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公开(公告)号：BR0016214A
公开(公告)日：2002-09-17
申请号：BR0016214
申请日：2000-11-27
Applicant: BASF AG
Inventor： STAMM ARMIN , TZ ROLAND G , TZ NORBERT G , HENKELMANN JOCHEM , KNEUPER HEINZ-JOSEF , WOLF BERND
Abstract: The invention relates to a method for producing o-choromethyl benzenecarbonyl chlorides of formula (I), wherein R -R can be the same or different and stand for hydrogen, C1-C4-alkyl, halogen or trifluoromnethyl, by converting benzocondensed lactones of formula (II), wherein R -R have the aforementioned meaning, with gaseous or liquid phosgene and the dimers or trimers thereof. The inventive method is characterized in that the conversion is carried out in the presence of catalytical amounts of a Lewis acid and catalytical amounts of a phosgenation catalyst
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公开(公告)号：DE10044165A1
公开(公告)日：2002-03-21
申请号：DE10044165
申请日：2000-09-07
Applicant: BASF AG
Inventor： HENKELMANN JOCHEM , MAAS HEIKO , STAMM ARMIN , RINK HEINZ-PETER , JUNG WERNER-ALFONS
IPC: C07C271/12 , C09D5/46 , C07C269/00 , C08G63/91
Abstract: The invention relates to polycarbamates of general formula (I), wherein R and R' are identical or similar and represent alkyl groups comprising 1-4 C atoms and n is a number with an average value of between 2 - 5.
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公开(公告)号：DE10010595A1
公开(公告)日：2001-09-06
申请号：DE10010595
申请日：2000-03-03
Applicant: BASF AG
Inventor： STAMM ARMIN , KNEUPER HEINZ-JOSEF , HENKELMANN JOCHEM , WEBER THEODOR , BUSCH RALPH
Abstract: In the production of chloroalkanoyl chlorides (I) with a (substituted) 1-10 carbon (hetero)alkylene chain by reacting a lactone (II) with hydrogen chloride (HCl) and phosgene (COCl2) in the presence of a catalyst, HCl is introduced before and/or during addition of COCl2, starting when the temperature reaches >= 60 deg C, and the catalyst is a pyridine compound. In the production of chloroalkanoyl chlorides of formula (I) with a (substituted) 1-10 carbon (hetero)alkylene chain by reacting a lactone of formula (II) with hydrogen chloride (HCl) and phosgene (COCl2) in the presence of a catalyst, HCl is introduced before and/or during addition of COCl2, starting when the temperature reaches >= 60 deg C, and the catalyst is a pyridine compound: R , R = H or R; R = halogen, nitro, CN or an organic group containing carbon (C); Y = optionally R-substituted 1-10 C alkylene, which may have a (thio)ether, tertiary amino or keto group in the chain, in which R groups on Y, R and/or R may be linked to form a non-aromatic system.
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公开(公告)号：AU5212701A
公开(公告)日：2001-08-27
申请号：AU5212701
申请日：2001-02-16
Applicant: BASF AG
Inventor： HENKELMANN JOCHEM , MAAS HEIKO , SCHULZ GERHARD , STAMM ARMIN , RINK HEINZ-PETER , JUNG WERNER-ALFONS , SCHWAB PETER
IPC: C07C263/10 , C07C265/14 , C08G18/62 , C08G18/72 , C08G18/73 , C09D175/04 , C09J175/04
Abstract: A description is given of polyisocyanates of the formula I in which R and R' are identical or different and are alkyl groups having 1-4 carbon atoms and n is on average from 1.5 to 5 and also of a process for preparing these polyisocyanates in which a polyamine of the formula II in which R, R', and n are as defined above, is reacted with phosgene. The new polyisocyanates are suitable for producing crosslinked polyurethanes from reaction mixtures with low solvent content and for producing coating compositions or adhesives. Also described are the coating compositions and adhesives, and their use.
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公开(公告)号：DE10007695A1
公开(公告)日：2001-08-23
申请号：DE10007695
申请日：2000-02-19
Applicant: BASF AG
Inventor： GOETZ ROLAND , STAMM ARMIN , GOETZ NORBERT , KEIL MICHAEL , WOLF BERND , STEINMETZ ADRIAN , HENKELMANN JOCHEN
Abstract: Production of o-chloromethylbenzoyl chlorides (I) by reacting benzo-condensed lactones (II) with thionyl chloride is carried out in the presence of catalytic amounts of (a) a catalyst (III) containing boron, selected from boric acid and anhydride, borates, boronic acid and boronic esters, and (b) a quaternary ammonium salt (IV). Production of o-chloromethylbenzoyl chlorides of formula (I) by reacting benzo-condensed lactones of formula (II) with thionyl chloride is carried out in the presence of catalytic amounts of (a) a catalyst (III) containing boron, selected from boric acid and anhydride, borates, boronic acid and boronic esters, and (b) a quaternary ammonium salt (IV). [Image] R 1-R 4H, 1-4C alkyl, halogen or CF 3.
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Patent Agency Ranking
公开(公告)号：DE19943844A1
公开(公告)日：2001-03-15
申请号：DE19943844
申请日：1999-09-13
Applicant: BASF AG
Inventor： BUSCH RALPH , KNEUPER HEINZ-JOSEF , WEBER THEODOR , MUELLER WINFRIED , STAMM ARMIN , HENKELMANN JOCHEM
IPC: C07B61/00 , C07C51/60 , C07C51/64 , C07C53/42 , C07C57/66 , C07B41/10 , B01J31/02 , C07C233/03 , C07D295/182
Abstract: The invention relates to a method for producing acid chlorides by converting carboxylic acids with carbon oxychlorides or thionyl chloride in the presence of a catalyst adduct of an N,N-disubstituted formamide of general formula (I) and carbon oxychloride or thionyl chloride. In the formula, R and R , independently from one another, mean C1- to C4-alkyl or R and R together mean a C4- or C5-alkylene chain. According to the inventive method, hydrogen chloride is added during and/or after the conversion.
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公开(公告)号：HU0003768A2
公开(公告)日：2001-02-28
申请号：HU0003768
申请日：1998-08-28
Applicant: BASF AG
Inventor： HENKELMANN JOCHEM , STAMM ARMIN , WEBER THEODOR , WEYER HANS-JUERGEN
IPC: B01J31/02 , C07B61/00 , C07C329/02
Abstract: PCT No. PCT/EP98/05525 Sec. 371 Date Feb. 17, 2000 Sec. 102(e) Date Feb. 17, 2000 PCT Filed Aug. 28, 1998 PCT Pub. No. WO99/11611 PCT Pub. Date Mar. 11, 1999A catalyst used for preparing thiochloroformates by reacting thiols with phosgene is a cyclic urea or cyclic thiourea which may be in the form of a salt obtainable by reaction with a hydrohalic acid or phosgene.
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公开(公告)号：DE19830556A1
公开(公告)日：2000-01-13
申请号：DE19830556
申请日：1998-07-08
Applicant: BASF AG
Inventor： STAMM ARMIN , HENKELMANN JOCHEM
IPC: C07D233/61 , C07D233/90 , C07D521/00
Abstract: The invention relates to a method for producing carbonyl diimidazoles of general formulas (Ia), (Ib), (Ic) or mixtures thereof, whereby R represents hydrogen or a C1-C4 alkyl radical and R represents hydrogen or a methyl radical. According to the invention, stoichiometric quantities of an organic nitrogenous base which comprises a lower pKb value than imidazole is added to the reaction mixture with regard to the imidazoles by reacting at least one imidazole of general formulas (IIa) and (IIb) in which R and R have the aforementioned meanings with phosgene in an inert solvent.
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49.发明专利
公开(公告)号：DE19810036A1
公开(公告)日：1999-09-16
申请号：DE19810036
申请日：1998-03-09
Applicant: BASF AG
Inventor： STAMM ARMIN , HENKELMANN JOCHEM , WEYER HANS-JUERGEN
Abstract: Propargyl chloride (I) is prepared continuously by reaction of propargyl alcohol (II) with a chlorination agent, in the presence of a catalyst (0.1-10 mol.% based on the amount of (II)), at 40-70 deg C. Continuous preparation of (I) comprises reaction of (II) with a chlorination agent in the presence of a catalyst. The chlorination agent, (II) and catalyst (0.1-10 mol.% based on the amount of (II) used) are added continuously into a reaction zone and reacted at 40-70 deg C.
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公开(公告)号：CZ304309B6
公开(公告)日：2014-02-26
申请号：CZ2002851
申请日：2000-08-31
Applicant: BASF AG
Inventor： BUSCH RALPH , KNEUPER HEINZ-JOSEF , WEBER THEODOR , MUELLER WINFRIED , STAMM ARMIN , HENKELMANN JOCHEM
Abstract: Způsob čištění karbonylchloridů, připravených reakcí karboxylových kyselin s fosgenem nebo s thionylchloridem v přítomnosti katalytického aduktu, přičemž při tomto způsobu čištění se na takto připravené karbonylchloridy působí hydrohalogenidem karboxamidu vzorce I, ve kterém R.sup.1.n. je vodík nebo C.sub.1.n.- až C.sub.3.n.-alkyl; R.sup.2.n. a R.sup.3.n. nezávisle jeden na druhém znamenají C.sub.1.n.- až C.sub.4.n.-alkyl, nebo R.sup.2.n. a R.sup.3 .n..sup.společně.n.tvoří C.sub.4.n.- nebo C.sub.5.n.-alkylenový řetězec, a karbonylchlorid, vyčištěný touto cestou, se izoluje oddělením od karboxamid- hydrohalogenidové fáze.
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