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公开(公告)号：BRPI0507662B1
公开(公告)日：2014-12-09
申请号：BRPI0507662
申请日：2005-02-08
Applicant: BASF AG
Inventor： DEMETER JUERGEN , DEININGER JUERGEN , HAHN THILO , KORY GAD , SOETJE OLIVER , ZEHNER PETER
Abstract: A continuous process for producing polyamides, their oligomers or mixtures thereof, if appropriate with further reaction products, comprises reaction of aminonitriles or dinitriles and diamines or mixtures thereof, if appropriate together with further polyamide-forming monomers and/or oligomers, with an aqueous medium composed of aqueous monomer and oligomer extracts obtained from polyamide production by extraction of the polymer with water in a reactor which has a vertical longitudinal axis and through which there is a flow substantially in the longitudinal direction wherein water and/or the aqueous medium are introduced into the reactor at two or more different locations along the vertical longitudinal axis, wherein the aqueous medium is introduced at one or more locations.
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公开(公告)号：BRPI0511648A
公开(公告)日：2008-01-02
申请号：BRPI0511648
申请日：2005-05-31
Applicant: BASF AG
Inventor： ASSMANN JENS , DEMETER JUERGEN , DEININGER JUERGEN , SOETJE OLIVER , KORY GAD , LOENING JAN-MARTIN
IPC: C08J11/06 , B01D3/14 , B01D5/00 , C01C1/02 , C01C1/10 , C02F1/04 , C08G69/04 , C08G69/16 , C08G69/28 , C08J11/02
Abstract: In a process for distillatively removing ammonia and water from mixtures obtained in the preparation of polyamides which comprise a lactam and/or diamines, and, if appropriate, an aminonitrile and/or dinitrile, and also a cyclopentanone impurity in two stages: 1) the mixture is distilled at from 11 to 35 bar to give, as the top product T1, water, ammonia and cyclopentanone, and, as the bottoms B1, water, the lactam and/or diamines, and, if appropriate, the aminonitrile and/or dinitrile, and 2) T1 is distilled at from 11 to 35 bar to give, as the top product T2, ammonia and cyclopentanone, and, as the bottoms B2, water.
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公开(公告)号：DE502004004653D1
公开(公告)日：2007-09-27
申请号：DE502004004653
申请日：2004-05-06
Applicant: BASF AG
Inventor： WINTERLING HELMUT , DEMETER JUERGEN , DEININGER JUERGEN , KORY GAD , SOETJE OLIVER , WILMS AXEL , WEISS ROBERT , KREMPEL KURT , BENISCH CHRISTOPH
Abstract: Polyamide, whose main chain contains a chemically bound amine selected from the group consisting of 2-methyl-1,5-diaminopentane and 1-amino-2-R-cyclopent-1-ene, where R is a functional group capable of combining with an amino group to form an amide group, and processes for preparing such a polyamide and fibers, films and moldings comprising such a polyamide.
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公开(公告)号：DE102005040656A1
公开(公告)日：2007-03-01
申请号：DE102005040656
申请日：2005-08-26
Applicant: BASF AG
Inventor： YAMAMOTO MOTONORI , DEININGER JUERGEN , SOETJE OLIVER , KORY GAD , EIBECK PETER
IPC: C08G69/00
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公开(公告)号：PL1611184T3
公开(公告)日：2007-02-28
申请号：PL04721865
申请日：2004-03-19
Applicant: BASF AG
Inventor： DEININGER JÜRGEN , DEMETER JÜRGEN , KORY GAD , SÖTJE OLIVER , WINTERLING HELMUT , ZEHNER PETER , HEEGER MICHAEL , GANN MARTIN , POLT AXEL , TREULING ULRICH , WEINLE WERNER
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Patent Agency Ranking
公开(公告)号：DE502004001613D1
公开(公告)日：2006-11-09
申请号：DE502004001613
申请日：2004-03-19
Applicant: BASF AG
Inventor： DEININGER JUERGEN , DEMETER JUERGEN , KORY GAD , SOETJE OLIVER , WINTERLING HELMUT , ZEHNER PETER , HEEGER MICHAEL , GANN MARTIN , POLT AXEL , TREULING ULRICH , WEINLE WERNER
Abstract: Polyamides, oligomers thereof or mixtures thereof, if required with further reaction products, are prepared by reacting aminonitriles or dinitriles and diamines or a mixture containing aminonitrile, dinitrile and diamine, and, if required, further polyamide-forming monomers and/oligomers with water in a reactor ( 1 ) having a vertically oriented longitudinal axis, by a process in which, in the reactor ( 1 ), the reaction product is removed from the bottom and ammonia formed and any further low molecular weight compounds formed and water are taken off via the top ( 2 ), wherein the reactor ( 1 ) has at least two chambers ( 4 ) arranged one on top of the other in the longitudinal direction, the chambers ( 4 ) being separated from one another by liquid-tight trays ( 5 ), each chamber ( 4 ) being connected by a liquid overflow ( 6 ) to the chamber ( 4 ) directly underneath and a liquid product stream being taken off by the liquid overflow ( 6 ) of the lowermost chamber ( 4 ), the gas space ( 7 ) above the liquid level in each chamber ( 4 ) being connected to the chamber ( 4 ) arranged directly above in each case by one or more conduit pipes ( 8 ) which in each case opens or open into a gas distributor ( 9 ) having orifices ( 11 ) for gas exit below the liquid level, and comprising in each case at least one baffle plate ( 12 ) which is arranged vertically around each gas distributor ( 9 ) and whose upper end terminates below the liquid level and whose lower end terminates above the liquid-tight tray ( 5 ) of the chamber ( 4 ) and which separates each chamber ( 4 ) into one or more gassed ( 13 ) and into one or more ungassed ( 14 ) spaces.
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公开(公告)号：AT340819T
公开(公告)日：2006-10-15
申请号：AT04721865
申请日：2004-03-19
Applicant: BASF AG
Inventor： DEININGER JUERGEN , DEMETER JUERGEN , KORY GAD , SOETJE OLIVER , WINTERLING HELMUT , ZEHNER PETER , HEEGER MICHAEL , GANN MARTIN , POLT AXEL , TREULING ULRICH , WEINLE WERNER
Abstract: Polyamides, oligomers thereof or mixtures thereof, if required with further reaction products, are prepared by reacting aminonitriles or dinitriles and diamines or a mixture containing aminonitrile, dinitrile and diamine, and, if required, further polyamide-forming monomers and/oligomers with water in a reactor ( 1 ) having a vertically oriented longitudinal axis, by a process in which, in the reactor ( 1 ), the reaction product is removed from the bottom and ammonia formed and any further low molecular weight compounds formed and water are taken off via the top ( 2 ), wherein the reactor ( 1 ) has at least two chambers ( 4 ) arranged one on top of the other in the longitudinal direction, the chambers ( 4 ) being separated from one another by liquid-tight trays ( 5 ), each chamber ( 4 ) being connected by a liquid overflow ( 6 ) to the chamber ( 4 ) directly underneath and a liquid product stream being taken off by the liquid overflow ( 6 ) of the lowermost chamber ( 4 ), the gas space ( 7 ) above the liquid level in each chamber ( 4 ) being connected to the chamber ( 4 ) arranged directly above in each case by one or more conduit pipes ( 8 ) which in each case opens or open into a gas distributor ( 9 ) having orifices ( 11 ) for gas exit below the liquid level, and comprising in each case at least one baffle plate ( 12 ) which is arranged vertically around each gas distributor ( 9 ) and whose upper end terminates below the liquid level and whose lower end terminates above the liquid-tight tray ( 5 ) of the chamber ( 4 ) and which separates each chamber ( 4 ) into one or more gassed ( 13 ) and into one or more ungassed ( 14 ) spaces.
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公开(公告)号：DE10313682A1
公开(公告)日：2004-10-07
申请号：DE10313682
申请日：2003-03-26
Applicant: BASF AG
Inventor： DEININGER JUERGEN , DEMETER JUERGEN , GRUBER FREDDY , KORY GAD , SOETJE OLIVER , WINTERLING HELMUT
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公开(公告)号：CA2519816A1
公开(公告)日：2004-10-07
申请号：CA2519816
申请日：2004-03-19
Applicant: BASF AG
Inventor： DEMETER JURGEN , DEININGER JURGEN , WINTERLING HELMUT , HEEGER MICHAEL , ZEHNER PETER , GANN MARTIN , KORY GAD , SOTJE OLIVER , POLT AXEL , TREULING ULRICH , WEINLE WERNER
Abstract: The invention relates to a method for producing polyamides, their oligomers or mixtures thereof, optionally containing other reaction products, by reacting aminonitriles or dinitriles and diamines or a mixture containing aminonitril e, dinitrile and diamine and optionally additional polyamide-forming monomers and/or oligomers with water in a reactor (1) with a vertical longitudinal axis. According to said method, the reaction product is exfiltrated from the sump in the reactor (1) and accumulated ammonia and optionally other accumulated low-molecular compounds and water are drawn off via the head (2) . The invention is characterised in that the reactor (1) comprises at least tw o chambers (4) arranged in a longitudinal direction one above the other, that the chambers (4) are separated from one another by liquid-tight floors (5), that each chamber (4) is connected to the one (4) immediately below by a respective liquid overflow (6) and a liquid product stream is drawn off via the liquid overflow (6) of the lowest chamber (4), that the gas chamber (7) above the liquid level in each chamber (4) is connected to the respective chamber (4) lying immediately above it via one or several conduits (8), whic h open respectively into a gas diffuser (9) comprising orifices (11) for the discharge of gas below the liquid level. The reactor also comprises at least one respective deflector plate (12) positioned vertically around each gas diffuser (9), the upper end of said plate terminating below the liquid level and the lower end terminating above the liquid-tight floor (5) of the chambe r (4), thus sub-dividing each chamber (4) into one or more compartments suppli ed with gas (13) and one or more compartments without gas (14).
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公开(公告)号：MY139354A
公开(公告)日：2009-09-30
申请号：MYPI20040965
申请日：2004-03-18
Applicant: BASF AG
Inventor： DEININGER JURGEN , TREULING ULRICH DR , WEINLE WERNER , DEMETER JUERGEN DR , KORY GAD , SOETJE OLIVER , WINTERLING HELMUT DR , ZEHNER PETER DR , HEEGER MICHAEL , GANN MARTIN , POLT AXEL DR
Abstract: POLYAMIDES, OLIGOMERS THEREOF OR MIXTURES THEREOF, IF REQUIRED WITH FURTHER REACTION PRODUCTS, ARE PREPARED BY REACTING AMINONITRILES OR DINITRILES AND DIAMINES OR A MIXTURE CONTAINING AMINONITRILE, DINITRILE AND DIAMINE, AND, IF REQUIRED, FURTHER POLYAMIDE-FORMING MONOMERS AND/OLIGOMERS WITH WATER IN A REACTOR (1) HAVING A VERTICALLY ORIENTED LONGITUDINAL AXIS, BY A PROCESS IN WHICH, IN THE REACTOR (1), THE REACTION PRODUCT IS REMOVED FROM THE BOTTOM AND AMMONIA FORMED AND ANY FURTHER LOW MOLECULAR WEIGHT COMPOUNDS FORMED AND WATER ARE TAKEN OFF VIA THE TOP (2), WHEREIN THE REACTOR (1) -HAS AT LEAST TWO CHAMBERS (4) ARRANGED ONE ON TOP OF THE OTHER IN THE LONGITUDINAL DIRECTION, -THE CHAMBERS (4) BEING SEPARATED FROM ONE ANOTHER BY LIQUID-TIGHT TRAYS (5),-EACH CHAMBER (4) BEING CONNECTED BY A LIQUID OVERFLOW (6) TO THE CHAMBER (4) DIRECTLY UNDERNEAT,H AND A LIQUID PRODUCT STREAM BEING TAKEN OFF BY THE LIQUID OVERFLOW (6) OF THE LOWERMOST CHAMBER (4), -THE GAS SPACE (7) ABOVE THE LIQUID LEVEL IN EACH CHAMBER (4) BEING CONNECTED TO THE CHAMBER (4) ARRANGED DIRECTLY ABOVE IN EACH CASE BY ONE OR MORE CONDUIT PIPES (8) WHICH IN EACH CASE OPENS OR OPEN INTO A GAS DISTRIBUTOR (9) HAVING ORIFICES (11) FOR GAS EXIT BELOW THE LIQUID LEVEL, -AND COMPRISING IN EACH CASE AT LEAST ONE BAFFLE PLATE (12) WHICH IS ARRANGED VERTICALLY AROUND EACH GAS DISTRIBUTOR (9) AND WHOSE UPPER END TERMINATES BELOW THE LIQUID LEVEL AND WHOSE LOWER END TERMINATES ABOVE THE LIQUID-TIGHT TRAY (5) OF THE CHAMBER (4) AND WHICH SEPARATES EACH CHAMBER (4) INTO ONE OR MORE GASSED (13) AND INTO ONE OR MORE UNGASSED (14) SPACES.
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