公开(公告)号：JP2004323526A

公开(公告)日：2004-11-18

申请号：JP2004132445

申请日：2004-04-28

Applicant: Basf Ag ,  ビーエーエスエフ アクチェンゲゼルシャフト

Inventor： LANG ORTMUND ,  RUMPF BERND ,  FRAUENKRON MATTHIAS ,  BOSCH MARCO ,  BERRSCHE HELMUT ,  MEIER ANTON

IPC: B01D3/14 ,  B01D3/32 ,  C07C209/84 ,  C07C211/10 ,  C07D487/08

CPC classification number: C07D487/08 ,  B01D3/14 ,  B01D3/141 ,  B01D3/322 ,  B01J2219/32 ,  C07C209/84 ,  C07C211/10

Abstract: PROBLEM TO BE SOLVED: To provide an improved process for purifying crude triethylenediamine (TEDA) with high quality and high purity in a simple and inexpensive process.
SOLUTION: The process purifies triethylenediamine (TEDA) by distillation, wherein the fractionation is carried out in a dividing wall column.
COPYRIGHT: (C)2005,JPO&NCIPI

公开(公告)号：JP2002363181A

公开(公告)日：2002-12-18

申请号：JP2002136221

申请日：2002-05-10

Applicant: BASF AG

Inventor： LANG ORTMUND ,  RUMPF BERND ,  FRAUENKRON MATTHIAS ,  FUNHOFF DIRK ,  MANDERBACH THOMAS ,  STEIN BERND

IPC: C07D487/04 ,  C07D487/08

Abstract: PROBLEM TO BE SOLVED: To provide a method for purifying triethylenediamine(TEDA) by evaporating TEDA, transferring the gas state TEDA into a liquid solvent and then continuously crystallizing from the solvent, enabling the re-circulation of at least a part of the used solvent into the purification method and also increasing the yield of the TEDA. SOLUTION: This method for purifying the TEDA is provided by extraction- treating a mother liquor obtained after the crystallization of the TEDA by using an extraction agent which is incompatible or slightly compatible with the solvent of the mother liquor and in which the TEDA is easily dissolvable, and returning the mother liquor poor in the TEDA obtained after the extraction and/or the extraction agent rich in the TEDA and used for the extraction to the purification method.

公开(公告)号：JP2002241380A

公开(公告)日：2002-08-28

申请号：JP2002000691

申请日：2002-01-07

Applicant: BASF AG

Inventor： LANG ORTMUND ,  RUMPF BERND ,  FRAUENKRON MATTHIAS ,  FUNHOFF DIRK ,  MANDERBACH THOMAS ,  STEIN BERND

IPC: C07D487/08

Abstract: PROBLEM TO BE SOLVED: To provide an efficient and economical method for production by which pure tetraethylenediamine(TEDA) and its solution are improved in order to obtain the TEDA and TEDA solution of improved quality in relation to color, color stability, odor and purity. SOLUTION: This method for producing the solution of the triethylenediamine(TEDA) comprises evaporating the TEDA from a mixture containing a solvent or a diluent wherein the solvent or diluent has 170-250 deg.C boiling point under atmospheric pressure (=1.01325 bars) and passing the TEDA in the form of vapor through a liquid solvent.

公开(公告)号：WO2005056507A3

公开(公告)日：2006-12-21

申请号：PCT/EP2004014119

申请日：2004-12-10

Applicant: BASF AG ,  RUMPF BERND ,  DECKERT PETRA ,  MUELLER THOMAS ,  GRIMMER JOHANNES

Inventor： RUMPF BERND ,  DECKERT PETRA ,  MUELLER THOMAS ,  GRIMMER JOHANNES

IPC: C07C403/08 ,  C07C45/00 ,  C07C45/59 ,  C07C49/743

CPC classification number: C07C403/08 ,  C07C2601/16 ,  Y02P20/55

Abstract: The invention relates to a method for producing cyclohexenone derivatives of general formula (I), wherein R 1 represents hydrogen or OH; R 2 represents (Ia), comprising the following steps: (a) hydrolyzing a cyclohexenol compound of formula (II), wherein R 3 represents hydrogen and R 4 represents C 1 -C 6 -alkoxy or R 3 and R 4 represent vicinal hydroxy groups, which carry a common acetal protective group or a ketone protective group, R 5 represents (IIa), and R 6 represents a protected hydroxy group, in the absence of an organic solvent and in the presence of an acid catalyst; and; (b) extracting the reaction mixture by using a polar extracting agent.

Abstract translation: 本发明涉及一种用于（I），其中R ^{1 是氢或OH通式环己烯酮衍生物的制备; [R 2 表示（Ia）中，其包括以下步骤：（a）式的Cyclohexenolverbindung水解（II）其中R 3 是氢并且R 4 < 6 为C _{1 -C >烷氧基，或R 3 和R 4 连位羟基的 都携带一个共同的缩醛或缩酮保护基团，R 5 是（IIa）中，R 6 是被保护的羟基，在酸中不存在有机溶剂的存在 催化剂; 和（b）用与极性萃取反应混合物。}}

公开(公告)号：WO0040774A3

公开(公告)日：2002-09-26

申请号：PCT/EP9910371

申请日：1999-12-24

Applicant: BASF AG ,  HUEFFER STEPHAN ,  KREBS THILO ,  LOTH WOLFGANG ,  RUMPF BERND ,  STURM JUERGEN ,  DIEBOLD BERND ,  KORKHAUS JUERGEN ,  NILGES JOACHIM ,  FRANKE AXEL

Inventor： HUEFFER STEPHAN ,  KREBS THILO ,  LOTH WOLFGANG ,  RUMPF BERND ,  STURM JUERGEN ,  DIEBOLD BERND ,  KORKHAUS JUERGEN ,  NILGES JOACHIM ,  FRANKE AXEL

IPC: C08F2/01 ,  C08F10/00 ,  C23C18/16 ,  C23C18/31 ,  C23C18/34 ,  C23C18/36 ,  C23C18/40 ,  C23C18/48 ,  C23C18/50 ,  C23C18/52 ,  F28F19/02 ,  F28F19/06 ,  B01J19/02

CPC classification number: F28F19/02 ,  C23C18/1616 ,  C23C18/1662 ,  C23C18/36 ,  Y10T428/12556 ,  Y10T428/12944 ,  Y10T428/31678

Abstract: The invention relates to a method for surface coating of apparatuses or parts of apparatuses used in chemical manufacturing. Walls of apparatuses, walls of containers and walls of reactors, dischargers, fixtures, pumps, filters, compressors, centrifuges, columns, dryers, comminuting machines, internal fittings and combinations are examples for said apparatuses or parts of apparatuses. The inventive method is characterised in that a metal layer or a metal polymer dispersion layer is currentlessly deposited on the apparatus/es or parts of apparatuses to be coated by contacting the parts to a metal electrolytic solution which contains a reduction means and optionally the dispersed polymer or polymer mixture in addition to the metal electrolyte, whereby at least one polymer is halogenated.

Abstract translation: 一种用于表面涂覆的设备和设备部件用于化工厂过程 - 包括，例如，装置，罐和反应器壁，放电装置，阀门，泵，过滤器，压缩机，离心分离机，列，干衣机，粉碎机，内部构件，填料元件和混合元件被理解为是指 - 在 其特征在于，金属层或在金属 - 聚合物分散体层或常分离要涂覆的装置或装置的部件，通过将这些部件与含有除金属电解质的还原剂的金属电解质溶液接触，和任选地，所沉积的聚合物或 含有分散的形式，其中至少一种聚合物是卤化的聚合物混合物中。

公开(公告)号：ES2263821T3

公开(公告)日：2006-12-16

申请号：ES02777064

申请日：2002-09-11

Applicant: BASF AG

Inventor： LANG ORTMUND ,  RUMPF BERND ,  FRAUENKRON MATTHIAS ,  MANDERBACH THOMAS ,  STEIN BERND

IPC: C07D487/08 ,  C07D241/00

Abstract: Procedimiento para la obtención de trietilendiamina, que presenta un grado de pureza > el 90 %, caracterizado porque se libera la trietilendiamina en bruto de los productos de elevado punto de ebullición y, a continuación, se evapora la trietilendiamina a partir de la mezcla, obtenida de este modo, y se hace pasar a través de un disolvente líquido.

公开(公告)号：DE10358003A1

公开(公告)日：2005-07-14

申请号：DE10358003

申请日：2003-12-11

Applicant: BASF AG

Inventor： RUMPF BERND ,  DECKERT PETRA ,  MUELLER THOMAS ,  GRIMMER JOHANNES

IPC: C07C45/00 ,  C07C45/59 ,  C07C49/743 ,  C07C403/08

公开(公告)号：DE50201592D1

公开(公告)日：2004-12-23

申请号：DE50201592

申请日：2002-07-02

Applicant: BASF AG

Inventor： WOSTBROCK KARL-HEINZ ,  THIEL JOACHIM ,  KRUEGER HEINZ ,  STROEFER ECKHARD ,  WEBER MARKUS ,  GERBER BERND ,  RUMPF BERND ,  SACHWEH BERND ,  KERTH STEFFEN

IPC: B01D3/14 ,  B01D3/16 ,  B01J19/30 ,  B01J19/32 ,  C01B21/14

Abstract: The invention relates to a method for producing a highly pure, aqueous hydroxylamine solution by distilling an aqueous solution, devoid of salt, of a hydroxyl ammonium salt in a plate column comprising at least two mechanical plates. Said method is characterised in that packing bodies are arranged between at least two plates of the plate column over the cross-section of said column.

公开(公告)号：AT237006T

公开(公告)日：2003-04-15

申请号：AT99967007

申请日：1999-12-24

Applicant: BASF AG

Inventor： HUEFFER STEPHAN ,  KREBS THILO ,  LOTH WOLFGANG ,  RUMPF BERND ,  STURM JUERGEN ,  DIEBOLD BERND ,  KORKHAUS JUERGEN ,  NILGES JOACHIM ,  FRANKE AXEL

IPC: C08F2/01 ,  C08F10/00 ,  C23C18/16 ,  C23C18/31 ,  C23C18/34 ,  C23C18/36 ,  C23C18/40 ,  C23C18/48 ,  C23C18/50 ,  C23C18/52 ,  F28F19/02 ,  F28F19/06

Abstract: The present invention relates to a process for coating apparatuses and apparatus parts for chemical plant construction-which are taken to mean, for example, apparatus, tank and reactor walls, discharge devices, valves, pumps, filters, compressors, centrifuges, columns, dryers, comminution machines, internals, packing elements and mixing elements-wherein a metal layer or a metal/polymer dispersion layer is deposited in an electroless manner on the apparatus(es) or apparatus part(s) to be coated by bringing the parts into contact with a metal electrolyte solution which, in addition to the metal electrolyte, comprises a reducing agent and optionally the polymer or polymer mixture to be deposited in dispersed form, where at least one polymer is halogenated.

公开(公告)号：DE10131788A1

公开(公告)日：2003-01-16

申请号：DE10131788

申请日：2001-07-04

Applicant: BASF AG

Inventor： WOSTBROCK KARL-HEINZ ,  THIEL JOACHIM ,  GERBER BERND ,  KRUEGER HEINZ ,  STROEFER ECKHARD ,  KERTH STEFFEN ,  SACHWEH BERND ,  RUMPF BERND ,  WEBER MARKUS

IPC: B01D3/14 ,  B01D3/16 ,  B01J19/30 ,  B01J19/32 ,  C01B21/14 ,  B01D3/00

Abstract: The invention relates to a method for producing a highly pure, aqueous hydroxylamine solution by distilling an aqueous solution, devoid of salt, of a hydroxyl ammonium salt in a plate column comprising at least two mechanical plates. Said method is characterised in that packing bodies are arranged between at least two plates of the plate column over the cross-section of said column.