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    Procedimiento para la producción de cetonas cíclicas
    21.
    发明专利
    Procedimiento para la producción de cetonas cíclicas 未知

    公开(公告)号：ES2602117T3

    公开(公告)日：2017-02-17

    申请号：ES09782183

    申请日：2009-08-26

    Applicant: BASF SE

    Inventor： TELES JOAQUIM ,  RUPPEL WILHELM ,  WEGERLE ULRIKE ,  MEIER ANTON ,  GENGER THOMAS ,  SCHELPER MICHAEL ,  RESCH PETER

    IPC: C07C49/11

    Abstract: Procedimiento continuo para la producción de al menos una cetona monocíclica con 4 a 20 átomos de carbono mediante reacción a una temperatura de 170 a 340 °C de una mezcla G1 que contiene al menos una olefina monocíclica con 4 a 20 átomos de carbono con una mezcla G2 que contiene al menos monóxido de dinitrógeno, caracterizado porque esta reacción se lleva a cabo de manera adiabática y la mezcla G1 y/o G2 antes de la reacción para dar al menos una cetona monocíclica con 4 a 20 átomos de carbono se precalientan hasta una temperatura de 170 a 270 °C, extrayéndose la energía térmica necesaria para precalentar la mezcla G1 y/o G2 al menos en parte de la corriente de producto del procedimiento.

    METHOD FOR PRODUCING FORMIC ACID BY REACTING CARBON DIOXIDE WITH HYDROGEN
    23.
    发明专利
    METHOD FOR PRODUCING FORMIC ACID BY REACTING CARBON DIOXIDE WITH HYDROGEN 未知

    公开(公告)号：IN3122DEN2014A

    公开(公告)日：2015-05-22

    申请号：IN3122DEN2014

    申请日：2014-04-21

    Applicant: BASF SE

    Inventor： SCHAUB THOMAS ,  BEY OLIVER ,  MEIER ANTON ,  FRIES DONATA MARIA ,  HUGO RANDOLF

    IPC: C07C51/00 ,  C07C51/02 ,  C07C51/42

    Abstract: The invention relates to a method for producing formic acid comprising the following steps: (a) reacting in a homogeneously catalyzed manner a reaction mixture (Rg) containing carbon dioxide hydrogen at least one polar solvent and at least one tertiary amine in the presence of at least one coordination catalyst in a hydrogenation reactor in order to obtain a two phase hydrogenation mixture (H) containing an upper phase (O1) which contains the at least one coordination catalyst and the at least one tertiary amine (A1) and a lower phase (U1) which contains the at least one polar solvent residues of the at least one coordination catalyst and at least one formic acid/amine adduct; (b) processing the hydrogenation mixture (H) obtained in step (a) according to one of the following steps: (b1) phase separating the hydrogenation mixture (H) obtained in step (a) in a first phase separating device into the upper phase (O1) and the lower phase (U1) or (b2) extracting the at least one coordination catalyst from the hydrogenation mixture (H) obtained in step (a) in an extraction unit with an extracting agent containing the at least one tertiary amine (A1) in order to obtain a raffinate (R1) containing the at least one formic acid/amine adduct (A2) and the at least one polar solvent and an extract (E1) containing the at least one tertiary amine (A1) and the at least one coordination catalyst or (b3) phase separating the hydrogenation mixture (H) obtained in step (a) in a first phase separating device into the upper phase (O1) and the lower phase (U1) and extracting the residues of the at least one coordination catalyst from the lower phase (U1) in an extraction unit by means of an extracting agent containing the at least one tertiary amine (A1) in order to obtain a raffinate (R2) containing the at least one formic acid/amine adduct (A2) and the at least one polar solvent and an extract (E2) containing the at least one tertiary amine (A1) and the residues of the at least one coordination catalyst; (c) separating the at least one polar solvent from the lower phase (U1) from the raffinate (R1) or from the raffinate (R2) in a first distillation device in order to obtain a distillate (D1) containing the at least one polar solvent which is fed back into the hydrogenation reactor in step (a) and a two phase bottom mixture (S1) containing an upper phase (O2) which contains the at least one tertiary amine (A1) and a lower phase (U2) which contains the at least one formic acid/amine adduct (A2); (e) cleaving the at least one formic acid/amine adduct (A2) contained in the bottom mixture (S1) or optionally in the lower phase (U2) in a thermal cleaving unit in order to obtain the at least one tertiary amine (A1) which is fed back to the hydrogenation reactor in step (a) and formic acid which is discharged from the thermal cleaving unit wherein carbon monoxide is added to the lower phase (U1) the raffinate (R1) or the raffinate (R2) directly before and/or during step (c) and/or carbon monoxide is added to the bottom mixture (S1) or optionally the bottom phase (U2) directly before and/or during step (e).

    Procedimiento para la obtención de ciclododecatrieno mediante evaporación
    26.
    发明专利
    Procedimiento para la obtención de ciclododecatrieno mediante evaporación 未知

    公开(公告)号：ES2377448T3

    公开(公告)日：2012-03-27

    申请号：ES06763996

    申请日：2006-06-30

    Applicant: BASF SE

    Inventor： RUMPF BERND ,  LANG ORTMUND ,  HAUNERT ANDREA ,  GENGER THOMAS ,  MEIER ANTON

    IPC: C07C7/04 ,  C07C13/277

    Abstract: Procedimiento para la obtención de ciclododecatrieno (CDT) a partir de una disolución que contiene CDT y compuestos de alto punto de ebullición como catalizador desactivado y polímeros, caracterizado porque se suministra la disolución a un precalentador y se calienta, a continuación se reduce su presión a través de un dispositivo de mantenimiento de la presión y se suministra la mezcla de dos fases obtenida a un evaporador de tubo en espiral y allí se reduce el contenido en CDT de la fase líquida mediante una evaporación parcial y se evacua un flujo de producto gaseoso con una concentración aumentada de CDT.

    29.
    发明专利
    未知

    公开(公告)号：DE502006001603D1

    公开(公告)日：2008-10-30

    申请号：DE502006001603

    申请日：2006-03-14

    Applicant: BASF SE

    Inventor： GERLACH TILL ,  HAESE FRANK ,  MEIER ANTON ,  MELDER JOHANN-PETER ,  RUETTER HEINZ

    IPC: C07C209/16 ,  C07C211/05

    Abstract: Processes comprising: (a) providing a first reactant comprising a bioethanol; and (b) reacting the first reactant with a second reactant comprising a component selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of hydrogen and a catalytically effective amount of a heterogeneous hydrogenation/dehydrogenation catalyst to form an ethylamine; wherein the catalyst has been activated at a temperature of 100 to 500° C. for at least 25 minutes; wherein prior to activation the catalyst comprises: (i) 20 to 65% by weight of a support material comprising one or both of zirconium dioxide (ZrO2) and aluminum oxide (Al2O3), (ii) 1 to 30% by weight of oxygen-comprising compounds of copper, calculated as CuO, and (iii) 21 to 70% by weight of oxygen-comprising compounds of nickel, calculated as NiO; and wherein after activation the catalyst has a CO uptake capacity of >110 mumol of CO/g of the catalyst.

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