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    SYNTHESIS OF LITHIUM-IRON-PHOSPHATES UNDER HYDROTHERMAL CONDITIONS
    82.
    发明公开
    SYNTHESIS OF LITHIUM-IRON-PHOSPHATES UNDER HYDROTHERMAL CONDITIONS 有权
    磷酸铁锂的水热条件下合成

    公开(公告)号：EP2408712A2

    公开(公告)日：2012-01-25

    申请号：EP10710825.0

    申请日：2010-03-16

    Applicant: BASF SE

    Inventor： BRAMNIK, Kirill ,  HIBST, Hartmut ,  LAMPERT, Jordan Keith

    IPC: C01B25/45 ,  H01M4/58 ,  H01M4/62 ,  C01B25/26 ,  H01M4/00

    CPC classification number: C01B25/45 ,  H01M4/5825

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) Li
    a-b M
    1
    b Fe
    1-c M
    2
    c P
    d-e M
    3
    e O
    x, wherein Fe has the oxidation state +2 and M
    1 , M
    2 , M
    3 , a, b, c, d, e and x are: M
    1 : Na, K, Rb and/or Cs, M
    2 : Mn, Mg, Al, Ca, Ti, Co, Ni, Cr, V, M
    3 : Si, S, F a: 0.8 - 1.9, b: 0 - 0.3, c: 0 - 0.9, d: 0.8 - 1.9, e: 0 - 0.5, x: 1.0 - 8, depending on the amount and oxidation state of Li, M
    1 , M
    2 , P, M
    3 , wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one iron-comprising compound, in which iron has the oxidation state 0, and at least one M
    1 -comprising compound, if present, and/or at least one M
    2 -comprising compound, if present, and/or least one M
    3 -comprising compound, if present, and at least one compound comprising at least one phosphorous atom in oxidation state +5, and (B) heating the mixture obtained in step (A) at a temperature of 100 to 500 °C and at an autogeneous pressure to obtain a compound of general formula (I).

    ANORGANISCHE PARTIKEL MIT EINER DURCH TEMPERATUR HYDROPHIL/HYDROPHOB SCHALTBAREN ORGANISCHEN BESCHICHTUNG
    86.
    发明公开
    ANORGANISCHE PARTIKEL MIT EINER DURCH TEMPERATUR HYDROPHIL/HYDROPHOB SCHALTBAREN ORGANISCHEN BESCHICHTUNG 有权
    WITH A受温度亲水/疏水切换有机涂层的无机颗粒

    公开(公告)号：EP2313200A1

    公开(公告)日：2011-04-27

    申请号：EP09780763.0

    申请日：2009-07-17

    Applicant: BASF SE ,  SIEMENS AKTIENGESELLSCHAFT

    Inventor： DOMKE, Imme ,  MICHAILOVSKI, Alexej ,  MRONGA, Norbert ,  HIBST, Hartmut ,  TROPSCH, Jürgen ,  STUTZ, Susanne

    IPC: B03C1/01 ,  H01F1/44

    CPC classification number: H01F1/44 ,  B03C1/015 ,  H01F1/0054

    Abstract: The invention relates to a method for separating at least one first substance from a mixture containing said at least one first substance and at least one second substance. Said method consists of the following steps: (A) the mixture containing the at least one first substance and at least one second substance is brought into contact with at least one selective hydrophobing agent in the presence of a suspension agent such that an adduct is formed form at least one hydrophobing agent and the at least one first substance, and not from the at least one second substance; (B) the adduct from step (A) is brought into contact with at least one magnetic particle which is functionalised on the surface with at least one polymer compound having a transition temperature LCST (Lower Critical Solution Temperature), at a temperature at which the polymer compound has a hydrophobic character, such that the adduct from step (A) and the at least one functionalised magnetic particle agglomerates; (C) another suspending agent is optionally added to the mixture obtained in step (B); (D) the agglomerate present in the suspension in steps (B) or (C) is separated by applying a magnetic field; (E) the agglomerate separated in step (D) is divided by controlling a temperature at which the polymer compound has a hydrophilic character, in order to obtain at least one first substance.

    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, VANADIUM- AND PHOSPHATE-COMPRISING MATERIALS
    87.
    发明公开
    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, VANADIUM- AND PHOSPHATE-COMPRISING MATERIALS 有权
    工艺生产结晶锂，钒和含磷酸盐的材料

    公开(公告)号：EP2212247A2

    公开(公告)日：2010-08-04

    申请号：EP08804369.0

    申请日：2008-09-18

    Applicant: BASF SE

    Inventor： HIBST, Hartmut ,  ROBERTS, Brian ,  LAMPERT, Jordan ,  BRAMNIK, Kirill

    IPC: C01B25/45 ,  H01M4/58

    CPC classification number: C01B25/45 ,  H01M4/5825 ,  H01M10/0525

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) Li
    a-b M
    1
    b V
    2-c M
    2
    c (PO
    4 )
    x (I) with M
    1 : Na, K, Rb and/or Cs, M
    2 : Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5 - 4.5, b: 0 - 0.6, c: 0 - 1.98 and x: number to equalize the charge of Li and V and M
    1 and/or M
    2 , if present, wherein a-b is > 0, by providing an essentially aqueous mixture comprising at least one lithium-comprising compound, at least one vanadium-comprising compound in which vanadium has the oxidation state +5 and/or +4, and at least one M
    1 -comprising compound, if present, and/or at least one M
    2 -comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, drying and calcining.

    AUFBEREITUNG VON WERTERZEN DURCH MAGNETPARTIKEL
    88.
    发明公开
    AUFBEREITUNG VON WERTERZEN DURCH MAGNETPARTIKEL 有权
    VALUE矿石磁性颗粒治疗

    公开(公告)号：EP2190584A2

    公开(公告)日：2010-06-02

    申请号：EP08803482.2

    申请日：2008-09-01

    Applicant: BASF SE

    Inventor： DOMKE, Imme ,  MRONGA, Norbert ,  MICHAILOVSKI, Alexej ,  HIBST, Hartmut ,  SERVAY, Thomas ,  KLOPSCH, Rainer

    IPC: B03C1/015

    CPC classification number: B03C1/015 ,  B03C2201/18

    Abstract: The invention relates to a method for removing at least one first substance from a mixture that contains the at least one first substance and at least one second substance. Said method comprises the following steps: (A) contacting the mixture containing at least one first substance and at least one second substance with at least one surface-active substance, optionally in the presence of at least one dispersant, the surface-active substance binding to the at least one first substance, (B) optionally adding at least one dispersant to the mixture obtained in step (A) to obtain a dispersion, (C) treating the dispersion obtained in step (A) or (B) with at least one hydrophobic magnetic particle so that the at least one first substance to which the at least one surface-active substance is bound and the at least one magnetic particle are added thereto, (D) removing the addition product obtained in step (C) from the mixture by applying a magnetic field, (E) breaking down the removed addition product obtained in step (D) to obtain the at least one first substance and the at least one magnetic particle as separate entities.

    VERFAHREN ZUR ERZANREICHERUNG MITTELS HYDROPHOBER, FESTER OBERFLÄCHEN
    89.
    发明公开
    VERFAHREN ZUR ERZANREICHERUNG MITTELS HYDROPHOBER, FESTER OBERFLÄCHEN 有权
    使用方法疏水矿石富集，固体表面

    公开(公告)号：EP2171106A1

    公开(公告)日：2010-04-07

    申请号：EP08785971.6

    申请日：2008-07-08

    Applicant: BASF SE

    Inventor： DOMKE, Imme ,  MICHAILOVSKI, Alexej ,  HIBST, Hartmut

    IPC: C22B1/00 ,  C22B15/00 ,  B03C1/01 ,  B03D1/10

    CPC classification number: C22B1/00 ,  B03C1/01 ,  B03C1/30 ,  B03C2201/20 ,  B03D1/10 ,  C22B15/0002 ,  C22B15/0008

    Abstract: The present invention relates to a method for separating at least one hydrophobic agent from a mixture comprising said at least one hydrophobic agent and at least one hydrophilic agent, comprising the steps of: A) Producing a slurry or dispersion of the mixture to be treated in at least one suitable dispersion agent, B) bringing the slurry or dispersion of step (A) into contact with at least one solid, hydrophobic surface for attaching the at least one hydrophobic agent to be separated to the surface thereof, C) removing the at least one solid, hydrophobic surface, whereon the at least one hydrophobic agent from step (B) is bonded, from the slurry or dispersion, in which the at least one hydrophilic agent is present, and D) separating the at least one hydrophobic agent from the solid, hydrophobic surface. According to the invention, the method is used for separating (hydrophobic) sulfidic minerals, particularly copper sulfides, from mixtures having hydrophilic metal oxides (gang minerals). The solid surface can be, for example, a conveyor belt having a hydrophobic, structured surface.

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