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    ACRYLATE POLYMERS BASED ON TERT-BUTYL ACRYLATE AND/OR TERT-BUTYL METHACRYLATE
    14.
    发明专利
    ACRYLATE POLYMERS BASED ON TERT-BUTYL ACRYLATE AND/OR TERT-BUTYL METHACRYLATE 未知

    公开(公告)号：CA2428309C

    公开(公告)日：2010-01-12

    申请号：CA2428309

    申请日：2001-11-09

    Applicant: BASF AG

    Inventor： ZEITZ KATRIN ,  DAUSCH WILMA M ,  SCHNEIDER TANJA ,  ANGEL MAXIMILIAN ,  WOOD CLAUDIA ,  DE POTZOLLI BERND

    IPC: A61K8/72 ,  C08F220/18 ,  A61K8/00 ,  A61K8/81 ,  A61Q1/00 ,  A61Q1/04 ,  A61Q1/10 ,  A61Q1/12 ,  A61Q5/00 ,  A61Q5/02 ,  A61Q5/04 ,  A61Q5/06 ,  A61Q5/10 ,  A61Q9/04 ,  C08F2/44 ,  C08F220/06

    Abstract: The invention relates to acrylate polymers comprising a K-value ranging from 10 to 60, which can be obtained by the radical polymerization of: 30 to 99 w t. % of tert-butyl acrylate and/or tert-butyl methacrylate designated as monome r A; 1 to 28 wt. % of acrylic acid and/or methacrylic acid designated as monom er B, and; 0 to 60 wt. % of a radically copolymerizable monomer or of a radical ly copolymerizable monomer mixture designated as monomer C, whereby at least on e of monomers C yields a homopolymer with a glass-transition temperature lower than 30 ~C, with the provision that the wt. %'s total 100. The radical polymerization is carried out in the presence of alkane thiols with a C chai n length of C 14 to C 22. The invention also relates to acrylate polymers comprising a K-value ranging from 10 to 60, which can be obtained by the radical polymerization of: 30 to 99 wt. % of tert-butyl acrylate and/or tert - butyl methacrylate designated as monomer A; 1 to 28 wt. % of acrylic acid and/or methacrylic acid designated as monomer B, and; 0 to 60 wt. % of a radically copolymerizable monomer or of a radically copolymerizable monomer mixture designated as monomer C, whereby at least one of monomers C yields a homopolymer with a glass-transition temperature lower than 30 ~C, with the provision that the wt. %'s total 100. The radical polymerization is carried out in the presence of alkane thiols with a C chain length of C 10 to C 22 followed by a hydrogen peroxide treatment. The invention also relates to the use of these acrylate polymers as film formers as well as to their use in cosmetic preparations.

    16.
    发明专利
    未知

    公开(公告)号：DE10343900A1

    公开(公告)日：2005-04-21

    申请号：DE10343900

    申请日：2003-09-19

    Applicant: BASF AG

    Inventor： MATHAUER KLEMENS ,  SCHNEIDER TANJA ,  WIDMAIER RALF ,  KAMM ANDRE ,  BELL CARL-MARTIN

    IPC: B01D71/38 ,  B01D71/44 ,  C08F222/02 ,  C08F226/02 ,  C08F226/06 ,  C08F226/10 ,  C08F226/00 ,  C08J5/22

    Abstract: The use of copolymers containing a) from 60% to 99% by weight of at least one vinyllactam or N-vinylamine selected from the group consisting of N-vinylpyrrolidone, N-vinylpiperidone, N-vinylcaprolactam or N-vinylformamide, and b) from 1% to 40% by weight of at least one monomer of the general formula where b1) R 1 , R 2 , R 3 each denote oxygen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl and R 4 denotes the general formula II X denotes oxygen, NH, NR (where R=R1) R 5 denotes C 1 -C 6 -alkyl, phenyl, A denotes OH, NH 2 , NR 2 (wheret R 2 =R1) R 6 , R 7 R 8 each denote hydrogen, C 1 -C 4 -alkyl n denotes an integer between 1 and 4 B, F each denote C, N D denotes C 1 -C 4 -alkyl, O, NH p denotes an integer between 0 and 15 E denotes N, O l, m each denote 0 or 1 R 9 , R 10 , R 11 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -C 10 -aryl, C 7 -C 10 -alkylaryl and s, q each denote an integer between 0 and 2. For E=nitrogen the s+q sum is equal to 1 or 2. For E=oxygen the s+q sum is equal to zero. For E=nitrogen and s+q=2 the counterions needed for charge neutrality are selected from elements of groups 1, 2 or 13 with the proviso that there is one element of group 1 per R4 radical when a group 1 element is selected, one element of group 2 per two R4 radicals when a group 2 element is selected and one element of group 13 per three R4 radicals when a group 13 element is selected. b2) R 1 , R 2 , R 3 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl or a radical of the general formula III R 4 denotes a radical of the general formula III R 6 , R 7 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl X denotes O, NH, NR (where R=R6) R5 denotes C 1 -C 10 -alkyl, C 6 -C 10 -aryl, C 7 -C 14 -alkylaryl n denotes an integer between 0 and 15 Y denotes O, N R6, R7 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl p, q each denote an integer between 0 and 2 with the proviso that at least one of R 1 , R 2 , R 3 and R 4 but not more than two denote the general formula III. b3) R 1 , R 2 , R 3 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl R 4 denotes a radical of the general formula IV R 5 denotes C 1 -C 8 -alkyl n denotes an integer between 0 and 4 m, l each denote 0 or 1 R 6 denotes C 1 -C 4 -alkyl R 7 denotes hydrogen, C 1 -C 4 -alkyl and X N(R1)(R2) or halogen. b4) R 1 , R 2 , R 3 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl R 4 denotes a radical of the general formula V X, Y each denote O, N, S R 5 , R 6 each denote C 1 -C 4 -alkyl, C 1 -C 4 -alkenyl l, m each denote an integer between 0 and 4 n denotes an integer between 0 and 2 R 7 denotes hydrogen, C 1 -C 4 -alkyl Z denotes sulfate, hydrogensulfate, chloride, bromide, iodide, phosphate, hydrogenphosphate, dihydrogenphosphate p denotes 0, 1/3, ½, 1 and q denotes an integer between 0 and 3. b5) R 1 , R 2 , R 3 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl, or a radical of the general formula VI R 4 denotes a radical of the general formula VI R 5 , R 7 , R 8 , R 11 each denote C 1 -C 6 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl R 6 , R 12 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl R 9 , R 10 each denote hydrogen, C 1 -C 4 -alkyl, C 6 -aryl, C 7 -C 10 -alkylaryl X denotes O E, F, Y, D each denote O, N, S M denotes an element of group 1, 2 or 13 of the periodic table a, k, l, s each denote 0 or 1 m, n, r, w each denote an integer between 0 and 10 o denotes an integer between 0 and 3 p denotes an integer between 0 and 20 q, t, u, v, z each denote an integer between 0 and 2 x denotes 0, 1/3, ½, 1 and y an integer between 1 and 3 with the proviso that at least one of R 1 , R 2 , R 3 and R 4 but not more than 2 denote the general formula VI, in conjunction with c) optionally one or more hydrophilic polymers C or mixtures thereof d) and optionally also further polymers D and mixtures thereof for producing membranes.

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