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    Process for the recovery of lithium and other metals from waste lithium ion batteries
    2.
    发明专利
    Process for the recovery of lithium and other metals from waste lithium ion batteries 未知

    公开(公告)号：AU2020323677A1

    公开(公告)日：2022-02-17

    申请号：AU2020323677

    申请日：2020-07-24

    Applicant: BASF SE

    Inventor： ROHDE WOLFGANG ,  GERKE BIRGIT ,  VOGELSANG REGINA ,  VOGES MATTHIAS ,  SCHIERLE-ARNDT KERSTIN ,  SEELER FABIAN ,  ADERMANN TORBEN

    IPC: C22B7/00 ,  C22B3/00 ,  C22B3/12 ,  C22B23/00 ,  C22B26/12

    Abstract: A process for the recovery of one or more transition metals and lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, e.g. in the metallic state; which particulate material further contains a lithium salt; (b) treating the material provided in step (a) with a polar solvent and optionally an alkaline earth hydroxide; (c) separating the solids from the liquid, optionally followed by a solid-solid separation step; and (d) treating the solids containing the transition metal in a way to dissolve at least part of the Ni and/or Co, typically using a mineral acid, provides good separation of lithium in high purity and of transition metal useful for the production of battery cathode active materials.

    Battery recycling by hydrogen gas injection in leach
    4.
    发明专利
    Battery recycling by hydrogen gas injection in leach 未知

    公开(公告)号：AU2019389199A1

    公开(公告)日：2021-06-03

    申请号：AU2019389199

    申请日：2019-11-18

    Applicant: BASF SE

    Inventor： ROHDE WOLFGANG ,  ADERMANN TORBEN ,  GERKE BIRGIT

    IPC: C22B7/00 ,  B22F9/26 ,  C22B3/00

    Abstract: The present invention relates to a process for the recovery of transition metals from batteries comprising (a) treating a transition metal material with a leaching agent to yield a leach which contains dissolved salts of nickel and/or cobalt, (b) injecting hydrogen gas in the leach at a temperature above 100 °C and a partial pressure above 5 bar to precipitate nickel and/or cobalt in elemental form, and (c) separation of the precipitate obtained in step (b).

    PROCESS FOR THE RECOVERY OF LITHIUM FROM WASTE LITHIUM ION BATTERIES
    5.
    发明专利
    PROCESS FOR THE RECOVERY OF LITHIUM FROM WASTE LITHIUM ION BATTERIES 未知

    公开(公告)号：CA3144711A1

    公开(公告)日：2021-02-04

    申请号：CA3144711

    申请日：2020-07-24

    Applicant: BASF SE

    Inventor： ROHDE WOLFGANG ,  GERKE BIRGIT ,  SCHIERLE-ARNDT KERSTIN ,  ADERMANN TORBEN ,  VOGES MATTHIAS ,  VOGELSANG REGINA

    IPC: C22B3/12 ,  C22B7/00 ,  C22B26/12

    Abstract: A process for the recovery of lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Mn, Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, and at least a fraction of said Mn, if present, is manganese(II)oxide; which particulate material further contains a lithium salt and a fluoride salt, and which particulate material optionally contains calcium provided that the element ratio calcium to fluorine is 1.7 or less or is zero; (b) treating the material provided in step (a) with a polar solvent and an alkaline earth hydroxide; and (c) separating the solids from the liquid, optionally followed by washing the solid residue with a polar solvent such as water provides good separation of lithium in high purity, and recovery of valuable transition metals.

    BATTERY RECYCLING BY HYDROGEN GAS INJECTION IN LEACH
    6.
    发明专利
    BATTERY RECYCLING BY HYDROGEN GAS INJECTION IN LEACH 未知

    公开(公告)号：CA3120402A1

    公开(公告)日：2020-06-04

    申请号：CA3120402

    申请日：2019-11-18

    Applicant: BASF SE

    Inventor： ROHDE WOLFGANG ,  ADERMANN TORBEN ,  GERKE BIRGIT

    IPC: C22B7/00 ,  B22F9/26 ,  C22B3/00

    Abstract: The present invention relates to a process for the recovery of transition metals from batteries comprising (a) treating a transition metal material with a leaching agent to yield a leach which contains dissolved salts of nickel and/or cobalt, (b) injecting hydrogen gas in the leach at a temperature above 100 °C and a partial pressure above 5 bar to precipitate nickel and/or cobalt in elemental form, and (c) separation of the precipitate obtained in step (b).

    PROCESS FOR THE GENERATION OF THIN INORGANIC FILMS
    8.
    发明专利
    PROCESS FOR THE GENERATION OF THIN INORGANIC FILMS 未知

    公开(公告)号：SG11201900607WA

    公开(公告)日：2019-03-28

    申请号：SG11201900607W

    申请日：2017-08-23

    Applicant: BASF SE

    Inventor： ADERMANN TORBEN ,  ABELS FALKO ,  LIMBURG CAROLIN ,  WILMER HAGEN ,  GERKENS JAN ,  SCHNEIDER SVEN

    IPC: C07F15/00 ,  C23C16/455

    Abstract: The present invention is in the field of processes for the generation of thin inorganic films on substrates, in particular atomic layer deposition processes. The present invention relates to a process for the generation of inorganic films comprising depositing the compound of general formula (I) onto a solid substrate (I), wherein M is Mn, Ni or Co, X is a ligand which coordinates M, n is 0, 1, 2, 3, or 4, R1 is an alkyl group, an alkenyl group, an aryl group, a halogen, or a silyl group, R2 is an alkyl group, an alkenyl group, an aryl group, or a silyl group, p and q are 1 or 2, wherein p+q=3, and m is 1, 2, or 3.

    Process for the recovery of lithium and other metals from waste lithium ion batteries
    10.
    发明专利
    Process for the recovery of lithium and other metals from waste lithium ion batteries 未知

    公开(公告)号：AU2020323235A1

    公开(公告)日：2022-02-17

    申请号：AU2020323235

    申请日：2020-07-24

    Applicant: BASF SE

    Inventor： ROHDE WOLFGANG ,  GERKE BIRGIT ,  SCHIERLE-ARNDT KERSTIN ,  VOGES MATTHIAS ,  VOGELSANG REGINA ,  SEELER FABIAN ,  SMITH GARETH ,  ADERMANN TORBEN

    IPC: C22B7/00 ,  C22B3/12 ,  C22B23/00 ,  C22B26/12

    Abstract: A process for the recovery of one or more transition metals and lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, e.g. in the metallic state; which particulate material further contains a lithium salt; (b) treating the material provided in step (a) with a polar solvent and optionally an alkaline earth hydroxide; (c) separating the solids from the liquid, optionally followed by a solid-solid separation step; and (d) treating the solids containing the transition metal in a smelting furnace to obtain a metal melt containing Ni and/or Co provides good separation of transition metal as alloy and of lithium in high purity.

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