191.
    发明专利
    未知

    公开(公告)号:AT382614T

    公开(公告)日:2008-01-15

    申请号:AT01951476

    申请日:2001-05-03

    Applicant: BASF AG

    Abstract: In a process for the continuous fractional distillation of mixtures comprising tetrahydrofuran, gamma-butyrolactone and/or 1,4-butanediol to give at least three fractions, the fractionation is carried out in an assembly of distillation columns comprising at least one dividing wall column or at least one assembly of thermally coupled conventional distillation columns.

    193.
    发明专利
    未知

    公开(公告)号:AT362905T

    公开(公告)日:2007-06-15

    申请号:AT02712897

    申请日:2002-02-06

    Applicant: BASF AG

    Abstract: A process for recovering crude 1,3-butadiene from a C 4 fraction by extractive distillation using a selective solvent in a dividing wall column (TK) in which a dividing wall (T) is arranged in the longitudinal direction of the column to form a first subregion (A), a second subregion (B) and a lower common column region (C) and which is preceded by an extractive scrubbing column (K) is proposed.

    198.
    发明专利
    未知

    公开(公告)号:DE50110518D1

    公开(公告)日:2006-09-07

    申请号:DE50110518

    申请日:2001-05-03

    Applicant: BASF AG

    Abstract: Separating wall column comprises an upper column region (6), a feed part (7), a removal part (8) and a lower column region (9) as segments. The feed part and the removal part are separated from each other by a separating wall (10) fixed in the column. The separating wall is partially formed from an elastic material and has a low over-dimension with respect to its width. The wall is fixed in the column so that it exerts an elastic force on the inner casing of the column. Preferred Features: The separating wall is completely formed from an elastic material and is present as a one piece strip. The wall is made from PTFE or a corrosion resistant chromium-nickel high grade steel. The side edges of the wall have an angle of 20-60 degrees . The wall has a thickness of 0.05-1, preferably 0.1-0.3 mm.

    199.
    发明专利
    未知

    公开(公告)号:AT334957T

    公开(公告)日:2006-08-15

    申请号:AT02792927

    申请日:2002-12-06

    Applicant: BASF AG

    Abstract: Trimethylolpropane is isolated from a reaction mixture which has been obtained by reaction of n-butyraldehyde with formaldehyde in the presence of a base and, if appropriate, hydrogenation of the resulting mixture by distilling the mixture by means of a dividing wall column or a distillation column with a precolumn or a distillation column with an after-column. The process has low capital costs and a low energy consumption and gives reduced formation of high-boiling by-products.

    200.
    发明专利
    未知

    公开(公告)号:DE50301577D1

    公开(公告)日:2005-12-08

    申请号:DE50301577

    申请日:2003-07-07

    Applicant: BASF AG

    Abstract: The invention relates to a method for the separation of ascorbic acid from a mixture containing ascorbic acid and 2-keto-L-gulonic acid in a polar, preferably aqueous solvent, by means of liquid/liquid extraction using an amide. The method preferably also comprises steps for the back-extraction of the ascorbic acid, recycling of the extraction solvent and/or the back extraction solvent and for isolation of the ascorbic acid from the back extraction solvent. The invention further relates to a method for the production of ascorbic acid from KGA and isolation of the ascorbic acid so produced.

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