公开(公告)号：CA2898963A1

公开(公告)日：2014-10-02

申请号：CA2898963

申请日：2014-03-03

Applicant: BASF SE

Inventor： ERNST BURKHARD ,  EHRESMANN MANFRED ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  BONNEKESSEL MELANIE ,  KAEDING THOMAS ,  SCHEIN-ALBRECHT KARIN ,  DEMMING STEFANIE ,  WEBER FRANZ ,  SIEGEL WOLFGANG ,  SCHRODER HARTWIG ,  FREYER STEPHAN ,  ODMAN PETER

IPC: C12P17/18

Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.

公开(公告)号：AT401297T

公开(公告)日：2008-08-15

申请号：AT02794543

申请日：2002-08-02

Applicant: BASF SE

Inventor： KUDIS STEFFEN ,  LOCHTMAN RENE ,  EHRESMANN MANFRED ,  KEIL MICHAEL ,  GEBHARDT JOACHIM ,  RACK MICHAEL ,  SCHIMETZEK RALF

IPC: C07C201/04 ,  C07B61/00 ,  C07C203/00

Abstract: In a continuous process for the preparation of alkyl nitrites and dinitrites, an alkanol or dialkanol is first mixed with an aqueous mineral acid, the reaction mixture obtained is then reacted with an inorganic nitrite and the product obtained can then be isolated immediately.

公开(公告)号：AU2014242607B2

公开(公告)日：2017-10-19

申请号：AU2014242607

申请日：2014-03-03

Applicant: BASF SE

Inventor： ERNST BURKHARD ,  EHRESMANN MANFRED ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  BONNEKESSEL MELANIE ,  KAEDING THOMAS ,  SCHEIN-ALBRECHT KARIN ,  DEMMING STEFANIE ,  WEBER FRANZ ,  SIEGEL WOLFGANG ,  SCHRODER HARTWIG ,  FREYER STEPHAN ,  ODMAN PETER

IPC: C12P17/18

Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.

公开(公告)号：AU2014206958B2

公开(公告)日：2017-08-10

申请号：AU2014206958

申请日：2014-01-15

Applicant: BASF SE

Inventor： BONNEKESSEL MELANIE ,  REICHERT WOLFGANG ,  HOOCK RALF ,  KAEDING THOMAS ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  EHRESMANN MANFRED ,  SCHRODER HARTWIG

IPC: C07D493/04 ,  A01N43/90

Abstract: The present invention relates to a method for preparing the pyripyropene compound of the formula (I) which method comprises the following steps: i) subjecting a pyripyropene compound of formula Pyripyropene A to an alkaline hydrolysis to yield a 1,7,11-trideacetylpyripyropene A, ii) reacting 1,7,11-trideacetylpyripyropene A obtained in step i) with cyclopropane carbonyl chloride to yield a raw product containing the pyripyropene compound of formula (I); iii) subjecting the raw product of step ii) to crystallization to yield a crystalline pyripyropene compound of formula (I) and a mother liquor;and iv) recycling the mother liquor or a pyripyropene compound containing fraction thereof to the alkaline hydrolysis of step i).

公开(公告)号：BRPI0806301A2

公开(公告)日：2011-09-06

申请号：BRPI0806301

申请日：2008-01-21

Applicant: BASF SE

Inventor： MAYWALD VOLKER ,  OTT CHRISTIAN ,  WOLF BERNAD ,  EHRESMANN MANFRED ,  RACK MICHAEL ,  KEIL MICHAEL ,  SMIDT SEBASTIAN PEER

IPC: C07C67/343 ,  C07C17/12 ,  C07C25/13 ,  C07C69/65

公开(公告)号：CA2898115C

公开(公告)日：2021-03-02

申请号：CA2898115

申请日：2014-01-15

Applicant: BASF SE

Inventor： BONNEKESSEL MELANIE ,  REICHERT WOLFGANG ,  HOOCK RALF ,  KAEDING THOMAS ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  EHRESMANN MANFRED ,  SCHRODER HARTWIG

IPC: C07D493/04 ,  A01N43/90

Abstract: The present invention relates to a method for preparing the pyripyropene compound of the formula (I) which method comprises the following steps: i) subjecting a pyripyropene compound of formula Pyripyropene A to an alkaline hydrolysis to yield a 1,7,11-trideacetylpyripyropene A, ii) reacting 1,7,1 1-trideacetylpyripyropene A obtained in step i) with cyclopropane carbonyl chloride to yield a raw product containing the pyripyropene compound of formula (I); iii) subjecting the raw product of step ii) to crystallization to yield a crystalline pyripyropene compound of formula (I) and a mother liquor;and iv) recycling the mother liquor or a pyripyropene compound containing fraction thereof to the alkaline hydrolysis of step i).

公开(公告)号：MX2015009223A

公开(公告)日：2015-10-15

申请号：MX2015009223

申请日：2014-01-15

Applicant: BASF SE

Inventor： SCHRÖDER HARTWIG ,  KORADIN CHRISTOPHER ,  BONNEKESSEL MELANIE ,  REICHERT WOLFGANG ,  HOOCK RALF ,  KAEDING THOMAS ,  PLETSCH ANDREAS ,  EHRESMANN MANFRED

IPC: C07D493/04 ,  A01N43/90

Abstract: La presente invención se refiere a un método para preparar el compuesto de piripiropeno de la Fórmula i (ver Fórmula) en donde el método comprende las siguientes etapas: i) someter un compuesto de piripiropeno de la fórmula piripiropeno A a una hidrólisis alcalina para obtener 1,7,11-trideacetilpiripiropeno A, ii) hacer reaccionar 1,7,11-trideacetilpiripiropeno A obtenido en la etapa i) con cloruro de ciclopropancarbonilo, a fin de obtener un producto crudo que contiene el compuesto de piripiropeno de la Fórmula I; iii) someter el producto crudo de la etapa ii) a cristalización para obtener un compuesto cristalino de piripiropeno de la Fórmula I y un licor madre; y iv) reciclar el licor madre o una fracción de este que contiene el compuesto de piripiropeno a la hidrólisis alcalina de la etapa i).

公开(公告)号：EP2978852A4

公开(公告)日：2016-10-26

申请号：EP14774843

申请日：2014-03-03

Applicant: BASF SE

Inventor： ERNST BURKHARD ,  EHRESMANN MANFRED ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  BONNEKESSEL MELANIE ,  KAEDING THOMAS ,  SCHEIN-ALBRECHT KARIN ,  DEMMING STEFANIE ,  WEBER FRANZ ,  SIEGEL WOLFGANG ,  SCHRÖDER HARTWIG ,  FREYER STEPHAN ,  ÖDMAN PETER

IPC: C12P17/18 ,  A01N43/40

CPC classification number: C07D493/04 ,  A01N43/40 ,  C12P17/181

Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula III and/or Formula IV and/or Formula V from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula III and/or Formula IV and/or Formula V, including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula IV and/or Formula V in order to produce pest control compositions, in particular insecticides, comprising such compounds.

Abstract translation: 本发明涉及产生拟南芥生产生物体的干燥生物质的方法，从这种干燥生物质中获得拟南芥的方法，以及从得自二氯苯的方法得到式III和/或式IV和/或式V化合物的方法 干生物量。 本发明进一步涉及干生物质本身，以及使用所述干生物质获得用于生产式III和/或式IV和/或式V化合物的吡啶并入的方法，包括使用所述干生物质获得吡啶并吡喃 或式III和/或式IV和/或式V的化合物，以便制备包含这些化合物的害虫控制组合物，特别是杀虫剂。

公开(公告)号：CA2898963C

公开(公告)日：2021-09-14

申请号：CA2898963

申请日：2014-03-03

Applicant: BASF SE

Inventor： ERNST BURKHARD ,  EHRESMANN MANFRED ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  BONNEKESSEL MELANIE ,  KAEDING THOMAS ,  SCHEIN-ALBRECHT KARIN ,  DEMMING STEFANIE ,  WEBER FRANZ ,  SIEGEL WOLFGANG ,  SCHRODER HARTWIG ,  FREYER STEPHAN ,  ODMAN PETER

IPC: C12P17/18

Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.

公开(公告)号：ES2742301T3

公开(公告)日：2020-02-13

申请号：ES14700640

申请日：2014-01-15

Applicant: BASF SE

Inventor： BONNEKESSEL MELANIE ,  REICHERT WOLFGANG ,  HOOCK RALF ,  KAEDING THOMAS ,  KORADIN CHRISTOPHER ,  PLETSCH ANDREAS ,  EHRESMANN MANFRED ,  SCHRÖDER HARTWIG

IPC: C07D493/04 ,  A01N43/90

Abstract: Método para preparar el compuesto de piripiropeno de fórmula I,**Fórmula** comprendiendo el método las siguientes etapas: i) someter un compuesto de piripiropeno de fórmula II a una hidrólisis alcalina para producir un compuesto de piripiropeno de fórmula III,**Fórmula** ii) hacer reaccionar el compuesto de piripiropeno de fórmula III obtenido en la etapa i) con cloruro de ciclopropanocarbonilo para producir un producto sin procesar que contiene el compuesto de piripiropeno de fórmula I; iii) someter el producto sin procesar de la etapa ii) a cristalización para producir un compuesto de piripiropeno cristalino de fórmula I y unas aguas madre; y iv) recircular las aguas madre o una fracción que contiene compuesto de piripiropeno de las mismas a la hidrólisis alcalina de la etapa i).