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公开(公告)号：WO2010139651A3
公开(公告)日：2011-03-03
申请号：PCT/EP2010057511
申请日：2010-05-31
Applicant: BASF SE , MAURER STEFFEN , HAUER BERNHARD , BONNEKESSEL MELANIE , FABER KURT , STUECKLER CLEMENS
Inventor： MAURER STEFFEN , HAUER BERNHARD , BONNEKESSEL MELANIE , FABER KURT , STUECKLER CLEMENS
CPC classification number: C12P7/24 , C12N9/001 , C12P7/22 , C12P7/26 , C12P7/40 , C12P7/42 , C12P7/46 , C12P7/62 , C12P17/10 , C12Y103/01031
Abstract: A process for the enzymatic reduction of an enoate (1) wherein the C=C bond of the enoate (1) is stereoselectively hydrogenated in the presence of an enoate-reductase and an oxidizable co-substrate (2) in a system which is free of NAD(P)H, a. formula (1); b. in which c. A is a ketone radical (-CRO), an aldehyde radical (-CHO), a carboxyl radical (-COOR), with R = H or optionally substituted C1-C6-alkyl radical, d. R1, R2 and R3 are independently of one another H, -O-C1-C6-alkyl, -O-W with W = a hydroxyl protecting group, C1-C6-alkyl, which can be substituted, C2-C6-alkenyl, carboxyl, or an optionally substituted carbo- or heterocyclic, aromatic or nonaromatic radical, or one of R1, R2 and R3 is a -OH radical, or R1 is linked to R3 so as to become part of a 4-8-membered cycle, or R1 is linked to R so as to become part of a 4-8-membered cycle, with the proviso that R1, R2 and R3 may not be identical.
Abstract translation: 在酸酐（1）的酶还原方法中，其中在酸酐还原酶和可氧化共底物（2）的存在下，在无自由基的体系中立体选择性地氢化了enoate（1）的C = C键 的NAD（P）H，a。 公式1）; 湾 其中c。 A是酮基（-CRO），醛基（-CHO），羧基（-COOR），其中R = H或任选取代的C 1 -C 6 - 烷基，d。 R 1，R 2和R 3彼此独立地为H，-O-C 1 -C 6烷基， - W，其中W =羟基保护基，可被取代的C 1 -C 6 - 烷基，C 2 -C 6 - 烯基，羧基， 或任选取代的碳 - 或杂环芳族或非芳族基团，或R 1，R 2和R 3中的一个为-OH基团，或R 1与R 3连接以成为4-8元环的一部分，或R 1 与R连接成为4-8元环的一部分，条件是R1，R2和R3可能不相同。
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公开(公告)号：CA2898963A1
公开(公告)日：2014-10-02
申请号：CA2898963
申请日：2014-03-03
Applicant: BASF SE
Inventor： ERNST BURKHARD , EHRESMANN MANFRED , KORADIN CHRISTOPHER , PLETSCH ANDREAS , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , SIEGEL WOLFGANG , SCHRODER HARTWIG , FREYER STEPHAN , ODMAN PETER
IPC: C12P17/18
Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.
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公开(公告)号：CA2898115C
公开(公告)日：2021-03-02
申请号：CA2898115
申请日：2014-01-15
Applicant: BASF SE
Inventor： BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , KORADIN CHRISTOPHER , PLETSCH ANDREAS , EHRESMANN MANFRED , SCHRODER HARTWIG
IPC: C07D493/04 , A01N43/90
Abstract: The present invention relates to a method for preparing the pyripyropene compound of the formula (I) which method comprises the following steps: i) subjecting a pyripyropene compound of formula Pyripyropene A to an alkaline hydrolysis to yield a 1,7,11-trideacetylpyripyropene A, ii) reacting 1,7,1 1-trideacetylpyripyropene A obtained in step i) with cyclopropane carbonyl chloride to yield a raw product containing the pyripyropene compound of formula (I); iii) subjecting the raw product of step ii) to crystallization to yield a crystalline pyripyropene compound of formula (I) and a mother liquor;and iv) recycling the mother liquor or a pyripyropene compound containing fraction thereof to the alkaline hydrolysis of step i).
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公开(公告)号：MX2015009223A
公开(公告)日：2015-10-15
申请号：MX2015009223
申请日：2014-01-15
Applicant: BASF SE
Inventor： SCHRÖDER HARTWIG , KORADIN CHRISTOPHER , BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , PLETSCH ANDREAS , EHRESMANN MANFRED
IPC: C07D493/04 , A01N43/90
Abstract: La presente invención se refiere a un método para preparar el compuesto de piripiropeno de la Fórmula i (ver Fórmula) en donde el método comprende las siguientes etapas: i) someter un compuesto de piripiropeno de la fórmula piripiropeno A a una hidrólisis alcalina para obtener 1,7,11-trideacetilpiripiropeno A, ii) hacer reaccionar 1,7,11-trideacetilpiripiropeno A obtenido en la etapa i) con cloruro de ciclopropancarbonilo, a fin de obtener un producto crudo que contiene el compuesto de piripiropeno de la Fórmula I; iii) someter el producto crudo de la etapa ii) a cristalización para obtener un compuesto cristalino de piripiropeno de la Fórmula I y un licor madre; y iv) reciclar el licor madre o una fracción de este que contiene el compuesto de piripiropeno a la hidrólisis alcalina de la etapa i).
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公开(公告)号：AU2014242607B2
公开(公告)日：2017-10-19
申请号：AU2014242607
申请日：2014-03-03
Applicant: BASF SE
Inventor： ERNST BURKHARD , EHRESMANN MANFRED , KORADIN CHRISTOPHER , PLETSCH ANDREAS , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , SIEGEL WOLFGANG , SCHRODER HARTWIG , FREYER STEPHAN , ODMAN PETER
IPC: C12P17/18
Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.
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Patent Agency Ranking
公开(公告)号：AU2014206958B2
公开(公告)日：2017-08-10
申请号：AU2014206958
申请日：2014-01-15
Applicant: BASF SE
Inventor： BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , KORADIN CHRISTOPHER , PLETSCH ANDREAS , EHRESMANN MANFRED , SCHRODER HARTWIG
IPC: C07D493/04 , A01N43/90
Abstract: The present invention relates to a method for preparing the pyripyropene compound of the formula (I) which method comprises the following steps: i) subjecting a pyripyropene compound of formula Pyripyropene A to an alkaline hydrolysis to yield a 1,7,11-trideacetylpyripyropene A, ii) reacting 1,7,11-trideacetylpyripyropene A obtained in step i) with cyclopropane carbonyl chloride to yield a raw product containing the pyripyropene compound of formula (I); iii) subjecting the raw product of step ii) to crystallization to yield a crystalline pyripyropene compound of formula (I) and a mother liquor;and iv) recycling the mother liquor or a pyripyropene compound containing fraction thereof to the alkaline hydrolysis of step i).
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公开(公告)号：ES2602190T3
公开(公告)日：2017-02-20
申请号：ES13715694
申请日：2013-04-12
Applicant: BASF SE
Inventor： BONNEKESSEL MELANIE , ERNST HANSGEORG , SIEGEL WOLFGANG , WINTERFELDT EKKEHARD , HOFFMANN REINHARD
IPC: C07C29/124 , C07C1/04 , C07C1/34 , C07C13/04 , C07C17/08 , C07C21/215 , C07C33/02 , C07C67/00 , C07C69/007 , C07C69/145 , C07D307/92
Abstract: Procedimiento para la producción de compuestos de la fórmula general I**Fórmula** en la que R1 representa un radical hidrocarburo con 1 a 50 átomos de carbono, de cadena recta o ramificada, dado el caso con una o varias insaturaciones, conteniendo la cadena de hidrocarburo dado el caso heteroátomos y R2 representa H o alquilo C1-C6, en el que a) un compuesto carbonilo de la fórmula II**Fórmula** en la que R1 y R2 poseen los significados indicados anteriormente, se hace reaccionar por medio de la formación de olefina de Wittig hasta dar un ciclopropano de la fórmula general (III)**Fórmula** en la que R1 y R2 poseen los significados indicados anteriormente, b) se hace reaccionar el ciclopropano de la fórmula III con apertura de anillo hasta dar un compuesto de la fórmula IV**Fórmula** en la que R1 y R2 poseen los significados indicados anteriormente, y X representa halógeno o representa O-R', en donde R' representa H, acilo, Tf-acetilo o SO2-R", en donde R" representa alquilo o arilo; y c) se transforma el compuesto de la fórmula general IV en el compuesto de la fórmula general I.
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公开(公告)号：DK2945949T3
公开(公告)日：2019-08-05
申请号：DK14700640
申请日：2014-01-15
Applicant: BASF SE
Inventor： HOOCK RALF , KORADIN CHRISTOPHER , PLETSCH ANDREAS , EHRESMANN MANFRED , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHRÖDER HARTWIG , REICHERT WOLFGANG
IPC: C07D493/04 , A01N43/90
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公开(公告)号：ES2705537T3
公开(公告)日：2019-03-25
申请号：ES14774843
申请日：2014-03-03
Applicant: BASF SE
Inventor： ERNST BURKHARD , EHRESMANN MANFRED , KORADIN CHRISTOPHER , PLETSCH ANDREAS , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , SIEGEL WOLFGANG , SCHRÖDER HARTWIG , FREYER STEPHAN , ÖDMAN PETER
Abstract: Un proceso para obtener al menos un piripiropeno, que comprende las etapas de a) cultivar un organismo productor de piripiropeno en un caldo de cultivo en condiciones de cultivo, en el que se produce al menos un piripiropeno, b) producir biomasa seca con un contenido de agua residual (peso/peso) inferior al 8 % de al menos una parte de la biomasa obtenida en la etapa a), c) obtener al menos un piripiropeno a partir de la biomasa seca producida en la etapa b).
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公开(公告)号：DK2978852T3
公开(公告)日：2019-02-18
申请号：DK14774843
申请日：2014-03-03
Applicant: BASF SE
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