公开(公告)号：DE10100943A1

公开(公告)日：2002-07-11

申请号：DE10100943

申请日：2001-01-10

Applicant: BASF AG

Inventor： LANG ORTMUND ,  RUMPF BERND ,  FRAUENKRON MATTHIAS ,  FUNHOFF DIRK ,  MANDERBACH THOMAS ,  STEIN BERND

IPC: C07D487/08

Abstract: A process for the production of a solution of pure triethylenediamine (TEDA) comprises evaporation of TEDA from a mixture comprising a solvent or a diluent, whereby the solvent or diluent has a boiling point of 175-250 deg C at normal pressure, and the TEDA vapor is fed into a liquid solvent.

公开(公告)号：DE10057899A1

公开(公告)日：2002-05-23

申请号：DE10057899

申请日：2000-11-22

Applicant: BASF AG

Inventor： FRAUENKRON MATTHIAS ,  MELDER JOHANN-PETER ,  HAAKE MATHIAS ,  HUBER SYLVIA ,  SCHWAB EKKEHARD ,  NOUWEN JAN

IPC: B01J27/16 ,  B01J27/185 ,  B01J35/04 ,  B01J35/06 ,  B01J37/02 ,  C07C209/60 ,  C07C211/14

Abstract: Production of acyclic polyalkylene polyamines by reacting diamines with ammonia and monoalkanolamines comprises using a thin-film catalyst prepared by coating a metal, plastics or carbon fiber support with a phosphorus compound. Independent claims are also included for the following: (1) Process for producing a phosphorus-containing thin-film catalyst, involves: (i) depositing a phosphorus compound on a metal, plastics or carbon fiber support; and (ii) drying and/or heat treating the product; (2) Catalyst produced by the process of (1).

公开(公告)号：DE502004004156D1

公开(公告)日：2007-08-02

申请号：DE502004004156

申请日：2004-10-02

Applicant: BASF AG

Inventor： REIF WOLFGANG ,  HAMMER HANS ,  RUIDER GUENTHER ,  MEIER ANTON ,  BUSKENS PHILIPP ,  FRAUENKRON MATTHIAS

IPC: C07C213/10 ,  C07C215/12

Abstract: Process for separating triethanolamine continuously by distillation from a mixture of monoethanolamine, diethanolamine and triethanolamine together with ethanolamine ethers and water obtained by reaction of ammonia with ethylene oxide in the liquid phase under superatmospheric pressure and at elevated temperature, in which the mixture is distilled in two stages. The low-boiling fraction and the high-boiling fraction are taken off and discharged in the first stage and the intermediate-boiling fraction comprising >99.4% by weight of triethanolamine and

公开(公告)号：DE102005038376A1

公开(公告)日：2007-02-15

申请号：DE102005038376

申请日：2005-08-13

Applicant: BASF AG

Inventor： JOEDECKE MICHAEL ,  LANG ORTMUND ,  CAUWENBERGE GUNTHER VAN ,  FRAUENKRON MATTHIAS

IPC: C07D295/023 ,  B01D3/14 ,  C07C211/10

Abstract: Continuous distillative separation of piperazine from ethylenediamine-piperazine mixture comprises subjecting the piperazine mixture into a cyclic motion, introducing the piperazine mixture into an evaporator unit at 160-170[deg]C, recycling the piperazine mixture into a distillation column and removing the piperazine from the sump of the distillation column after a retention time of approximately 30-60 minutes, where the ethylene diamine is discharged at the upper portion of the distillation column.

公开(公告)号：MXPA06003484A

公开(公告)日：2006-06-08

申请号：MXPA06003484

申请日：2004-10-02

Applicant: BASF AG

Inventor： FRAUENKRON MATTHIAS

IPC: C07C213/10 ,  C07C215/12

Abstract: Se da a conocer un proceso para separar continuamente la trietanolamina, por la destilacion de una mezcla de la monoetanolamina, dietanolamina y trietanolamina, junto con los eteres de la etanolamina y el agua obtenida por la reaccion del amoniaco con el oxido de etileno en la fase liquida, bajo una presion sobreatmosferica y a temperatura elevada, en la cual la mezcla se destila en dos etapas. la fraccion de punto de ebullicion bajo y la fraccion de punto de ebullicion alta se sacan y descargan en la primera etapa y la fraccion con punto de ebullicion intermedio comprende mas del 99.4% en peso de la trietanolamina y menos del 0.2% en peso de la dietanolamina, se destila en la segunda etapa. La destilacion de la mezcla se lleva a cabo preferiblemente en una primera columna y una segunda columna, conectada a la primera columna, en una columna de pared de division.

公开(公告)号：DE102004029544A1

公开(公告)日：2006-01-05

申请号：DE102004029544

申请日：2004-06-18

Applicant: BASF AG

Inventor： BOSCH MARCO ,  FRAUENKRON MATTHIAS ,  KOSTUR MILAN ,  HOFSTADT OTTO

IPC: B01J29/00 ,  B01J29/06 ,  B01J29/40 ,  B01J35/00 ,  B01J35/02 ,  B01J37/00 ,  B01J37/08 ,  C01B39/00 ,  C07D487/08

公开(公告)号：DE102004024274A1

公开(公告)日：2005-12-01

申请号：DE102004024274

申请日：2004-05-15

Applicant: BASF AG

Inventor： LANG ORTMUND ,  FRAUENKRON MATTHIAS

IPC: C07D487/08

Abstract: Process for preparing a solution of pure triethylenediamine (TEDA), in which TEDA is vaporized, the gaseous TEDA is passed into a liquid solvent 1 (quench) and the TEDA is crystallized from the resulting solution and separated off (solid-liquid separation), wherein the crystalline TEDA obtained is dissolved in a solvent 2 and a stripping gas is passed through the resulting solution (stripping).

公开(公告)号：DE10359811A1

公开(公告)日：2005-07-21

申请号：DE10359811

申请日：2003-12-19

Applicant: BASF AG

Inventor： EVERS HOLGER ,  MELDER JOHANN-PETER ,  BENISCH CHRISTOPH ,  FRAUENKRON MATTHIAS ,  GERLACH TILL ,  ALBA PEREZ ANA ,  NOUWEN JAN

IPC: C07C209/64 ,  C07C211/14 ,  C07C209/26 ,  B01J23/70 ,  C07C211/11

公开(公告)号：DE10356184A1

公开(公告)日：2005-07-07

申请号：DE10356184

申请日：2003-12-02

Applicant: BASF AG

Inventor： BOSCH MARCO ,  MUELLER ULRICH ,  FRAUENKRON MATTHIAS

IPC: B01J29/40 ,  B01J35/02 ,  B01J37/00 ,  B01J37/10 ,  C01B39/36 ,  C01B39/40 ,  C07D487/08 ,  C01B39/38 ,  C04B38/06

Abstract: Zeolite material of the pentasil type has an alkali metal and alkaline earth metal content of not more than 100 ppm and a molar ratio of Si to Al of from 250 to 1500, at least 90% of the primary particles of the zeolite material being spherical and 95% by weight of the spherical primary particles having a diameter of less than or equal to 1 μm.

公开(公告)号：DE10346779A1

公开(公告)日：2005-05-12

申请号：DE10346779

申请日：2003-10-08

Applicant: BASF AG

Inventor： REIF WOLFGANG ,  HAMMER HANS ,  RUIDER GUENTHER ,  MEIER ANTON ,  BUSKENS PHILIP ,  FRAUENKRON MATTHIAS

IPC: C07C213/10 ,  C07C215/12

Abstract: Process for separating triethanolamine continuously by distillation from a mixture of monoethanolamine, diethanolamine and triethanolamine together with ethanolamine ethers and water obtained by reaction of ammonia with ethylene oxide in the liquid phase under superatmospheric pressure and at elevated temperature, in which the mixture is distilled in two stages. The low-boiling fraction and the high-boiling fraction are taken off and discharged in the first stage and the intermediate-boiling fraction comprising >99.4% by weight of triethanolamine and