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    Photoreactor for photochemical syntheses
    41.
    发明专利
    Photoreactor for photochemical syntheses 未知

    公开(公告)号：DE3625006A1

    公开(公告)日：1987-04-30

    申请号：DE3625006

    申请日：1986-07-24

    Applicant: BASF AG

    Inventor： TRAUTMANN WALTER DR ,  HLAWITSCHKA WERNER ,  HENNE ANDREAS DR ,  WEBER WILHELM DR

    IPC: B01J19/12 ,  B01J19/08

    Abstract: Photoreactor for photochemical syntheses, comprising, concentrically arranged from the inside to the outside, a lamp (4) with the electrical connections, an annular lamp cooler (5) made of glass with connections for a cooling medium flowing in and out and a reaction space (6) delimited by the outer casing of the lamp cooler and by the inner casing of the reactor (1) having a metal-coated interior wall, an apparatus (7) equipped with brushes or wipers (8) rotating in the reaction space, which apparatus is arranged so that on operation of the photoreactor, the outer casing of the lamp cooler is kept free from a light-absorbing deposit.

    Process for the preparation of diarylalkoxyphosphines
    44.
    发明专利
    Process for the preparation of diarylalkoxyphosphines 未知

    公开(公告)号：DE3521770A1

    公开(公告)日：1986-01-09

    申请号：DE3521770

    申请日：1985-06-19

    Applicant: BASF AG

    Inventor： HENNE ANDREAS DR

    IPC: C07F9/46

    Abstract: Preparation of diarylalkoxyphosphines Ar2P-O-R (I; Ar = optionally substituted phenyl; R = C1-C4-alkyl) from dihaloalkoxyphosphines of the formula Hal2P-O-R (II; Hal = Cl, Br) and arylmagnesium halides Ar-Mg-Hal (III) in the form of a solution in ether, by allowing II and III to react with each other in such a manner that II is not present in stoichiometric excess.

    48.
    发明专利
    未知

    公开(公告)号：AT233747T

    公开(公告)日：2003-03-15

    申请号：AT99125083

    申请日：1999-12-16

    Applicant: BASF AG

    Inventor： RIECHERS HARTMUT DR ,  SIMON JOACHIM DR ,  HENNE ANDREAS DR ,  HOEHN ARTHUR DR

    IPC: C07D295/08 ,  B01J23/72 ,  C07D295/088

    Abstract: 2,2'-Dimorpholinodiethyl ether is produced by reacting diethylene glycol with ammonia under pressure at elevated temperature in the presence of hydrogen. The active hydrogenation catalyst, before reduction with hydrogen, contains 20-85 wt.% alumina, zirconium dioxide, titanium dioxide and/or silica, 1-70 wt.% copper oxide (CuO), less than 20 wt.% nickel oxide with respect to CuO and 0-50 wt.% other metal oxide(s). In the production of 2,2'-dimorpholinodiethyl ether (DMDEE) by reacting diethylene glycol with ammonia under pressure at elevated temperature in the presence of hydrogen and a hydrogenation catalyst, the active catalyst, before reduction with hydrogen, contains 20-85 wt.% aluminum oxide (Al2O3), zirconium dioxide (ZrO2), titanium dioxide (TiO2) and/or silica (SiO2), 1-70 wt.% copper oxide (expressed as CuO), 0-50 wt.% magnesium, chromium, zinc, barium and/or calcium oxide (expressed as MgO, Cr2O3, ZnO, BaO and CaO) and less than 20 wt.% nickel oxide (expressed as NiO) with respect to CuO.

    50.
    发明专利
    未知

    公开(公告)号：ES2131732T3

    公开(公告)日：1999-08-01

    申请号：ES95112481

    申请日：1995-08-09

    Applicant: BASF AG

    Inventor： BECKER RAINER DR ,  MENGER VOLKMAR DR ,  REIF WOLFGANG DR ,  HENNE ANDREAS DR

    IPC: B01J23/88 ,  B01J21/06 ,  B01J23/755 ,  B01J37/03 ,  C07B61/00 ,  C07C209/16 ,  C07C211/09

    Abstract: Prepn. of a diamine (I) involves reacting an aminoalcohol (II) with ammonia or a prim. or sec. amine and hydrogen at 1-400 bars and 80-250 degrees C in presence of a catalyst (A) contg. the following oxygen-contg. metal cpds. in amts. (by wt.) 20-85% Zr cpd. (calculated as ZrO2), 1-30% Cu cpd. (calculated as CuO), 30-70% Ni cpd. (calculated as NiO), 0.1-5% cpd. of molybdenum (calculated as MoO3) and 0-10% cpds. of aluminium and/or manganese (calculated as Al2O3 or MnO2). Pref. (I) is NR R -Y-NR R , (II) is HO-Y-NR R and (III) is NHR R . R , R = 1-20C alkyl, 3-12C cycloalkyl, aryl, 7-20C aralkyl or 7-20C alkaryl; or R +R = (CH2)m-X-(CH2)n; R , R = H or as R , R ; X = O, CH2 or NR ; R = 1-20C alkyl, 3-12C cycloalkyl, aryl, 7-20C aralkyl or 7-20C alkaryl; Y = 2-12C alkylene chain, opt. substd. by 1-5 1-4C alkyl.

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