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公开(公告)号：ES2001726A6
公开(公告)日：1988-06-01
申请号：ES8603311
申请日：1986-12-05
Applicant: KAO CORP
Inventor： NOZAKI TOSHIO , KUROSAKI TOMIHIRO , WAKATSUKI JUNYA , AIMONO KIYOSHI
Abstract: SE PRODUCE UNA SAL DE UN ESTER FOSFORICO DE GRAN PUREZA CONVIRTIENDO UN ESTER FOSFORICO, EN UNA MEZCLA QUE CONTIENE EL ESTER FOSFORICO Y UNO O MAS COMPUESTOS ANIONICOS, EN UNA SAL DE ESTER FOSFORICO EMPLEANDO UN COMPUESTO BASICO Y EXTRAYENDO LOS COMPUESTOS NO IONICOS DE LA MEZCLA ANTERIOR EMPLEANDO UNA MEZCLA DISOLVENTE DE HIDROCARBUROS ALIFATICOS O HIDROCARBUROS CICLOALIFATICOS, UN ALCANOL INFERIOR Y AGUA. EL METODO ANTERIOR ES APLICABLE A UN ESTER FOSFORICO NO CRISTALINO DEL QUE NO PUEDEN SEPARARSE POR RECRISTALIZACION COMPUESTOS NO IONICOS. LA SAL DE ESTER FOSFORICO DE GRAN PUREZA ASI OBTENIDA PUEDE SER UTILIZADA TAL COMO ES O DESPUES DE SOMETERLA A CONDENSACION.
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公开(公告)号：DE3641603A1
公开(公告)日：1987-06-11
申请号：DE3641603
申请日：1986-12-05
Applicant: KAO CORP
Inventor： NOZAKI TOSHIO , KUROSAKI TOMIHIRO , WAKATSUKI JUNYA , AIMONO KIYOSHI
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公开(公告)号：JPH0892263A
公开(公告)日：1996-04-09
申请号：JP22459394
申请日：1994-09-20
Applicant: KAO CORP
Inventor： TSUYUTANI SHINJI , SHIBATA KENGO , AIMONO KIYOSHI
Abstract: PURPOSE: To obtain a phosphoric monoester useful for detergents, textile treating agents, etc., in high purity and yield without converting the reactional product into a gelatinous material by reacting phosphorus pentoxide, etc., with an organic hydroxy compound under specific conditions. CONSTITUTION: The method for producing a phosphoric monoester is to react phosphorus pentoxide and polyphosphoric acid as phosphorylating agents with an organic hydroxy compound such as octanol under conditions so that a value represented by the formula may exceed 3.2, then add the phosphorus pentoxide to the resultant reactional product and carry out the reaction under conditions that the value, represented by the formula and based on the total amount of the polyphosphoric acid and the phosphorus pentoxide may be 2.8-3.2. Furthermore, the concentration of the polyphosphoric acid is preferably 105-120wt.% expressed in terms of orthophosphoric acid and the unreacted organic hydroxy compound is preferably removed from the reactional product containing the phosphoric monoester by the steam distillation to deodorize the reactional product.
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公开(公告)号：JPH0753577A
公开(公告)日：1995-02-28
申请号：JP21901893
申请日：1993-08-10
Applicant: KAO CORP
Inventor： NOMOTO HIDETOSHI , TSUYUTANI SHINJI , AIMONO KIYOSHI
Abstract: PURPOSE:To provide a purification method capable of suppressing thermal hysteresis effect to a minimum and obtaining a high-purity phosphoric ester salt. CONSTITUTION:This purification method is to eliminate a lower alcohol (and a hydrocarbon), from an aqueous solution containing a phosphoric ester salt and the lower alcohol (and the hydrocarbon) by using a thin film evaporator.
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公开(公告)号：JPH06336492A
公开(公告)日：1994-12-06
申请号：JP12593893
申请日：1993-05-27
Applicant: KAO CORP
Inventor： SHIBATA KENGO , OKA KOJI , AIMONO KIYOSHI
Abstract: PURPOSE:To provide a method for fractionating a sucrose fatty acid ester having a specific composition from a reaction mixture of sucrose fatty acid esters by a simple operation without using an organic solvent. CONSTITUTION:Sucrose fatty acid esters composed of a mixture of [SME], [SDE] and [SPE] ([SME] is a sucrose fatty acid ester having 1 ester exchange degree, [SDE] is a sucrose fatty acid ester having 2 ester exchange degree and [SPE] is a sucrose fatty 7 acid ester having >=3 ester exchange degree) are mixed with fats and oils under heating and the prepared heated mixture is incorporated with water to extract a sucrose fatty acid ester having high [SME] content. The prepared water phase and the oil phase are separated to give a sucrose fatty acid ester having high [SME] content and sucrose fatty acid esters having high [SDE] and [SPE] contents.
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Patent Agency Ranking
公开(公告)号：JPH03106895A
公开(公告)日：1991-05-07
申请号：JP24252989
申请日：1989-09-19
Applicant: KAO CORP
Inventor： FUJITA TADAAKI , AIMONO KIYOSHI , HASHIBA KUNIMITSU , OHORI KOICHI
Abstract: PURPOSE:To simply and inexpensively prepare the subject high quality compound or an aqueous solution thereof by flowing a reaction product prepared by directly reacting a saccharide with a higher alcohol, etc., or an aqueous solution of the reaction product in a thin filmy state and subsequently bringing the thin-filmy reaction solution into contact with steam, etc., at a specific temperature. CONSTITUTION:A saccharide such as glucose, maltose or inulin is directly reacted with a higher alcohol of the formula (R is 6-22C alkyl, etc.; A is 2-4C alkylene; n is on the average 0-5), or the saccharide is reacted with a lower alcohol and subsequently with the higher alcohol. The unreacted alcohol contained in the reaction product used for the preparation of an alkylglycoside or an aqueous solution is reduced to 3-10wt.%. The reaction product or the aqueous solution thereof is flowed on a thin film evaporator in a thin film state of
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公开(公告)号：JPH10330338A
公开(公告)日：1998-12-15
申请号：JP13844297
申请日：1997-05-28
Applicant: KAO CORP
Inventor： IWASAKI TOSHIYA , MIZUSHIMA YOUSEN , AIMONO KIYOSHI
IPC: C11D1/28 , C07C231/02 , C07C231/12 , C07C235/06 , C07C235/08 , C07C303/24 , C07C305/10
Abstract: PROBLEM TO BE SOLVED: To obtain the subject compound useful as a raw material for perfumeries, etc., and reduced in an unreacted amine and other volatile impurities by blowing steam or an inactive gas in an N-alkylamidoalkanol during or after an amidation reaction. SOLUTION: This method for producing (C) an N-alkylamidoalkanol of formula IV comprises reacting (A) an amine of formula I (R is a 6-22C linear chain or branched alkyl, an alkenyl, etc.; R is H, a 1-22C liner chain or branched alkyl, an alkenyl, etc.), with (B) a lactone of formula II (R is a 1-5C linear chain or branched alkylene) or an ω-hydroxycarboxylic acid of formula III (R is H, a 1-4C linear chain or branched alkyl) or its ester. Therein, stem or an inactive gas is blown in the reaction solution during or after the amidation reaction. The component A and B are preferably reacted with each other in a component A/component B molar ratio of 0.8-1.2 at a reaction temperate of 50-200 deg.C.
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公开(公告)号：JPH06319973A
公开(公告)日：1994-11-22
申请号：JP11192093
申请日：1993-05-13
Applicant: KAO CORP
Inventor： OKA KOJI , MAEDA TOSHIJI , AIMONO KIYOSHI
Abstract: PURPOSE:To provide a method for preparation of a surfactant wherein impurities which causes change of smell for the worse, deterioration of hue and irritation can be extracted and eliminated efficiently by using an extractant (an extracting solvent) and an inexpensive apparatus and a surfactant with a high quality can be obtd. CONSTITUTION:The title method has a purification process wherein a water soln. of a surfactant contg. a component to be extracted is fed from a tower head part 5A of an extracting apparatus having a cylindrical extracting tower 1A and a plurality of perforated plates 2A arranged horizontally and in the longitudinal direction in the extracting tower 1A and an extractant for extracting a component to be extracted is fed from the tower bottom part 6A and extraction of the component to be extracted is performed while the interfacial position between the water soln. of the surfactant and the extractant is controlled so as to be kept it below the middle stage perforated plate 2A among the plurality of perforated plates 2A.
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公开(公告)号：JPH06157432A
公开(公告)日：1994-06-03
申请号：JP31349292
申请日：1992-11-24
Applicant: KAO CORP
Inventor： FUNENO TOMOHIRO , AIMONO KIYOSHI , MAEDA TOSHIJI
IPC: C07C209/12 , C07C209/86 , C07C211/63
Abstract: PURPOSE:To obtain a compound having excellent color and odor and high quality at a low cost by preparing a reaction solution containing benzalkonium halide from dimethyl-t-amine and a benzyl halide and flowing the reaction solution in the form of a thin film in an inert gas or steam. CONSTITUTION:A solution containing benzalkonium halide of formula (R is 8-30C alkyl or alkenyl) is produced by reacting a dimethyl-t-amine with a benzyl halide. The solution is flowed in the form of a thin film in a flow of a gas inert to the benzalkonium halide or in a steam flow. The evaporation of unreacted benzyl halide is promoted, the odor is improved and a benzalkonium halide having high quality is produced by this process. The contact area of the solution with the steam or inert gas can be increased without causing the foaming of the solution and the effect of the treatment can be improved by flowing the solution in the form of a thin film. The benzalkonium halide is a cationic surfactant useful as a sterilizing agent, an antiseptic agent, a wound cleaning agent, etc. The process enables the production of the compound with easy operation in a short time.
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公开(公告)号：JPH04308599A
公开(公告)日：1992-10-30
申请号：JP7148191
申请日：1991-04-04
Applicant: KAO CORP
Inventor： TSUYUTANI SHINJI , AIMONO KIYOSHI , OKA KOJI
IPC: C07H15/04
Abstract: PURPOSE:To obtain the title compound useful for low-irritating surfactant without deterioration of smell by reacting a sugar with a higher alcohol while irradiating the reaction system with light having specific wavelength, and then carrying out removal of unreacted higher alcohol and decoloration by light irradiation. CONSTITUTION:When a sugar is reacted with a higher alcohol or the sugar is firstly reacted with a lower alcohol and then reacted with a higher alcohol to produce an alkylglycoside, the above-mentioned reaction is carried out while irradiating the reaction system with light having 100-800nm wavelength, and unreacted higher alcohol is removed from the resultant unreacted higher alcohol- containing alkylglycoside or the unreacted higher alcohol-containing alkylglycoside is once more irradiated with light having 100-800nm wavelength and then unreacted higher alcohol is removed, or an alkylglycoside solution after removing unreacted higher alcohol is irradiated with light having 100-800nm wavelength to provide the objective decolored alkylglycoside having good hue.
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