25.
    发明专利
    未知

    公开(公告)号:NO20020349L

    公开(公告)日:2002-01-23

    申请号:NO20020349

    申请日:2002-01-23

    Applicant: BASF AG

    Abstract: A description is given of a process for preparing methyl formate by reacting excess methanol with carbon monoxide under superatmospheric pressure and at elevated temperature in the presence of alkali metal methoxide or alkaline earth metal methoxide as catalyst in a pressure-rated reactor, in which the use of at least two reactor elements, preferably operated in countercurrent, at about 100° C. and a pressure of about 100 bar in combination with a solids-free desalting of the reaction product makes possible very economical, largely trouble-free production of methyl formate in any desired quality and with a very good production capacity. Furthermore, the process for solids-free desalting and apparatuses for carrying out this process are described.

    27.
    发明专利
    未知

    公开(公告)号:ID30252A

    公开(公告)日:2001-11-15

    申请号:ID20002702

    申请日:1999-06-30

    Applicant: BASF AG

    Abstract: In a process for the purification of acrylic acid or methacrylic acid by crystallization and distillation, the following steps are carried out:(a) crystallization of a mixture containing the acrylic acid or methacrylic acid with formation of product crystals having a higher concentration of acrylic acid or methacrylic acid and of a mother liquor,(b) distillation of at least part of the mother liquor from step (a) with formation of a distillation residue, which is at least partly removed, and of a top product,(c) crystallization of at least part of the top product from step (b) with formation of a crystallization residue, which is removed, and of crystals and(d) recycling of the crystals from step (c) to the crystallization (a).

Patent Agency Ranking