DYNAMIC CALIBRATION METHOD FOR ECHELLE SPECTROMETER IN LASER-INDUCED BREAKDOWN SPECTROSCOPY

    公开(公告)号:US20190003887A1

    公开(公告)日:2019-01-03

    申请号:US15771338

    申请日:2017-04-24

    Abstract: The present invention belongs to the technical field of elemental analysis, and more particularly, relates to a dynamic calibration method for echelle spectrometer in laser-induced breakdown spectroscopy, comprising: S1: collecting a standard light source by using an echelle spectrometer; S2: in combination with a calibration function, calculating a pixel position coordinate ({circumflex over (x)}, ŷ) corresponding to a spectral wavelength ŵ; S3: performing dynamic searching and filtering near the pixel position coordinate ({circumflex over (x)}, ŷ) to obtain a set D of all pixel position coordinates, and adjusting all original intensity values in the set D to obtain intensity values F(Ix,y), and S4: calculating a spectral line intensity value after dynamic calibration by summing the adjusted intensity values F(Ix,y), thereby completing dynamic calibration of the result of the echelle spectrometer. The method in the present invention can overcome the shortcoming, i.e., the existing echelle spectrometer is only calibrated before measurement without solving the spectral line drift during use, increasing the absolute intensity of the wavelength and reducing the detection limit of the quantitative analysis, as well as improving the precision of the quantitative analysis of an element to be analyzed.

    PLASMA PROCESSING APPARATUS AND CONTROL METHOD

    公开(公告)号:US20180301388A1

    公开(公告)日:2018-10-18

    申请号:US15947994

    申请日:2018-04-09

    Abstract: Provided is a plasma processing apparatus including a microwave radiating mechanism configured to radiate microwaves output from a microwave output unit into a processing container. The microwave radiating mechanism includes: an antenna configured to radiate the microwaves; a dielectric member configured to transmit the microwaves radiated from the antenna, and form an electric field for generating surface wave plasma by the microwaves; a sensor provided in the microwave radiating mechanism or adjacent to the microwave radiating mechanism, and configured to monitor electron temperature of the generated plasma; and a controller configured to determine a plasma ignition state based on the electron temperature of the plasma monitored by the sensor.

    CHAMBERS FOR MICROWAVE PLASMA GENERATION
    65.
    发明申请

    公开(公告)号:US20180228012A1

    公开(公告)日:2018-08-09

    申请号:US15749430

    申请日:2016-07-20

    CPC classification number: H05H1/30 G01J3/443 H01J49/105 H05H1/46 H05H2001/4622

    Abstract: A microwave chamber for plasma generation. The microwave chamber comprises a launch structure at a first end of the microwave chamber to accommodate a microwave source for producing microwave energy and a termination section at a second end of the microwave chamber opposite the first end. The termination section is configured to substantially block propagation of the microwave energy from the second end of the chamber. The microwave chamber further comprises an internal wall structure for guiding the microwave energy received within the microwave chamber at the first end toward the second end and defines a cavity. The internal wall structure comprises an impedance matching section intermediate the first end and the second end, and a capacitive loaded section intermediate the impedance matching section and the second end, wherein the capacitive loaded section comprises at least one ridge extending along a longitudinal axis of the chamber. The microwave chamber defines a first opening extending through a first wall of the capacitive loaded section and a second opening extending through a second wall of the capacitive loaded section. The second wall is opposite the first wall. The first opening and second opening are configured to cooperate with one another to receive a plasma torch in the capacitive loaded section along an axis extending through first opening and second opening and substantially perpendicular to the longitudinal axis of the chamber.

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