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    Oxidation resisting hydrocarbon products
    21.
    发明授权
    Oxidation resisting hydrocarbon products 失效

    公开(公告)号：US2552570A

    公开(公告)日：1951-05-15

    申请号：US78867047

    申请日：1947-11-28

    Applicant: STANDARD OIL DEV CO

    Inventor： MCNAB JOHN G ,  HAKALA NIILO V ,  MCDERMOTT JOHN P

    IPC: C10L1/26 ,  C10M137/10

    CPC classification number: C10M137/10 ,  C10L1/26 ,  C10L1/265 ,  C10L1/2691 ,  C10M2201/041 ,  C10M2201/042 ,  C10M2201/062 ,  C10M2203/00 ,  C10M2203/10 ,  C10M2203/108 ,  C10M2205/00 ,  C10M2205/16 ,  C10M2205/18 ,  C10M2205/20 ,  C10M2207/021 ,  C10M2207/023 ,  C10M2207/027 ,  C10M2207/08 ,  C10M2207/10 ,  C10M2207/125 ,  C10M2207/129 ,  C10M2207/144 ,  C10M2207/146 ,  C10M2207/16 ,  C10M2207/24 ,  C10M2207/28 ,  C10M2207/40 ,  C10M2207/404 ,  C10M2209/082 ,  C10M2209/10 ,  C10M2211/00 ,  C10M2211/044 ,  C10M2211/06 ,  C10M2215/02 ,  C10M2215/04 ,  C10M2215/202 ,  C10M2215/26 ,  C10M2219/024 ,  C10M2219/044 ,  C10M2219/062 ,  C10M2219/066 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089 ,  C10M2223/04 ,  C10M2223/042 ,  C10M2223/045 ,  C10M2223/121 ,  C10N2210/00 ,  C10N2210/01 ,  C10N2210/02 ,  C10N2210/03 ,  C10N2230/12 ,  C10N2240/00 ,  C10N2240/04 ,  C10N2240/042 ,  C10N2240/044 ,  C10N2240/046 ,  C10N2240/22 ,  C10N2240/30 ,  C10N2240/40 ,  C10N2240/50 ,  C10N2240/52 ,  C10N2240/54 ,  C10N2240/56 ,  C10N2240/58 ,  C10N2240/60 ,  C10N2240/66 ,  C10N2250/10 ,  C10N2260/04 ,  C10N2270/02

    Abstract: Cuprous thiophosphates of formula where R and R1 are organic radicals which may be hydrocarbon, halogen-substituted hydrocarbon or nitro-substituted hydrocarbon radicals, the sum of the carbon atoms in aliphatic or cycloaliphatic groups in R and R1 being not less than 10 and X is oxygen or sulphur, are prepared by treating the corresponding thiophosphoric acid with cuprous oxide, preferably in the presence of a reducing agent and/or in an inert atmosphere. The thiophosphoric acid may be prepared by treating an appropriate alcohol, phenol, mercaptan or thiophenol with phosphorus pentasulphide. Alcohols mentioned are 2-ethylhexanol, methyl cyclohexanol, a mixture of C12 to C16 alcohols, normal straight-chain alcohols, alcohols derived from natural waxes or from the oxidation of petroleum hydrocarbons, lauryl, stearyl and oleyl alcohols, wool-fat alcohols, and sperm oil alcohols; alkylated phenols and naphthols such as amyl and octyl phenols, wax-alkylated phenols and petroleum phenols are also mentioned. The corresponding mercaptans and thiophenols may also be used, as well as a mixture of alcohols, such as a mixture of isopropanol and 2-ethylhexanol. In one example, 2-ethylhexanol is heated with phosphorus pentasulphide for 1 1/2 hours at 90 DEG C. After filtration the acid is added to a slurry of cuprous oxide and sodium hydrosulphite in benzene. The product is filtered, the filtrate is dissolved in mineral oil, and the benzene and water are removed by heating. The preparation of cuprous nonyl, octyl, methylcyclohexyl, isopropyl, ethyl-hexyl and C12-C16 alkyl secondary butyl thiophosphates is also described. Specification 601.586 is referred to.ALSO:Hydrocarbon products are mixed with a small proportion of a compound of formula where R and R1 are organic radicals which may be hydrocarbon, halogen-substituted hydrocarbon and nitro substituted hydrocarbon radicals, the sum of the carbon atoms in aliphatic or cycloaliphatic groups in R and R1 being not less than 10, and where X is oxygen or sulphur. The tendency of the products to corrode metal surfaces and to undergo atmospheric oxidation is thus reduced. The hydrocarbon products may be hydrocarbon lubricating oils, hydrocarbon fuels such as Diesel fuel and kerosene, synthetic rubbers and hydrocarbon waxes. The hydrocarbon oils may be mineral oils or synthetic oils such as those prepared by the polymerisation of olefins, and mixtures of mineral oils with animal, vegetable and fish oils may also be used. The alcohol from which the thiophosphoric acid is derived may be 2-ethylhexanol, methylcyclohexanol, a mixture of C12 to C16 alcohols, normal straight-chain alcohols, alcohols derived from natural waxes or from the oxidation of petroleum hydrocarbons, lauryl, stearyl and oleyl alcohols, wool-fat alcohols and sperm oil alcohols; alkylated phenols and naphthols such as amyl and octyl phenols, wax-alkylated phenols and petroleum phenols are also mentioned. The corresponding mercaptans or thiophenols may also be used. Additives specified are cuprous methylcyclohexyl, 2-ethylhexyl, nonyl, octyl, isopropyl-ethylhexyl and C12-C16 alkyl - secondary butyl thiophosphates. These compounds are compared in their effects with sodium, potassium and calcium ethylhexyl thiophosphates. From 0.02 to about 3 per cent of the additives may be used. Detergents such as soaps, sulphonates, phenates, alcoholates, carboxylates, alkyl phenol sulphides, organo phosphates, other thiophosphates, phosphites and thiophosphites, salicylates, xanthates, thioxanthates, thiocarbamates, amines, reaction products of phenates and sulphur or phosphorus sulphides may also be added to the compositions. Examples of such detergents include barium tert. octyl phenol sulphide, nickel oleate, aluminium naphthenate, calcium phenyl stearate, calcium petroleum sulphonate and zinc methyl cyclohexyl thiophosphate. In the case of hydrocarbon lubricating compositions, other optional ingredients are dyes, pour point depressors, heat-thickened fatty oils, sulphurised fatty oils, organo-metallic compounds, sludge - dispersers, anti-oxidants, thickeners, viscosity index improvers, oiliness agents, resins, rubber olefin polymers, voltolized fats, voltolized mineral oils or voltolized waxes, graphite, zinc oxide, solvents and assisting agents. Assisting agents particularly mentioned are the higher alcohols, for example octyl, lauryl, cetyl, stearyl, heptadecyl, oleyl, napthenic, phenyl octyl and octadecyl benzyl alcohols, wool fat and sperm oil alcohols, and alcohols produced by the oxidation of petroleum hydrocarbons. Specification 601,586 is referred to.

    Additive for naphthenic acid corrosion inhibition and method of using the same
    25.
    发明授权
    Additive for naphthenic acid corrosion inhibition and method of using the same 有权
    环烷酸腐蚀抑制添加剂及其使用方法

    公开(公告)号：US09115319B2

    公开(公告)日：2015-08-25

    申请号：US12677791

    申请日：2008-09-12

    Applicant: Mahesh Subramaniyam

    Inventor： Mahesh Subramaniyam

    IPC: C10G75/02 ,  C10L1/26 ,  C10L10/04 ,  C10M137/14 ,  C10L1/188

    CPC classification number: C10G75/02 ,  C10G2300/1033 ,  C10G2300/202 ,  C10G2300/203 ,  C10G2300/4075 ,  C10G2300/80 ,  C10L1/1886 ,  C10L1/26 ,  C10L1/2616 ,  C10L1/265 ,  C10L1/2683 ,  C10L1/2691 ,  C10L10/04 ,  C10M137/14 ,  C10M2207/16 ,  C10M2223/065 ,  C10N2230/12

    Abstract: The present invention relates to the field of processing hydrocarbons which causes corrosion in the metal surfaces of processing units. The invention addresses the technical problem of high temperature naphthenic acid corrosion and sulphur corrosion and provides a solution to inhibit these types of corrosion. The three combination compositions are formed by two mixtures separately, with one mixture obtained by mixing compound A, which is obtained by reacting high reactive polyisobutylene (HRPIB) with phosphorous pentasulphide in presence of catalytic amount of sulphur with compound B which is thiophosphorous compound such as phosphorous thioacid ester of Formula (1) and second mixture obtained by mixing compound A with compound C of Formula (2) which is obtained by reacting compound B with ethylene oxide, wherein each of these two mixtures independently provide high corrosion inhibition efficiency in case of high temperature naphthenic acid corrosion inhibition and sulphur corrosion inhibition. The invention is useful in all hydrocarbon processing units, such as, refineries, distillation columns and other petrochemical industries.

    Abstract translation: 本发明涉及在处理单元的金属表面中引起腐蚀的烃的加工领域。 本发明解决了高温环烷酸腐蚀和硫腐蚀的技术问题，并提供了抑制这些腐蚀类型的溶液。 三种组合组合物分别由两种混合物形成，一种混合​​物通过混合化合物A，其通过使高活性聚异丁烯（HRPIB）与五硫化磷在催化量的硫存在下与化合物B（其是硫代磷酸化合物）反应而获得， 通过将化合物B与通式（2）的化合物C混合而获得的第二种混合物，其通过使化合物B与环氧乙烷反应获得，其中这两种混合物中的每一种独立地提供高的腐蚀抑制效率 高温环烷酸腐蚀抑制和硫磺腐蚀抑制。 本发明可用于所有烃处理装置，如炼油厂，蒸馏塔和其他石化行业。

    Soot reduction by combustor conditioning
    26.
    发明授权
    Soot reduction by combustor conditioning 有权
    燃烧器调节烟灰减少

    公开(公告)号：US08453425B2

    公开(公告)日：2013-06-04

    申请号：US12358635

    申请日：2009-01-23

    Applicant: Robert James Perry ,  Patrick Pastecki

    Inventor： Robert James Perry ,  Patrick Pastecki

    IPC: F02B43/00

    CPC classification number: F23K5/10 ,  C10L1/26 ,  C10L1/2608 ,  C10L1/2616 ,  C10L1/2633 ,  C10L1/2641 ,  C10L1/265 ,  C10L10/02

    Abstract: A method of affecting soot particulate size in an internal combustion engine exhaust by selectively providing a phosphorous based additive to the engine during combustion. Soot particulate size can be increased or decreased depending on the particular additive provided. Also disclosed in a conditioning effect experienced by using a phosphorous based additive for a period of time. A conditioned engine can also have its exhaust properties affected during the life of its conditioned state. Manipulating particle size during engine operation can employ an oligomeric phosphorous compound. Engine conditioning can employ a monomeric phosphorous containing compound, an oligomeric phosphorous containing compound, a polymeric phosphorous containing compound, or combinations thereof.

    Abstract translation: 一种通过在燃烧期间选择性地向发动机提供磷基添加剂来影响内燃机排气中烟尘颗粒尺寸的方法。 根据所提供的特定添加剂，烟灰颗粒尺寸可以增加或减少。 还在通过使用基于磷的添加剂经历一段时间的调理效果中也公开。 经调节的发动机在其调节状态的寿命期间也可以具有受其影响的排气性能。 在发动机操作期间操纵粒度可以使用低聚磷化合物。 发动机调节可以使用含单体磷的化合物，含低聚磷的化合物，含聚合磷的化合物或其组合。

    Perfected device to transport vehicles in assembly lines
    28.
    发明申请
    Perfected device to transport vehicles in assembly lines 失效
    在装配线上运输车辆的完美装置

    公开(公告)号：US20030085192A1

    公开(公告)日：2003-05-08

    申请号：US09986097

    申请日：2001-11-07

    Inventor： Adelardo Lopez Alba

    IPC: B66C017/00

    CPC classification number: B66C13/06 ,  B62D65/18 ,  B66F7/0616 ,  B66F7/0666 ,  C10L1/14 ,  C10L1/1616 ,  C10L1/2641 ,  C10L1/265

    Abstract: A device for transporting vehicles during manufacturing is disclosed that allows for upward and downward movement of the vehicle but avoids adverse longitudinal or transverse swinging. The inventive device includes a moving carriage mounted on a fixed rail, an upper frame, a lower frame moveably connected with an elevation mechanism and at least one first pair of articulated arms for stabilizing the vertical movement of the vehicle. An additional pair of articulated arms may be provided which extend and retract in a plane that is perpendicular to the first pair of articulated arms. Additional stabilizing roller elements connected to a fixed rail are provided on a lateral arm of the upper frame to prevent swinging of the upper and the lower frames of the transporting device.

    Abstract translation: 公开了一种用于在制造期间运输车辆的装置，其允许车辆的向上和向下运动，但是避免不利的纵向或横向摆动。 本发明的装置包括安装在固定轨道上的移动滑架，上框架，与升降机构可移动地连接的下框架以及用于稳定车辆垂直运动的至少一对关节臂。 可以提供另外的一对铰接臂，其在垂直于第一对铰接臂的平面中延伸和缩回。 连接到固定轨道的附加稳定辊元件设置在上框架的侧臂上，以防止输送装置的上框架和下框架的摆动。

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