95.
    发明专利
    未知

    公开(公告)号:AT343561T

    公开(公告)日:2006-11-15

    申请号:AT03794858

    申请日:2003-08-08

    Applicant: BASF AG

    Abstract: Recovery of isophoronediamine (IPDA) comprises preparation of IPDA having a cis/trans isomer ratio of less than 73/27 and separation into at least 5 fractions by distillation including an IPDA fraction having a cis/trans ratio of greater than 73/27 and a fraction having a cis/trans ratio of less than 66/34. A process for the recovery of 3-aminomethyl-3,5,5-trimethylcyclohexylamine (isophoronediamine, IPDA) comprises; (a) preparation of IPDA having a cis/trans isomer ratio of less than 73/27; (b) introduction of IPDA to the middle region of a distillation column having inserts and distillation of IPDA at 5-300 degreesC and 10-2000 mbar; (c) optionally further purification of the IPDA from (b) by distillation in at least one further column whereby the IPDA from step (b) and (c) are separated into at least 5 fractions comprising an organic fraction (1a) containing impurities having a lower b. pt. than trans-IPDA, an aqueous fraction (1b) containing impurities having a lower b. pt. than trans-IPDA, a fraction (2) containing impurities having a higher b. pt. than cis-IPDA, an IPDA fraction (3) having a cis/trans ratio of greater than 73/27 and an IPDA fraction (4) having a cis/trans ratio of less than 66/34.

    99.
    发明专利
    未知

    公开(公告)号:DE59810556D1

    公开(公告)日:2004-02-12

    申请号:DE59810556

    申请日:1998-06-05

    Applicant: BASF AG

    Abstract: A process for regenerating a zeolite catalyst comprises the following stages: (I) Heating a partially or completely deactivated catalyst to 250-600° C. in an atmosphere which contains less than 2% by volume of oxygen, (II) treating the catalyst at from 250 to 800° C., preferably from 350 to 600° C., with a gas stream which contains from 0.1 to 4% by volume of an oxygen-donating substance or of oxygen or of a mixture of two or more thereof, and (III) treating the catalyst at from 250 to 800° C., preferably from 350 to 600° C., with a gas stream which contains from more than 4 to 100% by volume of an oxygen-donating substance or of oxygen or of a mixture of two or more thereof.

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