25.
    发明专利
    未知

    公开(公告)号:DE2845075A1

    公开(公告)日:1980-05-08

    申请号:DE2845075

    申请日:1978-10-17

    Applicant: BASF AG

    Abstract: A process for purifying crude caprolactam which has been obtained by rearrangement of cyclohexanone-oxime in the gas phase over a catalyst containing boron trioxide, wherein caprolactam is crystallized out, by cooling, from a melt which contains, per 100 parts by weight of crude caprolactam, from 5 to 30 parts by weight of primary alkanols or fatty acids which have a carbon chain of 6 to 10 carbon atoms and are substituted by alkyl radicals of 1 to 5 carbon atoms, and from 0 to 5 parts by weight of water, and is separated from the mother liquor.

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