the amount of propargyl alcohol is continuously dosed in a reaction zone and is reacted at a temperature ranging from 40 to 70 DEG C.
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公开(公告)号：AT259770T
公开(公告)日：2004-03-15
申请号：AT00987303
申请日：2000-11-27
Applicant: BASF AG
Inventor： GOETZ ROLAND , GOETZ NORBERT , KEIL MICHAEL , WOLF BERND , STEINMETZ ADRIAN , STAMM ARMIN , HENKELMANN JOCHEM
Abstract: A process for preparing o-chloromethylbenzoyl chlorides of the formula I,in which R to R can be identical or different and are hydrogen, C1-C4-alkyl, halogen or trifluoromethyl, by reacting benzo-fused lactones of the formula II,in which R to R are as defined above, with thionyl chloride, which comprises carrying out the reaction in the presence of catalytic amounts of boric acid, boric anhydride, borate, boronic acid or boronic acid esters and catalytic amounts of a quaternary ammonium salt is described.
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