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    PROCESS FOR PREPARING ALIPHATIC ALPHA,OMEGA-AMINONITRILES
    73.
    发明专利
    PROCESS FOR PREPARING ALIPHATIC ALPHA,OMEGA-AMINONITRILES 未知

    公开(公告)号：GR3033456T3

    公开(公告)日：2000-09-29

    申请号：GR20000401145

    申请日：2000-05-19

    Applicant: BASF AG

    Inventor： MELDER JOHANN-PETER ,  SCHNURR WERNER ,  FLICK KLEMENS ,  EBEL KLAUS ,  WITZEL TOM ,  FISCHER ROLF ,  HARDER WOLFGANG ,  REHFINGER ALWIN

    IPC: B01J23/76 ,  B01J23/889 ,  B01J23/89 ,  B01J27/18 ,  B01J37/02 ,  C07B61/00 ,  C07C253/30 ,  C07C255/24

    Abstract: Aliphatic alpha,omega-aminonitriles are prepared by partial hydrogenation of aliphatic alpha,omega-dinitriles at elevated temperatures and superatmospheric pressure in the presence of a solvent and of a catalyst by a process which comprises using a catalyst which (a) contains a compound based on a metal selected from the group consisting of nickel, cobalt, iron, ruthenium and rhodium and (b) contains from 0.01 to 25% by weight, based on (a), of a promoter based on a metal selected from the group consisting of palladium, platinum, iridium, osmium, copper, silver, gold, chromium, molybdenum, tungsten, manganese, rhenium, zinc, cadmium, lead, aluminum, tin, phosphorus, arsenic, antimony, bismuth and rare earth metals and (c) from 0 to 5% by weight, based on (a), of a compound based on an alkali metal or on an alkaline earth metal. with the proviso that the component (a) is not based on iron or iron and one of the metals selected from the group consisting of cobalt, ruthenium and rhodium when (b) is a promoter based on a metal selected from the group consisting of titanium, manganese, chromium and molybdenum, and with the further proviso that, when a compound based on only ruthenium or rhodium or ruthenium and rhodium or nickel and rhodium is selected as component (a), the promoter (b) may be dispensed with.

    74.
    发明专利
    未知

    公开(公告)号：PT800508E

    公开(公告)日：2000-07-31

    申请号：PT95941718

    申请日：1995-12-16

    Applicant: BASF AG

    Inventor： EBEL KLAUS ,  TOM WITZEL DR ,  SCHNURR WERNER ,  FISCHER ROLF ,  HARDER WOLFGANG ,  MELDER JOHANN-PETER ,  FLICK KLEMENS ,  REHFINGER ALWIN

    IPC: B01J23/76 ,  B01J23/889 ,  B01J23/89 ,  B01J27/18 ,  B01J37/02 ,  C07B61/00 ,  C07C253/30 ,  C07C255/24

    Abstract: Aliphatic alpha,omega-aminonitriles are prepared by partial hydrogenation of aliphatic alpha,omega-dinitriles at elevated temperatures and superatmospheric pressure in the presence of a solvent and of a catalyst by a process which comprises using a catalyst which (a) contains a compound based on a metal selected from the group consisting of nickel, cobalt, iron, ruthenium and rhodium and (b) contains from 0.01 to 25% by weight, based on (a), of a promoter based on a metal selected from the group consisting of palladium, platinum, iridium, osmium, copper, silver, gold, chromium, molybdenum, tungsten, manganese, rhenium, zinc, cadmium, lead, aluminum, tin, phosphorus, arsenic, antimony, bismuth and rare earth metals and (c) from 0 to 5% by weight, based on (a), of a compound based on an alkali metal or on an alkaline earth metal. with the proviso that the component (a) is not based on iron or iron and one of the metals selected from the group consisting of cobalt, ruthenium and rhodium when (b) is a promoter based on a metal selected from the group consisting of titanium, manganese, chromium and molybdenum, and with the further proviso that, when a compound based on only ruthenium or rhodium or ruthenium and rhodium or nickel and rhodium is selected as component (a), the promoter (b) may be dispensed with.

    77.
    发明专利
    未知

    公开(公告)号：ES2135108T3

    公开(公告)日：1999-10-16

    申请号：ES95941717

    申请日：1995-12-16

    Applicant: BASF AG

    Inventor： SCHNURR WERNER ,  FISCHER ROLF ,  BASSLER PETER ,  HARDER WOLFGANG

    IPC: C07B61/00 ,  C07C253/30 ,  C07C255/24

    Abstract: Aliphatic alpha,omega-aminonitriles are prepared by partial hydrogenation of aliphatic alpha,omega-dinitriles at elevated temperatures and superatmospheric pressure in the presence of a base and of a hydrogenation catalyst, by carrying out the hydrogenation in the presence of ammonia and lithium hydroxide or of a compound which gives lithium hydroxide during the hydrogenation.

    78.
    发明专利
    未知

    公开(公告)号：BR9711257A

    公开(公告)日：1999-08-17

    申请号：BR9711257

    申请日：1997-08-26

    Applicant: BASF AG

    Inventor： WEISS ROBERT ,  KELLER DIETER ,  PIPPER GUNTER ,  HARDER WOLFGANG ,  LUDWIG ALFONS ,  MOHSCHLADT RALF

    IPC: C08G69/00 ,  C08G69/04 ,  C08G69/08 ,  C08G69/28 ,  C08G69/36

    Abstract: A process for preparing a polyamide by reacting at least one aminonitrile with water comprises:(1) reacting at least one aminonitrile with water at a temperature from 100 to 360° C. and a pressure from 0.1 to 35x106 Pa to obtain a reaction mixture,(2) further reacting the reaction mixture at a temperature from 150 to 400° C. and a pressure which is lower than the pressure in step 1, the temperature and the pressure being selected so as to obtain a first gas phase and a first liquid or a first solid phase or a mixture of first solid and first liquid phase, and the first gas phase is separated from the first liquid or the first solid phase or from the mixture of first liquid and first solid phase, and(3) admixing the first liquid or the first solid phase or the mixture of first liquid and first solid phase with a gaseous or liquid phase comprising water at a temperature from 150 to 360° C. and a pressure from 0.1 to 30x106 Pa to obtain a product mixture.

    79.
    发明专利
    未知

    公开(公告)号：ES2130780T3

    公开(公告)日：1999-07-01

    申请号：ES96900564

    申请日：1996-01-04

    Applicant: BASF AG

    Inventor： DOSTALEK ROMAN ,  FISCHER ROLF ,  HARDER WOLFGANG ,  PAUL AXEL ,  PINKOS ROLF

    IPC: C07C29/88 ,  C07C31/20 ,  C07C55/14 ,  C07C59/01

    Abstract: PCT No. PCT/EP96/00023 Sec. 371 Date Jul. 1, 1997 Sec. 102(e) Date Jul. 1, 1997 PCT Filed Jan. 4, 1996 PCT Pub. No. WO96/20909 PCT Pub. Date Jul. 11, 1996Impurities are separated from aqueous solutions of 1,6-hexanediol or 1,6-hexanediol precursors, such as adipic and 6-hydroxycaproic acid, by a process which comprises adding at least one carboxylic acid to a solution (a) of 1,6-hexanediol and subjecting this solution (a) or a solution (b) containing carboxylic acid(s) as precursor(s) of 1,6-hexanediol to a heat treatment at temperatures above room temperature in the absence of hydrogen.

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