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    OPTICAL ENHANCING DURABLE ANTI-REFLECTIVE COATING
    3.
    发明申请
    OPTICAL ENHANCING DURABLE ANTI-REFLECTIVE COATING 有权
    光学增强耐反射涂层

    公开(公告)号：US20160083620A1

    公开(公告)日：2016-03-24

    申请号：US14491259

    申请日：2014-09-19

    Applicant: Enki Technology, Inc.

    Inventor： Sina Maghsoodi ,  Aravamuthan Varadarajan ,  Meisam Movassat

    IPC: C09D183/04 ,  C08J9/00 ,  C08J9/14 ,  G02B1/111 ,  G02B1/18 ,  C08K3/36 ,  C08K5/19 ,  C08K7/26 ,  G02B1/14 ,  C03C17/30 ,  C08K3/04

    CPC classification number: C09D183/04 ,  C03C17/25 ,  C03C17/30 ,  C03C2217/20 ,  C03C2217/213 ,  C03C2217/732 ,  C03C2218/113 ,  C03C2218/32 ,  C08G77/045 ,  C08G77/16 ,  C08J9/0061 ,  C08J9/142 ,  C08J9/28 ,  C08J2201/026 ,  C08J2201/0502 ,  C08J2383/04 ,  C08J2471/02 ,  C08K3/04 ,  C08K3/041 ,  C08K3/045 ,  C08K3/36 ,  C08K5/19 ,  C08K7/26 ,  C08K2003/045 ,  G02B1/111 ,  G02B1/14 ,  G02B1/18 ,  Y02P20/582

    Abstract: Disclosed herein are polysilsesquioxane based anti-reflective coating (ARC) compositions, methods of preparation, and methods of deposition on a substrate. In embodiments, the polysilsesquioxane of this disclosure is prepared in a two-step process of acid catalyzed hydrolysis of organoalkoxysilane followed by addition of tetralkoxysilane that generates silicone polymers with >40 mol % silanol based on Si-NMR. These high silanol siloxane polymers are stable and have a long shelf-life in the polar organic solvents at room temperature. Also disclosed are low refractive index ARC made from these compositions with and without additives such as porogens, templates, Si—OH condensation catalyst and/or nano-fillers. Also disclosed are methods and apparatus for applying coatings to flat substrates including substrate pre-treatment processes, coating processes including flow coating and roll coating, and coating curing processes including skin-curing using hot-air knives. Also disclosed are coating compositions and formulations for highly tunable, durable, highly abrasion-resistant functionalized anti-reflective coatings.

    Abstract translation: 本文公开了基于聚倍半硅氧烷的抗反射涂层（ARC）组合物，制备方法和沉积在基材上的方法。 在实施方案中，本公开的聚倍半硅氧烷以有机烷氧基硅烷的酸催化水解的两步法制备，然后加入基于Si-NMR产生具有> 40mol％硅烷醇的硅氧烷聚合物的四氢化烷氧基硅烷。 这些高硅烷醇硅氧烷聚合物是稳定的，并且在室温下在极性有机溶剂中具有长的保存期限。 还公开了由具有和不具有添加剂如这些成核剂，模板，Si-OH缩合催化剂和/或纳米填料的这些组合物制成的低折射率ARC。 还公开了用于将涂层施加到平坦基底的方法和装置，包括基底预处理工艺，包括流动涂布和辊涂在内的涂覆工艺，以及包括使用热风刀的皮肤固化的涂层固化过程。 还公开了用于高度可调，耐用，高耐磨性的功能化抗反射涂层的涂料组合物和制剂。

    Optical enhancing durable anti-reflective coating
    4.
    发明授权
    Optical enhancing durable anti-reflective coating 有权
    光学增强耐用抗反射涂层

    公开(公告)号：US09382449B2

    公开(公告)日：2016-07-05

    申请号：US14491259

    申请日：2014-09-19

    Applicant: Enki Technology, Inc.

    Inventor： Sina Maghsoodi ,  Aravamuthan Varadarajan ,  Meisam Movassat

    IPC: C09D183/00 ,  C09D183/04 ,  C03C17/30 ,  C08J9/00 ,  C08J9/14 ,  G02B1/111 ,  C08K3/04 ,  C08K3/36 ,  C08K5/19 ,  C08K7/26 ,  G02B1/14 ,  G02B1/18

    CPC classification number: C09D183/04 ,  C03C17/25 ,  C03C17/30 ,  C03C2217/20 ,  C03C2217/213 ,  C03C2217/732 ,  C03C2218/113 ,  C03C2218/32 ,  C08G77/045 ,  C08G77/16 ,  C08J9/0061 ,  C08J9/142 ,  C08J9/28 ,  C08J2201/026 ,  C08J2201/0502 ,  C08J2383/04 ,  C08J2471/02 ,  C08K3/04 ,  C08K3/041 ,  C08K3/045 ,  C08K3/36 ,  C08K5/19 ,  C08K7/26 ,  C08K2003/045 ,  G02B1/111 ,  G02B1/14 ,  G02B1/18 ,  Y02P20/582

    Abstract: Disclosed herein are polysilsesquioxane based anti-reflective coating (ARC) compositions, methods of preparation, and methods of deposition on a substrate. In embodiments, the polysilsesquioxane of this disclosure is prepared in a two-step process of acid catalyzed hydrolysis of organoalkoxysilane followed by addition of tetralkoxysilane that generates silicone polymers with >40 mol % silanol based on Si-NMR. These high silanol siloxane polymers are stable and have a long shelf-life in the polar organic solvents at room temperature. Also disclosed are low refractive index ARC made from these compositions with and without additives such as porogens, templates, Si—OH condensation catalyst and/or nanofillers. Also disclosed are methods and apparatus for applying coatings to flat substrates including substrate pre-treatment processes, coating processes including flow coating and roll coating, and coating curing processes including skin-curing using hot-air knives. Also disclosed are coating compositions and formulations for highly tunable, durable, highly abrasion-resistant functionalized anti-reflective coatings.

    Abstract translation: 本文公开了基于聚倍半硅氧烷的抗反射涂层（ARC）组合物，制备方法和沉积在基材上的方法。 在实施方案中，本公开的聚倍半硅氧烷以有机烷氧基硅烷的酸催化水解的两步法制备，然后加入基于Si-NMR产生具有> 40mol％硅烷醇的硅氧烷聚合物的四氢化烷氧基硅烷。 这些高硅烷醇硅氧烷聚合物是稳定的，并且在室温下在极性有机溶剂中具有长的保存期限。 还公开了由具有和不具有添加剂如这些成核剂，模板，Si-OH缩合催化剂和/或纳米填料的这些组合物制成的低折射率ARC。 还公开了用于将涂层施加到平坦基底的方法和装置，包括基底预处理工艺，包括流动涂布和辊涂在内的涂覆工艺，以及包括使用热风刀的皮肤固化的涂层固化过程。 还公开了用于高度可调，耐用，高耐磨性的功能化抗反射涂层的涂料组合物和制剂。

    COATING MATERIALS AND METHODS FOR ENHANCED RELIABILITY
    8.
    发明申请
    COATING MATERIALS AND METHODS FOR ENHANCED RELIABILITY 有权
    涂层材料和增强可靠性的方法

    公开(公告)号：US20160013329A1

    公开(公告)日：2016-01-14

    申请号：US14799223

    申请日：2015-07-14

    Applicant: Enki Technology, Inc.

    Inventor： Brenor L. Brophy ,  Sina Maghsoodi ,  Kevin Kopczynski

    IPC: H01L31/0216 ,  H01L31/18 ,  H01L31/048 ,  C09D5/00 ,  C09D5/24

    CPC classification number: C09D5/24 ,  C03C17/002 ,  C03C17/007 ,  C03C17/008 ,  C03C17/23 ,  C03C2217/43 ,  C03C2217/475 ,  C03C2217/732 ,  C03C2217/76 ,  C03C2218/113 ,  C03C2218/31 ,  C09D5/006 ,  H01L31/048 ,  Y02E10/50 ,  Y02P70/521

    Abstract: Glass coating materials and methods are disclosed for the coating of glass substrates used in the manufacturer of photovoltaic solar modules such that the coating enhances the reliability of the module by reducing its susceptibility to potential induced degradation (PID). Coating materials are disclosed that reduce soiling on the front surface of the glass; that increase the surface resistivity of the glass and that repel moisture and that seal the surface from the ingress of moisture. Further electrically conductive coatings are disclosed that reduce the electric field between the front and back surfaces of the glass and hence reduce ion mobility within the glass and transport from the interior glass surface to the solar cell. There are additional configuration choices for fine tuning associated with separately optimizing the exterior and interior glass coating. Finally, coating processes and methods are disclosed for coating glass substrates with the disclosed materials.

    Abstract translation: 公开了用于光伏太阳能模块制造商中使用的玻璃基板的涂覆的玻璃涂层材料和方法，使得涂层通过降低其对潜在的诱导退化（PID）的敏感性来增强模块的可靠性。 公开了减少玻璃前表面污染的涂料; 这增加了玻璃的表面电阻率并且排斥了水分，并且使表面与水分的进入密封。 公开了另外的导电涂层，其减少玻璃的前表面和后表面之间的电场，并因此降低玻璃内的离子迁移率并从内部玻璃表面传输到太阳能电池。 还有另外的配置选择，用于与外部和内部玻璃涂层分开优化相关的微调。 最后，公开了用所公开的材料涂覆玻璃基板的涂布方法和方法。

    HIGH GAIN DURABLE ANTI-REFLECTIVE COATING
    9.
    发明申请
    HIGH GAIN DURABLE ANTI-REFLECTIVE COATING 有权
    高增益耐反射涂层

    公开(公告)号：US20160289457A1

    公开(公告)日：2016-10-06

    申请号：US15182729

    申请日：2016-06-15

    Applicant: Enki Technology, Inc.

    Inventor： Sina Maghsoodi ,  Brenor L. Brophy ,  Thomas E. Colson ,  Peter R. Gonsalves ,  Ze'ev R. Abrams

    IPC: C09D5/00 ,  G02B1/111 ,  C03C17/30 ,  C09D183/08 ,  C09D7/12

    CPC classification number: C09D5/006 ,  C03C17/007 ,  C03C17/30 ,  C03C2217/20 ,  C03C2217/425 ,  C03C2217/45 ,  C03C2217/465 ,  C03C2217/47 ,  C03C2217/732 ,  C08K3/36 ,  C09D7/61 ,  C09D173/00 ,  C09D183/04 ,  C09D183/08 ,  G02B1/11 ,  G02B1/111 ,  G02B1/12 ,  G02B1/14 ,  G02B5/021 ,  G02B5/0215 ,  G02B5/0221 ,  H01L31/02168 ,  H01L31/18 ,  H01L33/005 ,  H01L33/44 ,  Y02E10/50 ,  Y02P20/582

    Abstract: Disclosed herein are polysilsesquioxane-based anti-reflective coating (ARC) compositions, methods of preparation, and methods of deposition on a substrate. In one embodiment, the polysilsesquioxane of this disclosure is prepared in a two-step process of acid catalyzed hydrolysis of organoalkoxysilane followed by addition of tetralkoxysilane that generates silicone polymers with >40 mol % silanol based on Si-NMR. These high silanol siloxane polymers are stable and have a long shelf-life in polar organic solvents at room temperature. Also disclosed are low refractive index ARC made from these compositions with and without additives such as porogens, templates, thermal radical initiator, photo radical initiators, crosslinkers, Si—OH condensation catalyst and nano-fillers. Also disclosed are methods and apparatus for applying coatings to flat substrates including substrate pre-treatment processes, coating processes and coating curing processes including skin-curing using hot-air knives. Also disclosed are coating compositions and formulations for highly tunable, durable, highly abrasion-resistant functionalized anti-reflective coatings.

    Abstract translation: 本文公开了基于聚倍半硅氧烷的抗反射涂层（ARC）组合物，制备方法和沉积在基材上的方法。 在一个实施方案中，本公开的聚倍半硅氧烷是以有机烷氧基硅烷的酸催化水解的两步法制备的，然后加入基于Si-NMR产生具有> 40mol％硅烷醇的硅氧烷聚合物的四氢化烷氧基硅烷。 这些高硅烷醇硅氧烷聚合物是稳定的，并且在室温下在极性有机溶剂中具有长的保质期。 还公开了由具有和不具有添加剂的这些组合物制成的低折射率ARC，例如致孔剂，模板，热自由基引发剂，光自由基引发剂，交联剂，Si-OH缩合催化剂和纳米填料。 还公开了用于将涂层施加到平面基板上的方法和装置，包括基板预处理工艺，涂覆工艺和涂层固化工艺，包括使用热风刀的皮肤固化。 还公开了用于高度可调，耐用，高耐磨性的功能化抗反射涂层的涂料组合物和制剂。

    High gain durable anti-reflective coating
    10.
    发明授权
    High gain durable anti-reflective coating 有权
    高增益耐用抗反射涂层

    公开(公告)号：US09399720B2

    公开(公告)日：2016-07-26

    申请号：US14799507

    申请日：2015-07-14

    Applicant: Enki Technology, Inc.

    Inventor： Sina Maghsoodi ,  Brenor L. Brophy ,  Thomas E. Colson ,  Peter R. Gonsalves ,  Ze'ev R. Abrams

    IPC: C09D183/00 ,  C09D173/00 ,  C09D5/00 ,  G02B1/11 ,  C03C17/30 ,  C09D183/08 ,  G02B1/111 ,  G02B1/12 ,  H01L31/0216 ,  H01L31/18 ,  H01L33/00 ,  H01L33/44

    CPC classification number: C09D5/006 ,  C03C17/007 ,  C03C17/30 ,  C03C2217/20 ,  C03C2217/425 ,  C03C2217/45 ,  C03C2217/465 ,  C03C2217/47 ,  C03C2217/732 ,  C08K3/36 ,  C09D7/61 ,  C09D173/00 ,  C09D183/04 ,  C09D183/08 ,  G02B1/11 ,  G02B1/111 ,  G02B1/12 ,  G02B1/14 ,  G02B5/021 ,  G02B5/0215 ,  G02B5/0221 ,  H01L31/02168 ,  H01L31/18 ,  H01L33/005 ,  H01L33/44 ,  Y02E10/50 ,  Y02P20/582

    Abstract: Disclosed herein are polysilsesquioxane-based anti-reflective coating (ARC) compositions, methods of preparation, and methods of deposition on a substrate. In one embodiment, the polysilsesquioxane of this disclosure is prepared in a two-step process of acid catalyzed hydrolysis of organoalkoxysilane followed by addition of tetralkoxysilane that generates silicone polymers with >40 mol % silanol based on Si-NMR. These high silanol siloxane polymers are stable and have a long shelf-life in polar organic solvents at room temperature. Also disclosed are low refractive index ARC made from these compositions with and without additives such as porogens, templates, thermal radical initiator, photo radical initiators, crosslinkers, Si—OH condensation catalyst and nano-fillers. Also disclosed are methods and apparatus for applying coatings to flat substrates including substrate pre-treatment processes, coating processes and coating curing processes including skin-curing using hot-air knives. Also disclosed are coating compositions and formulations for highly tunable, durable, highly abrasion-resistant functionalized anti-reflective coatings.

    Abstract translation: 本文公开了基于聚倍半硅氧烷的抗反射涂层（ARC）组合物，制备方法和沉积在基材上的方法。 在一个实施方案中，本公开的聚倍半硅氧烷是以有机烷氧基硅烷的酸催化水解的两步法制备的，然后加入基于Si-NMR产生具有> 40mol％硅烷醇的硅氧烷聚合物的四氢化烷氧基硅烷。 这些高硅烷醇硅氧烷聚合物是稳定的，并且在室温下在极性有机溶剂中具有长的保质期。 还公开了由具有和不具有添加剂的这些组合物制成的低折射率ARC，例如致孔剂，模板，热自由基引发剂，光自由基引发剂，交联剂，Si-OH缩合催化剂和纳米填料。 还公开了用于将涂层施加到平面基板上的方法和装置，包括基板预处理工艺，涂覆工艺和涂层固化工艺，包括使用热风刀的皮肤固化。 还公开了用于高度可调，耐用，高耐磨性的功能化抗反射涂层的涂料组合物和制剂。

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