Glass preform manufacturing method
    75.
    发明授权
    Glass preform manufacturing method 有权
    玻璃预制件制造方法

    公开(公告)号:US08844323B2

    公开(公告)日:2014-09-30

    申请号:US13233654

    申请日:2011-09-15

    CPC classification number: C03B37/01807 C03B2201/50 C03B2201/54

    Abstract: A glass preform manufacturing method, includes: preparing a glass element having a rough surface; turning a raw material of an alkali metal compound or a raw material of an alkaline earth metal compound into particles; depositing particles of the alkali metal compound or the alkaline earth metal compound on the rough surface of the glass element; oxidizing the particles of the alkali metal compound or the alkaline earth metal compound while diffusing alkali metal oxide or alkaline earth metal oxide in the glass element; and manufacturing a glass preform into which the alkali metal oxide or the alkaline earth metal oxide is doped.

    Abstract translation: 玻璃预制件的制造方法,包括:准备具有粗糙面的玻璃元件; 将碱金属化合物的原料或碱土金属化合物的原料转化成颗粒; 在玻璃元件的粗糙表面上沉积碱金属化合物或碱土金属化合物的颗粒; 在玻璃元件中扩散碱金属氧化物或碱土金属氧化物的同时氧化碱金属化合物或碱土金属化合物的颗粒; 并制造掺杂有碱金属氧化物或碱土金属氧化物的玻璃预成型体。

    Powdered silica, silica container, and method for producing them
    76.
    发明授权
    Powdered silica, silica container, and method for producing them 失效
    粉状二氧化硅,二氧化硅容器及其制造方法

    公开(公告)号:US08460769B2

    公开(公告)日:2013-06-11

    申请号:US13140982

    申请日:2010-09-01

    Abstract: A method is provided for producing a silica container arranged with a substrate, having a rotational symmetry, comprised of mainly a silica, and containing gaseous bubbles at least in its peripheral part, and an inner layer, formed on an inner surface of the substrate and comprised of a transparent silica glass; wherein a powdered silica, having particle diameter of 10 to 1000 μm, containing Ca, Sr, and Ba with the total concentration of 50 to 5000 ppm by weight, and releasing hydrogen molecules with the amount of 3×1016 to 3×1019 molecules/g upon heating at 1000° C. under vacuum, is prepared at least as a powdered raw material for forming the inner layer, and then the inner layer is formed from the powdered silica as the powdered raw material for forming the inner layer.

    Abstract translation: 提供一种制造二氧化硅容器的方法,该二氧化硅容器具有旋转对称性,主要由二氧化硅构成的基板,至少在其周边部分含有气泡,内层形成在基板的内表面上, 由透明石英玻璃组成; 其中,粉末状二氧化硅的粒径为10〜1000μm,含有总量为50〜5000重量ppm的Ca,Sr,Ba,释放量为3×1016〜3×1019分子/ 至少作为形成内层的粉末状原料制备,然后内层由作为形成内层的粉末状原料的二氧化硅粉末形成。

    METHOD FOR FABRICATING RARE EARTH (RE) DOPED OPTICAL FIBER USING A NEW CODOPANT
    77.
    发明申请
    METHOD FOR FABRICATING RARE EARTH (RE) DOPED OPTICAL FIBER USING A NEW CODOPANT 有权
    使用新的CODOPANT制造稀土(RE)掺杂光纤的方法

    公开(公告)号:US20120201504A1

    公开(公告)日:2012-08-09

    申请号:US13260415

    申请日:2010-03-29

    Abstract: The present invention provides a method of making rare earth (RE) doped optical fiber using BaO as co-dopant instead of Al or P commonly used for incorporation of the RE in silica glass by MCVD and solution doping technique. The method comprises deposition of particulate layer of GeO2 doped SiO2 with or without small P2O5 for formation of the core and solution doping by soaking the porous soot layer into an aqueous solution of RE and Ba containing salt. This is followed by dehydration and sintering of the soaked deposit, collapsing at a high temperature to produce the preform and drawing of fibers of appropriate dimension. The use of Ba-oxide enables to eliminate unwanted core-clad interface defect which is common in case of Al doped fibers. The fibers also show good RE uniformity, relatively low optical loss in the 0.6-1.6 μm wavelength region and good optical properties suitable for their application in amplifiers, fiber lasers and sensor devices.

    Abstract translation: 本发明提供一种使用BaO作为共掺杂剂代替通常用于通过MCVD和溶液掺杂技术将石英玻璃中的RE掺入的Al或P的掺杂稀土(RE)掺杂光纤的方法。 该方法包括沉积具有或不具有小的P 2 O 5的GeO 2掺杂的SiO 2的颗粒层以形成芯并通过将多孔烟灰层浸入含RE和Ba的盐的水溶液中来进行溶液掺杂。 随后将浸渍的沉积物脱水和烧结,在高温下塌陷以制备预制件并拉出适当尺寸的纤维。 使用Ba氧化物能够消除在Al掺杂光纤的情况下常见的不需要的芯包层界面缺陷。 纤维也表现出良好的均匀性,0.6-1.6μm波长区域的光损耗相对较低,适用于放大器,光纤激光器和传感器装置的光学性能良好。

    APPARATUS AND METHOD FOR MANUFACTURING GLASS PREFORM
    78.
    发明申请
    APPARATUS AND METHOD FOR MANUFACTURING GLASS PREFORM 审中-公开
    用于制造玻璃预制件的装置和方法

    公开(公告)号:US20110314874A1

    公开(公告)日:2011-12-29

    申请号:US13165236

    申请日:2011-06-21

    Abstract: An apparatus for manufacturing a glass perform, includes: a dummy tube section, a reservoir portion, and a cooling portion; and a glass tube section in which particles of an alkali metal compound or an alkaline earth metal compound which have flowed into the glass tube section from the dummy tube section are heated by a second heat source which performs traverse, and oxides of the particles being deposited on an inner wall and dispersed in the glass tube section. In the cooling portion of the dummy tube section, vapor of the alkali metal compound or the alkaline earth metal compound generated by heating of a first heat source is cooled and condensed by a dry gas flowing into the dummy tube section, and thereby the particles are generated.

    Abstract translation: 一种玻璃制造装置,包括:虚拟管部,储存部和冷却部; 以及玻璃管部分,其中由虚拟管部分流入玻璃管部分的碱金属化合物或碱土金属化合物的颗粒被进行横越的第二热源加热,并且沉积的颗粒的氧化物 在内壁上分散在玻璃管部分。 在虚拟管部的冷却部中,通过第一热源的加热而产生的碱金属化合物或碱土金属化合物的蒸气被流入虚拟管部的干燥气体冷却并冷凝, 生成。

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