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公开(公告)号：AU2014242607B2
公开(公告)日：2017-10-19
申请号：AU2014242607
申请日：2014-03-03
Applicant: BASF SE
Inventor： ERNST BURKHARD , EHRESMANN MANFRED , KORADIN CHRISTOPHER , PLETSCH ANDREAS , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , SIEGEL WOLFGANG , SCHRODER HARTWIG , FREYER STEPHAN , ODMAN PETER
IPC: C12P17/18
Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.
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公开(公告)号：AU2014206958B2
公开(公告)日：2017-08-10
申请号：AU2014206958
申请日：2014-01-15
Applicant: BASF SE
Inventor： BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , KORADIN CHRISTOPHER , PLETSCH ANDREAS , EHRESMANN MANFRED , SCHRODER HARTWIG
IPC: C07D493/04 , A01N43/90
Abstract: The present invention relates to a method for preparing the pyripyropene compound of the formula (I) which method comprises the following steps: i) subjecting a pyripyropene compound of formula Pyripyropene A to an alkaline hydrolysis to yield a 1,7,11-trideacetylpyripyropene A, ii) reacting 1,7,11-trideacetylpyripyropene A obtained in step i) with cyclopropane carbonyl chloride to yield a raw product containing the pyripyropene compound of formula (I); iii) subjecting the raw product of step ii) to crystallization to yield a crystalline pyripyropene compound of formula (I) and a mother liquor;and iv) recycling the mother liquor or a pyripyropene compound containing fraction thereof to the alkaline hydrolysis of step i).
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公开(公告)号：CA2898115C
公开(公告)日：2021-03-02
申请号：CA2898115
申请日：2014-01-15
Applicant: BASF SE
Inventor： BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , KORADIN CHRISTOPHER , PLETSCH ANDREAS , EHRESMANN MANFRED , SCHRODER HARTWIG
IPC: C07D493/04 , A01N43/90
Abstract: The present invention relates to a method for preparing the pyripyropene compound of the formula (I) which method comprises the following steps: i) subjecting a pyripyropene compound of formula Pyripyropene A to an alkaline hydrolysis to yield a 1,7,11-trideacetylpyripyropene A, ii) reacting 1,7,1 1-trideacetylpyripyropene A obtained in step i) with cyclopropane carbonyl chloride to yield a raw product containing the pyripyropene compound of formula (I); iii) subjecting the raw product of step ii) to crystallization to yield a crystalline pyripyropene compound of formula (I) and a mother liquor;and iv) recycling the mother liquor or a pyripyropene compound containing fraction thereof to the alkaline hydrolysis of step i).
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公开(公告)号：MX2015009223A
公开(公告)日：2015-10-15
申请号：MX2015009223
申请日：2014-01-15
Applicant: BASF SE
Inventor： SCHRÖDER HARTWIG , KORADIN CHRISTOPHER , BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , PLETSCH ANDREAS , EHRESMANN MANFRED
IPC: C07D493/04 , A01N43/90
Abstract: La presente invención se refiere a un método para preparar el compuesto de piripiropeno de la Fórmula i (ver Fórmula) en donde el método comprende las siguientes etapas: i) someter un compuesto de piripiropeno de la fórmula piripiropeno A a una hidrólisis alcalina para obtener 1,7,11-trideacetilpiripiropeno A, ii) hacer reaccionar 1,7,11-trideacetilpiripiropeno A obtenido en la etapa i) con cloruro de ciclopropancarbonilo, a fin de obtener un producto crudo que contiene el compuesto de piripiropeno de la Fórmula I; iii) someter el producto crudo de la etapa ii) a cristalización para obtener un compuesto cristalino de piripiropeno de la Fórmula I y un licor madre; y iv) reciclar el licor madre o una fracción de este que contiene el compuesto de piripiropeno a la hidrólisis alcalina de la etapa i).
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公开(公告)号：DK3484996T3
公开(公告)日：2020-12-07
申请号：DK17736682
申请日：2017-07-12
Applicant: BASF SE
Inventor： HAGE KERSTIN , SCHWALB CARSTEN , STEIGELMANN GUNTER , KAEDING THOMAS , BRIECHLE SEBASTIAN
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Patent Agency Ranking
公开(公告)号：CA3005292A1
公开(公告)日：2017-06-15
申请号：CA3005292
申请日：2016-12-08
Applicant: BASF SE
Inventor： TREIER-MARXEN KATRIN , DECKERT PETRA , SCHAEDLER ANDREAS , NAVICKAS VAIDOTAS , WENGERT VOLKER , KAEDING THOMAS
Abstract: The present invention is directed to a method of purifying a protein of interest from the particulate matter of a fermentation broth comprising the step of purifying the protein of interest from the particulate matter of the fermentation broth, wherein the step of purifying the protein of interest from the particulate matter of the fermentation broth comprises one or more washing steps, which comprises contacting the particulate matter with a washing solution comprising one or more conditions that favor the solubilization of the protein of interest and/or the desorption of the protein of interest from the particulate matter.
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公开(公告)号：CA2898963A1
公开(公告)日：2014-10-02
申请号：CA2898963
申请日：2014-03-03
Applicant: BASF SE
Inventor： ERNST BURKHARD , EHRESMANN MANFRED , KORADIN CHRISTOPHER , PLETSCH ANDREAS , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , SIEGEL WOLFGANG , SCHRODER HARTWIG , FREYER STEPHAN , ODMAN PETER
IPC: C12P17/18
Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.
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公开(公告)号：CA2898963C
公开(公告)日：2021-09-14
申请号：CA2898963
申请日：2014-03-03
Applicant: BASF SE
Inventor： ERNST BURKHARD , EHRESMANN MANFRED , KORADIN CHRISTOPHER , PLETSCH ANDREAS , BONNEKESSEL MELANIE , KAEDING THOMAS , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , SIEGEL WOLFGANG , SCHRODER HARTWIG , FREYER STEPHAN , ODMAN PETER
IPC: C12P17/18
Abstract: The invention pertains to processes to produce dry biomass of pyripyropene producer organisms, processes to obtain pyripyropenes from such dry biomass, as well as to processes to produce compounds of Formula (III) and/or Formula (IV) and/or Formula (V) from the pyripyropenes obtained from the dry biomass. The invention does further pertain to the dry biomass itself, as well as processes using said dry biomass to obtain pyripyropenes for the production of compounds of Formula (III) and/or Formula (IV) and/or Formula (V), including processes using said dry biomass to obtain pyripyropenes or compounds of Formula III and/or Formula (IV) and/or Formula (V) in order to produce pest control compositions, in particular insecticides, comprising such compounds.
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公开(公告)号：ES2742301T3
公开(公告)日：2020-02-13
申请号：ES14700640
申请日：2014-01-15
Applicant: BASF SE
Inventor： BONNEKESSEL MELANIE , REICHERT WOLFGANG , HOOCK RALF , KAEDING THOMAS , KORADIN CHRISTOPHER , PLETSCH ANDREAS , EHRESMANN MANFRED , SCHRÖDER HARTWIG
IPC: C07D493/04 , A01N43/90
Abstract: Método para preparar el compuesto de piripiropeno de fórmula I,**Fórmula** comprendiendo el método las siguientes etapas: i) someter un compuesto de piripiropeno de fórmula II a una hidrólisis alcalina para producir un compuesto de piripiropeno de fórmula III,**Fórmula** ii) hacer reaccionar el compuesto de piripiropeno de fórmula III obtenido en la etapa i) con cloruro de ciclopropanocarbonilo para producir un producto sin procesar que contiene el compuesto de piripiropeno de fórmula I; iii) someter el producto sin procesar de la etapa ii) a cristalización para producir un compuesto de piripiropeno cristalino de fórmula I y unas aguas madre; y iv) recircular las aguas madre o una fracción que contiene compuesto de piripiropeno de las mismas a la hidrólisis alcalina de la etapa i).
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公开(公告)号：MX2015013807A
公开(公告)日：2016-06-02
申请号：MX2015013807
申请日：2014-03-03
Applicant: BASF SE
Inventor： SCHRÖDER HARTWIG , SIEGEL WOLFGANG , KORADIN CHRISTOPHER , BONNEKESSEL MELANIE , KAEDING THOMAS , PLETSCH ANDREAS , EHRESMANN MANFRED , ERNST BURKHARD , SCHEIN-ALBRECHT KARIN , DEMMING STEFANIE , WEBER FRANZ , FREYER STEPHAN , ÖDMAN PETER
IPC: C12P17/18
Abstract: La invención concierne procedimientos para producir biomasa seca de organismos productores de piripiropeno, procedimientos para obtener piripiropenos a partir de esa biomasa seca, así como procedimientos para producir compuestos de la Fórmula III y/o la Fórmula IV y/o Fórmula V a partir de los piripiropenos obtenidos a partir de la biomasa seca. La invención se refiere además a la biomasa seca misma, así como a procedimientos que se valen de dicha biomasa seca a fin de obtener piripiropenos para la producción de compuestos de la Fórmula III y/o la Fórmula IV y/o la fórmula V, inclusive a procedimientos que usan dicha biomasa seca para obtener piripiropenos o compuestos de la Fórmula III y/o la fórmula IV y/o la fórmula V a fin de producir composiciones para control de plagas, en particular insecticidas que contienen esos compuestos.
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