Method for producing a chromatography analysis column

    公开(公告)号:US09835599B2

    公开(公告)日:2017-12-05

    申请号:US14414848

    申请日:2013-07-02

    Abstract: The invention concerns a method for producing a chromatography analysis column, the resulting column, and a device comprising such a column. The method according to the invention comprises the following steps: (a) depositing on the flat surface of a substrate a first layer of particles which are intended to form the stationary phase; (b) depositing on the layer at least one second layer of compactly assembled particles; (c) impregnating the first and second layers with a light radiation-sensitive material, to form at least two compactly assembled particle layers impregnated with sensitive material; (d) insolating these layers in the regions corresponding to the desired internal shape of the chromatography analysis column, if the light radiation-sensitive material behaves like a positive resin, or outlining this internal shape if the light radiation-sensitive material behaves like a negative photosensitive resin; (e) eliminating either the regions insolated in step (d) if the light radiation-sensitive layer behaves like a positive photosensitive resin, or the regions not insolated in step (d) if the light radiation-sensitive material behaves like a negative photosensitive resin; and (f) covering and sealing the structure obtained in step (e) with a cover covered on the face facing the layers with at least one layer of compactly assembled particles which are identical to or different from those deposited on the substrate surface. The invention is used in particular in the field of chemical analysis.

    Method And Apparatus For Characterising A Diffracting Surface
    3.
    发明申请
    Method And Apparatus For Characterising A Diffracting Surface 审中-公开
    用于表征衍射面的方法和装置

    公开(公告)号:US20160011119A1

    公开(公告)日:2016-01-14

    申请号:US14770981

    申请日:2014-02-26

    Abstract: A method for characterizing a diffracting surface having a structure made of crystalline grain is provided. The method includes the steps of: a) sequentially illuminating the surface with a plurality of light beams (Fi) having propagation directions that are angled at a same angle Θ relative to the normal of the surface and the projections, onto the surface, of which form different azimuth angles ψi relative to a reference direction; b) acquiring an image of the surface corresponding to each of the light beams; and c) digitally processing the images such as to obtain information on at least one property of the surface selected among: the grain structure, the texture and the sequencing rate thereof. The invention also relates to an optical head and to an apparatus for implementing such a method.

    Abstract translation: 提供了一种用于表征具有由晶粒构成的结构的衍射表面的方法。 该方法包括以下步骤:a)使用多个光束(Fi)顺序地照射表面,该多个光束(Fi)具有相对于表面法线和突起以相同角度θ成角度的传播方向到其表面上 形成相对于参考方向的不同方位角ψi; b)获取与每个光束相对应的表面的图像; 以及c)数字处理所述图像,以获得关于所述表面的至少一个性质的信息:所述纹理结构,纹理和排序速率。 本发明还涉及一种光学头和用于实现这种方法的装置。

    FORMATION OF BORON CARBIDE NANOPARTICLES FROM A BORON ALKOXIDE AND A POLYVINYL ALCOHOL

    公开(公告)号:US20180065857A1

    公开(公告)日:2018-03-08

    申请号:US15692870

    申请日:2017-08-31

    CPC classification number: C01B32/991 B01J13/0065 C01P2004/64 G21F1/06

    Abstract: The present invention relates to a process for the preparation of boron carbide nanoparticles, characterized in that it comprises at least the stages consisting in: (i) interacting boric acid, boron oxide B2O3 or a boric acid ester of B(OR)3 type, with R, which are identical or different, representing C1-4-alkyl groups, with 1 to 2 molar equivalents of at least one C2 to C4 polyol, under conditions favorable to the formation of a boron alkoxide powder; (ii) interacting, in an aqueous medium, the boron alkoxide powder obtained on conclusion of stage (i) with an effective amount of one or more completely hydrolyzed polyvinyl alcohols, with a molar mass of between 10 000 and 80 000 g.mol−1, under conditions favorable to the formation of a crosslinked PVA gel, and (iii) carrying out an oxidizing pyrolysis of the crosslinked gel formed on conclusion of the preceding stage (ii), under conditions favorable to the formation of the CB4 nanoparticles.

    Method for Producing a Chromatography Analysis Column
    6.
    发明申请
    Method for Producing a Chromatography Analysis Column 有权
    色谱分析柱的制备方法

    公开(公告)号:US20150219605A1

    公开(公告)日:2015-08-06

    申请号:US14414848

    申请日:2013-07-02

    Abstract: The invention concerns a method for producing a chromatography analysis column, the resulting column, and a device comprising such a column. The method according to the invention comprises the following steps: (a) depositing on the flat surface of a substrate a first layer of particles which are intended to form the stationary phase; (b) depositing on the layer at least one second layer of compactly assembled particles; (c) impregnating the first and second layers with a light radiation-sensitive material, to form at least two compactly assembled particle layers impregnated with sensitive material; (d) insolating these layers in the regions corresponding to the desired internal shape of the chromatography analysis column, if the light radiation-sensitive material behaves like a positive resin, or outlining this internal shape if the light radiation-sensitive material behaves like a negative photosensitive resin; (e) eliminating either the regions insolated in step (d) if the light radiation-sensitive layer behaves like a positive photosensitive resin, or the regions not insolated in step (d) if the light radiation-sensitive material behaves like a negative photosensitive resin; and (f) covering and sealing the structure obtained in step (e) with a cover covered on the face facing the layers with at least one layer of compactly assembled particles which are identical to or different from those deposited on the substrate surface. The invention is used in particular in the field of chemical analysis.

    Abstract translation: 本发明涉及一种用于生产色谱分析柱,所得到的柱和包括这种柱的装置的方法。 根据本发明的方法包括以下步骤:(a)在基板的平坦表面上沉积旨在形成固定相的第一层颗粒; (b)在所述层上沉积至少一个紧密组装的颗粒的第二层; (c)用光辐射敏感材料浸渍第一层和第二层,以形成浸渍有敏感材料的至少两个紧密组装的颗粒层; (d)在对应于色谱分析柱的所需内部形状的区域中使这些层分离,如果光辐射敏感材料表现得像正性树脂,或者如果光辐射敏感材料表现得像负片 光敏树脂; (e)如果光辐射敏感层的表现像正性感光树脂,或步骤(d)中未被蚀刻的区域,如果光敏材料表现为负型感光性树脂,则消除步骤(d) ; 和(f)用面对面层的表面覆盖和密封步骤(e)中获得的结构,其中至少一层紧密组装的颗粒与沉积在基材表面上的颗粒相同或不同。 本发明特别用于化学分析领域。

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