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    BENZYLIDENE PYRAZOLONES, PRODUCTION AND USE THEREOF
    2.
    发明申请
    BENZYLIDENE PYRAZOLONES, PRODUCTION AND USE THEREOF 审中-公开
    BENZYLIDENPYRAZOLONE，生产和使用

    公开(公告)号：WO9926930A2

    公开(公告)日：1999-06-03

    申请号：PCT/EP9807099

    申请日：1998-11-06

    Applicant: BASF AG ,  RHEINHEIMER JOACHIM ,  WITSCHEL MATTHIAS ,  ENGEL STEFAN ,  BAUMANN ERNST ,  DEYN WOLFGANG VON ,  HILL REGINA LUISE ,  MAYER GUIDO ,  MISSLITZ ULF ,  WAGNER OLIVER ,  OTTEN MARTINA ,  WESTPHALEN KARL OTTO ,  WALTER HELMUT

    Inventor： RHEINHEIMER JOACHIM ,  WITSCHEL MATTHIAS ,  ENGEL STEFAN ,  BAUMANN ERNST ,  VON DEYN WOLFGANG ,  HILL REGINA LUISE ,  MAYER GUIDO ,  MISSLITZ ULF ,  WAGNER OLIVER ,  OTTEN MARTINA ,  WESTPHALEN KARL-OTTO ,  WALTER HELMUT

    IPC: A01N43/56 ,  A01N43/78 ,  A01N43/80 ,  C07D231/16 ,  C07D231/20 ,  C07D401/10 ,  C07D403/10 ,  C07D405/10 ,  C07D409/10 ,  C07D413/06 ,  C07D413/10 ,  C07D417/10 ,  C07D231/18

    CPC classification number: C07D413/06 ,  A01N43/56 ,  A01N43/78 ,  A01N43/80 ,  C07D231/16 ,  C07D231/20

    Abstract: The invention relates to benzylidene pyrazolones of formula (I), wherein the substituents and index n have the following meanings: R = optionally substituted C1-C6 alkyl; R = optionally substituted C1-C6 alkyl, optionally substituted C1-C6 alkoxy, halogen, nitro, cyano; R = hydrogen, halogen, nitro, cyano, a group NR R , OCOR , NR COR ,CO2R , -COSR , -CONR R , C1-C4-alkoxyiminoalkyl, C1-C6 alkoxycarbonyl, optionally substituted C1-C6 alkyl, optionally substituted C1-C6 alkoxy, optionally substituted C1-C6 alkylthio, optionally substituted C2-C6 alkenyl, optionally substituted phenyl, optionally substituted phenoxy, an optionally substituted 5- or 6-membered saturated or unsaturated heterocycle which can contain up to 4 nitrogen atoms and/or up to 2 oxygen or sulphur atoms as ring members; R = C1-C6 alkyl, C1-C4 halogen alkyl; or R and R = an optionally substituted saturated or unsaturated 2- or 3-membered bridge which can contain one sulphur atom which can be oxidized into sulfoxide or sulfone, R = hydrogen or optionally substituted C1-C6 alkyl; R = hydrogen, C1-C6 alkyl or C1-C4 halogenalkyl; n = 0, 1 or 2; X = hydrogen, chlorine or bromine. The compounds to which claim is laid are available in both a trans and a cis form or can be a mixture of these isomers.

    Abstract translation: 式（I）的Benzylidenpyrazolone其中取代基和指数n具有以下含义：R t <1>是未取代的或取代的。 C1-C6烷基; [R <2>是未取代的或取代的。 C1-C6烷基，未取代或取代的。 C1-C6烷氧基，卤素，硝基，氰基; [R <3>是氢，卤素，硝基，氰基，基团NR <5> - [R <6>，OCOR <5>，NR <5> COR <6>，CO 2 <5>，-COSR <5>，-CONR <5> - [R <6>，C1-C4-alkoxyiminoalkyl，C1-C6烷基羰基，未取代的或取代的。 C1-C6烷基，未取代或取代的。 C1-C6烷氧基，未取代的或取代的。 C1-C6烷硫基，未取代或取代的。 C2-C6链烯基，未取代的或取代的。 C2-C6炔基，未取代的或取代的。 苯基，未取代的或取代的。 苯氧基，未取代的或取代的。 5-或6-元饱和或可含有至多4个氮原子和/或至多2个氧或硫原子作为环成员的不饱和的杂环; [R <4> C1-C6-烷基，C1-C4卤代烷基; 或R <3>，R <4>为可以含有可被氧化为亚砜或砜硫原子的任选取代的饱和或不饱和2-或3-元桥; [R <5>为氢或未取代或取代的。 C1-C6烷基; [R <6>是未取代的或取代的。 C1-C6烷基; [R <7>是氢，C1-C6烷基或C1-C4卤代烷基; n为0.1或2; X是氢，氯或溴; 其中要求保护的化合物在跨及在所述顺式 - 形式两者呈现，或者可以是这些异构体的混合物。

    processo para preparar bifenilas substituídas
    4.
    发明专利
    processo para preparar bifenilas substituídas 未知

    公开(公告)号：BRPI0607424B1

    公开(公告)日：2015-09-29

    申请号：BRPI0607424

    申请日：2006-03-02

    Applicant: BASF AG ,  BASF SE

    Inventor： ENGEL STEFAN ,  OBERDING TANJA

    IPC: C07C201/12 ,  C07C205/12

    Abstract: processo para preparar bifenilas substituídas. a invenção se refere a um processo para produzir bifenilas substituidas (1) nos quais: r é nitro, amino ou nhr~ 3~; r^ 2^ é ciano, nitro, halogênio, alquila c~ 1~-c~ 6~, alquenila c~ 2~-c~ 6~, alquinila c~ 2~-c~ 6~, alcóxi c~ 1~-c~ 6~, haloalquila c~ 1~-c~ 6~, (c~ 1~-c~ 6~-alquil)carbonila ou fenila; r^ 3^ é alquila c~ 1~-c~ 4~, alquenila c~ 2~-c~ 4~ ou alquinila c~ 2~-c~ 4~; m é 1 ou 2,; n = o a 3. a invenção é caracterizada em que um composto (ii) é reagido com um ácido difenil borínico (iii) na presença de uma base e de um catalisador de paládio selecionado do grupo que consiste de: a) complexo de trialquilfosfina ou trialquilfosfina-paládio com paládio sendo zero no estado de oxidação; b) sal do paládio na presença de triarilfosfina ou trialquilfosfina servindo como um ligante complexo ou; c) opcionalmente paládio metálico elevada com substratos, na presença de triarilfosfina ou trialquilfosfina em um solvente.

    5.
    发明专利
    未知

    公开(公告)号：EE05291B1

    公开(公告)日：2010-04-15

    申请号：EEP9900292

    申请日：1998-01-08

    Applicant: BASF AG

    Inventor： HILL REGINA LUISE ,  DEYN WOLFGANG VON ,  BAUMANN ERNST ,  ENGEL STEFAN ,  MAYER GUIDO ,  RHEINHEIMER JOACHIM ,  WITSCHEL MATTHIAS ,  MISSLITZ ULF ,  WAGNER OLIVER ,  OTTEN MARTINA ,  WALTER HELMUT ,  WESTPHALEN KARL-OTTO

    IPC: A01N43/48 ,  C07D277/10 ,  A01N43/18 ,  A01N43/56 ,  A01N43/72 ,  A01N43/76 ,  A01N43/78 ,  A01N43/80 ,  C07D231/20 ,  C07D231/24 ,  C07D261/04 ,  C07D261/20 ,  C07D263/10 ,  C07D273/00 ,  C07D277/20 ,  C07D277/34 ,  C07D291/04 ,  C07D401/10 ,  C07D403/10 ,  C07D405/10 ,  C07D409/10 ,  C07D411/10 ,  C07D413/10 ,  C07D417/10 ,  C07D419/10 ,  C07D498/10

    Abstract: 4-(3-Heterocyclyl-benzoyl)-pyrazole derivatives (I) and their salts are new: R1, R3 = H; NO2; halo; CN; 1-6C alkyl, 1-6C alkoxy, 1-6C alkylthio, 1-6C alkylsulphinyl or 1-6C alkylsulphonyl optionally substituted by halo; H2NSO2; (1-6C alkyl)NHSO2; (1-6C alkyl)2NSO2; (1-6C alkyl)SO2NH-; (1-6C haloalkyl-SO2)NH-; (1-6C alkyl)(1-6C alkyl-SO2)N-; or (1-6C haloalkyl)(1-6C alkyl-SO2)N-; R2 = optionally substituted 5- or 6-membered heterocycle containing 1-4 O, S and/or N atoms; R6 = 1-6C alkyl; R7 = 1-6C alkyl; 3-6C alkenyl or 3-6C alkynyl optionally substituted by halo; 3-6C cycloalkyl; 1-6C alkylcarbonyl; 2-6C alkenylcarbonyl; 2-6C alkynylcarbonyl; 3-6C cycloalkylcarbonyl; 1-6C alkoxycarbonyl; 3-6C alkenyloxycarbonyl; 3-6C alkynyloxycarbonyl; 1-6C alkyl-NH-CO-; 3-6C alkenyl-NH-CO-; 3-6C alkynyl-NH-CO-; (1-6C alkyl)2N-CO-; (3-6C alkenyl)(1-6C alkyl)N-CO-carbonyl; (3-6C alkynyl)(1-6C alkyl)N-CO-; (1-6C alkoxy)(1-6C alkyl)N-CO-; (3-6C alkenyl)(1-6C alkoxy)N-CO-; (3-6C alkynyl)(1-6C alkoxy)N-CO-; (1-6C alkyl)2N-CS-; 1-6C alkoxyimino-1-6C alkyl; 1-6C alkylamino imino-1-6C alkyl; or di(1-6C alkylamino)imino-1-6C alkyl (alkyl, cycloalkyl and alkoxy groups are optionally substituted by 1 or more halo and/or by 1-3 CN, OH, 1-4C alkoxy, 1-4C alkylthio, di(1-4C alkyl)amino, 1-4C alkylcarbonyl, 1-4C alkoxycarbonyl, 1-4C alkoxy-1-4C alkoxycarbonyl, (1-4C alkyl)2N-1-4C alkoxycarbonyl, COOH, 1-4C alkyl-NH-CO-, (1-4C alkyl)2N-CO-, CONH2; 1-4C alkylcarbonyloxy or 3-6C cycloalkyl); or Ar; Ar-1-6C alkyl; Ar-CO-1-6C alkyl; Ar-CO-; Ar-O-CO-; Ar-NH-CO-; (1-6C alkyl)(Ar)N-CO-; or Ar-2-6C alkenylcarbonyl; Ar = phenyl or heterocyclyl optionally substituted by 1 or more halo and/or by 1-3 NO2, CN or 1-4C alkyl or 1-4C alkoxy (optionally substituted by halo), and R8 = H, 1-6C alkyl or 1-6C haloalkyl.

    8.
    发明专利
    未知

    公开(公告)号：DE59814019D1

    公开(公告)日：2007-07-12

    申请号：DE59814019

    申请日：1998-07-23

    Applicant: BASF AG

    Inventor： ENGEL STEFAN ,  RHEINHEIMER JOACHIM ,  BAUMANN ERNST ,  DEYN WOLFGANG VON ,  HILL REGINA LUISE ,  MAYER GUIDO ,  MISSLITZ ULF ,  WAGNER OLIVER ,  WITSCHEL MATTHIAS ,  OTTEN MARTINA ,  WALTER HELMUT ,  WESTPHALEN KARL-OTTO

    IPC: C07D261/04 ,  C07D333/24 ,  A01N43/08 ,  A01N43/80 ,  C07D207/333 ,  C07D231/12 ,  C07D261/08 ,  C07D263/32 ,  C07D265/06 ,  C07D271/06 ,  C07D271/10 ,  C07D275/02 ,  C07D277/24 ,  C07D285/08 ,  C07D285/12 ,  C07D307/28 ,  C07D307/38 ,  C07D307/40 ,  C07D307/58 ,  C07D333/28

    Abstract: Substituted 2-benzoylcyclohexane-1,3-diones of the formula Iwhere:R1 and R2 are each hydrogen, mercapto, nitro, halogen, cyano, thiocyanato, C1-C6-alkyl, C1-C6-haloalkyl, C1-C6-alkoxy, C2-C6-alkenyl, C2-C6-alkynyl, -OR3, -OCOR3, -OSO2R3, -S(O)nR3, -SO2OR3, -SO2N(R3)2, -NR3SO2R3 or -NR3COR3;R3 is hydrogen, C1-C6-alkyl, C1-C6-haloalkyl, C2-C6-alkenyl, C2-C6-alkynyl, phenyl or phenyl-C1-C6-alkyl; where the abovementioned alkyl radicals may be partially or fully halogenated and/or may carry one to three of the following groups:hydroxyl, mercapto, amino, cyano, R3, -OR3, -SR3, -N(R3)2, =NOR3, -OCOR3, -SCOR3, -NR3COR3, -CO2R3, -COSR3, -CON(R3)2, C1-C4-alkyliminooxy, C1-C4-alkoxyamino, C1-C4-alkylcarbonyl, C1-C4-alkoxy-C2-C6-alkoxycarbonyl, C1-C4-alkylsulfonyl, heterocyclyl, heterocyclyloxy, phenyl, benzyl, hetaryl, phenoxy, benzyloxy and hetaryloxy, where the eight last mentioned radicals may in turn be substituted;n is 0, 1 or 2;Q is a cyclohexane-1,3-dione ring with or without substitution which is attached in position 2;X1 is a straight-chain or branched C1-C6-alkylene, a C2-C6-alkenylene or a C2-C6-alkynylene chain, where the abovementioned alkylene, alkenylene or alkynylene radicals may be partially halogenated and/or may carry one to three of the following groups:-OR4, -OCOR4, -OCONHR4 or -OSO2R4;except for those of the abovementioned alkenylene radicals where the double bond is alpha,beta to the phenyl ring and where Het is linked to the double bond via the beta position;R4 is hydrogen, C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkynyl, phenyl, phenyl-C1-C6-alkyl, where the abovementioned alkyl, alkenyl or alkynyl radicals may be partially or fully halogenated and/or may be substituted by one or more of the following radicals:hydroxyl, mercapto, amino, cyano, nitro, formyl, C1-C4-alkylamino, C1-C4-dialkylamino, C1-C4-alkoxycarbonyl, C1-C4-alkylcarbonyl, C1-C4-alkylcarbonyloxy, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkylthio, C1-C4-haloalkylthio, C1-C4-alkoxy, C1-C4-haloalkoxy;Het is a three- to six-membered partially or fully saturated heterocyclic group or a three- to six-membered heteroaromatic group having up to three hetero atoms selected from the group consisting of:nitrogen, oxygen or sulfur,where the abovementioned heterocyclic or heteroaromatic group may be partially or fully halogenated and/or may be substituted by R5;R5 is hydrogen, hydroxyl, mercapto, amino, cyano, nitro, formyl, C1-C4-alkylamino, C1-C4-dialkylamino, C1-C4-alkoxycarbonyl, C1-C4-alkylcarbonyl, C1-C4-alkylcarbonyloxy, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkylthio, C1-C4-haloalkylthio, C1-C4-alkoxy, C1-C4-haloalkoxy, where the alkyl radicals may in each case be substituted by in each case one or more of the following radicals:cyano, formyl, C1-C4-alkylamino, C1-C4-dialkylamino, C1-C4-alkoxycarbonyl, C1-C4-alkylcarbonyl, C1-C4-alkylcarbonyloxy, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkylthio, C1-C4-haloalkylthio, C1-C4-alkoxy, C1-C4-haloalkoxy;and agriculturally useful salts thereof, processes and intermediates for preparing compounds of the formula I, compositions comprising them, and the use of the compounds of the formula I and compositions comprising them for controlling harmful plants are described.

    9.
    发明专利
    未知

    公开(公告)号：DE59813869D1

    公开(公告)日：2007-02-15

    申请号：DE59813869

    申请日：1998-01-08

    Applicant: BASF AG

    Inventor： VON DEYN WOLFGANG ,  HILL LUISE ,  BAUMANN ERNST ,  ENGEL STEFAN ,  MAYER GUIDO ,  RHEINHEIMER JOACHIM ,  WITSCHEL MATTHIAS ,  MISSLITZ ULF ,  WAGNER OLIVER ,  OTTEN MARTINA ,  WALTER HELMUT ,  WESTPHALEN KARL-OTTO

    IPC: C07D277/10 ,  C07D413/10 ,  A01N43/18 ,  A01N43/48 ,  A01N43/56 ,  A01N43/72 ,  A01N43/76 ,  A01N43/78 ,  A01N43/80 ,  C07D231/20 ,  C07D231/24 ,  C07D261/04 ,  C07D261/20 ,  C07D263/10 ,  C07D273/00 ,  C07D277/20 ,  C07D277/34 ,  C07D291/04 ,  C07D401/10 ,  C07D403/10 ,  C07D405/10 ,  C07D409/10 ,  C07D411/10 ,  C07D417/10 ,  C07D419/10 ,  C07D498/10

    Abstract: 4-(3-Heterocyclyl-benzoyl)-pyrazole derivatives (I) and their salts are new: R1, R3 = H; NO2; halo; CN; 1-6C alkyl, 1-6C alkoxy, 1-6C alkylthio, 1-6C alkylsulphinyl or 1-6C alkylsulphonyl optionally substituted by halo; H2NSO2; (1-6C alkyl)NHSO2; (1-6C alkyl)2NSO2; (1-6C alkyl)SO2NH-; (1-6C haloalkyl-SO2)NH-; (1-6C alkyl)(1-6C alkyl-SO2)N-; or (1-6C haloalkyl)(1-6C alkyl-SO2)N-; R2 = optionally substituted 5- or 6-membered heterocycle containing 1-4 O, S and/or N atoms; R6 = 1-6C alkyl; R7 = 1-6C alkyl; 3-6C alkenyl or 3-6C alkynyl optionally substituted by halo; 3-6C cycloalkyl; 1-6C alkylcarbonyl; 2-6C alkenylcarbonyl; 2-6C alkynylcarbonyl; 3-6C cycloalkylcarbonyl; 1-6C alkoxycarbonyl; 3-6C alkenyloxycarbonyl; 3-6C alkynyloxycarbonyl; 1-6C alkyl-NH-CO-; 3-6C alkenyl-NH-CO-; 3-6C alkynyl-NH-CO-; (1-6C alkyl)2N-CO-; (3-6C alkenyl)(1-6C alkyl)N-CO-carbonyl; (3-6C alkynyl)(1-6C alkyl)N-CO-; (1-6C alkoxy)(1-6C alkyl)N-CO-; (3-6C alkenyl)(1-6C alkoxy)N-CO-; (3-6C alkynyl)(1-6C alkoxy)N-CO-; (1-6C alkyl)2N-CS-; 1-6C alkoxyimino-1-6C alkyl; 1-6C alkylamino imino-1-6C alkyl; or di(1-6C alkylamino)imino-1-6C alkyl (alkyl, cycloalkyl and alkoxy groups are optionally substituted by 1 or more halo and/or by 1-3 CN, OH, 1-4C alkoxy, 1-4C alkylthio, di(1-4C alkyl)amino, 1-4C alkylcarbonyl, 1-4C alkoxycarbonyl, 1-4C alkoxy-1-4C alkoxycarbonyl, (1-4C alkyl)2N-1-4C alkoxycarbonyl, COOH, 1-4C alkyl-NH-CO-, (1-4C alkyl)2N-CO-, CONH2; 1-4C alkylcarbonyloxy or 3-6C cycloalkyl); or Ar; Ar-1-6C alkyl; Ar-CO-1-6C alkyl; Ar-CO-; Ar-O-CO-; Ar-NH-CO-; (1-6C alkyl)(Ar)N-CO-; or Ar-2-6C alkenylcarbonyl; Ar = phenyl or heterocyclyl optionally substituted by 1 or more halo and/or by 1-3 NO2, CN or 1-4C alkyl or 1-4C alkoxy (optionally substituted by halo), and R8 = H, 1-6C alkyl or 1-6C haloalkyl.

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