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    METHOD FOR PRODUCING AMINOALKOXY BENZYLAMINES AND AMINOALKOXY BENZONITRILES AS INTERMEDIATES
    1.
    发明申请
    METHOD FOR PRODUCING AMINOALKOXY BENZYLAMINES AND AMINOALKOXY BENZONITRILES AS INTERMEDIATES 审中-公开
    工艺用于生产和AMINOALKOXYBENZYLAMINEN AMINOALKOXYBENZONITRILEN中间产品

    公开(公告)号：WO2004013082A3

    公开(公告)日：2004-07-15

    申请号：PCT/EP0307871

    申请日：2003-07-18

    Applicant: BASF AG ,  LOEBER OLIVER ,  BENISCH CHRISTOPH ,  EBEL KLAUS ,  MELDER JOHANN-PETER

    Inventor： LOEBER OLIVER ,  BENISCH CHRISTOPH ,  EBEL KLAUS ,  MELDER JOHANN-PETER

    IPC: C07B61/00 ,  C07C213/02 ,  C07C217/58 ,  C07C253/30 ,  C07C255/54

    CPC classification number: C07C213/02 ,  C07C253/30 ,  C07C217/58 ,  C07C255/54

    Abstract: The invention relates to methods for producing 4-[aminoalkoxy]benzylamines of general formula (I) by means of catalytic hydrogenation of 4-[aminoalkoxy]benzonitriles of general formula (II). In the compounds of general formulae (I) and (II), R represents C1-C8 alkylene, and R and R independently represent C1-C8 alkyl or are linked to form a ring which can also contain a heteroatom. The hydrogenation is carried out at increased pressure and increased temperatures. The invention also relates to a method for producing the intermediate (II).

    Abstract translation: 本发明涉及一种方法，通过4- [氨基烷氧基] -benzonitrilen通式（II），其中所述通式的化合物中的I和II [R <1的催化氢化制备通式（I）的4- [氨基烷氧基]苄 >代表C1-C8亚烷基，R <2>和R <3>独立地是C1-C8烷基或连接形成一个环，该环还可以含有杂原子，其中所述氢化在升高的压力和升高的温度下进行 执行。 此外，本发明涉及一种用于中间体（II）的制备方法。

    Production of dialdehydes and/or ethylenically unsaturated monoaldehydes, useful as intermediates, comprises hydroformylation of a compound having two ethylenically unsaturated double bonds using a Group VIII metal-pnicogen chelate catalyst
    2.
    发明专利
    Production of dialdehydes and/or ethylenically unsaturated monoaldehydes, useful as intermediates, comprises hydroformylation of a compound having two ethylenically unsaturated double bonds using a Group VIII metal-pnicogen chelate catalyst 未知

    公开(公告)号：DE10242636A1

    公开(公告)日：2004-03-18

    申请号：DE10242636

    申请日：2002-09-13

    Applicant: BASF AG

    Inventor： VOLLAND MARTIN ,  AHLERS WOLFGANG ,  EBEL KLAUS ,  PACIELLO ROCCO ,  ROEPER MICHAEL ,  MACKEWITZ THOMAS ,  BOEHM VOLKER ,  SAVA XAVIER ,  LOEBER OLIVER ,  BEY OLIVER ,  STEPHAN JUERGEN ,  HAESE FRANK

    IPC: C07B61/00 ,  C07C45/50 ,  C07C47/12 ,  C07F9/572 ,  C07F9/655 ,  C07F9/6558 ,  C07F9/6584 ,  C07F9/6596 ,  C07C47/21

    Abstract: A process for the production of dialdehydes and/or ethylenically unsaturated monoaldehydes by reaction of at least one compound having at least two ethylenically unsaturated double bonds with carbon monoxide and hydrogen in the presence of a hydroformylation catalyst comprising at least one complex of a Group VIII metal with at least one ligand comprising a pnicogen chelate compound. A process for the production of dialdehydes and/or ethylenically unsaturated monoaldehydes by reaction of at least one compound having at least two ethylenically unsaturated double bonds with carbon monoxide and hydrogen in the presence of a hydroformylation catalyst comprising at least one complex of a Group VIII metal with at least one ligand comprising a pnicogen chelate compound of formula (1). Q = bridging group of formula (2); A1, A2 = O, S, SiRaRb, NRc or CRdRe; Ra-Rc = H, alkyl, cycloalkyl, heterocycloalkyl, aryl or heteroaryl; Rd, Re = H, alkyl, cycloalkyl, heterocycloalkyl, aryl or heteroaryl or two Rd groups and/or two Re groups form an intermolecular bridging group D; D = bivalent bridging group of formula (3)-(6); R9,R10 = H, alkyl, cycloalkyl, aryl, halo, trifluoromethyl, carboxyl, carboxylate or cyano or together form a 3-4C alkylene bridge; R11-R14 = H, alkyl, cycloalkyl, aryl, halo, trifluoromethyl, COOH, carboxylate, cyano, alkoxy, SO3H, sulfonate, NE1E2, alkylene-NE1E2E3+X-, acyl or nitro; C = 0 or 1; Y = chemical bond; RI-RVI = H, alky, cycloalkyl, heterocycloalkyl, aryl or heteroaryl; COORf, COO-M+, SO3Rf, SO3-M+, NE1E2, NE1E2E3+X-, alkylene-NE1E2E3+X-, ORf, SRf, (CHRgCH2O)xRf, (CH2N(E1))xRf, (CH2CH2N(E1))xRf, halo, trifluoromethyl, nitro, acyl or cyano or 2 neighboring groups, together with two neighboring C atoms of the benzene ring to which they are bonded form a condensed ring system of 1-3 further rings; Rf, E1-E3 = H, alkyl, cycloalkyl or aryl; R9 = H, methyl or ethyl; M+ = cation, X-=anion; x = 1-120; a, b = 0 or 1; Pn = P, As or Sb; R1-R4 = heteroaryl, heteroaryloxy, alkyl, alkoxy, aryl, aryloxy, cycloalkyl, cycloalkoxy, heterocycloalkyl, heterocycloalkoxy or NE1E2 with the proviso that is R1 and R3 are bonded via the N atom to the pnicogen atom bonded pyrrole ring or R1 with R2 and/or R3 together with R4 form a divalent group E of formula Py-I-W or R1 and R2 and/or R3 and R4 form a bispyrrole group of formula Py-I-Py; Py = pyrrole group that is bonded via its N atom to Pn; I = chemical bond, O, S, SiRaRb, NRc, optionally substituted 1-10C alkylene or CRhCRi; W = cycloalkyl, cycloalkoxy, aryl, aryloxy, heteroaryl or heteroaryloxy; Rh and Ri = H, alkyl, cycloalkyl, heterocycloalkyl, aryl or heteroaryl

    4.
    发明专利
    未知

    公开(公告)号：DE10235312A1

    公开(公告)日：2004-02-12

    申请号：DE10235312

    申请日：2002-08-01

    Applicant: BASF AG

    Inventor： LOEBER OLIVER ,  BENISCH CHRISTOPH ,  EBEL KLAUS ,  MELDER JOHANN-PETER

    IPC: C07B61/00 ,  C07C213/02 ,  C07C217/58 ,  C07C253/30 ,  C07C255/54

    Abstract: The invention relates to a process for preparing 4-[aminoalkoxy]benzylamines of the general formula (I) by catalytically hydrogenating 4-[aminoalkoxy]benzonitriles of the general formula (II) where, in the compounds of the general formulae I and II, R 1 is C 1 -C 8 -alkylene, R 2 and R 3 are each independently C 1 -C 8 -alkyl or are joined to give a ring which may additionally contain a heteroatom, which comprises carrying out the hydrogenation at elevated pressure and elevated temperatures. The invention further relates to a process for preparing the intermediate (II).

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