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    Method for producing alkylaryl compounds
    1.
    发明专利
    Method for producing alkylaryl compounds 未知

    公开(公告)号：ZA200604943B

    公开(公告)日：2007-12-27

    申请号：ZA200604943

    申请日：2006-06-15

    Applicant: BASF AG

    Inventor： BOTTKE NILS ,  TROPSCH JURGEN ,  NARBESHUBER THOMAS ,  STEPHAN JURGEN ,  ROPER MICHAEL ,  STEINBRENNER ULRICH ,  BENFER REGINA ,  HEIDEMANN THOMAS

    IPC: C07C20090101 ,  C07C2/66 ,  C07C303/06 ,  C07C309/31 ,  C11D1/22 ,  C11D11/04

    Abstract: The preparation of alkylaryl compounds takes place by a) reaction of a C 4 /C 5 -olefin mixture over a metathesis catalyst to prepare a C 4-8 -olefin mixture comprising 2-pentene, and optional removal of the C 4-8 -olefin mixture, b) removal of from 5 to 100% of the 2-pentene present in stage a) and subsequent reaction over an isomerization catalyst to give a mixture of 2-pentene and 1-pentene which is returned to stage a), c) dimerization of the C 4-8 -olefin mixture obtained in stage b) following removal in the presence of a dimerization catalyst to give a mixture containing C 8-16 -olefins, removal of these C 8-16 -olefins and optional removal of a partial stream thereof, d) reaction of the c 8-16 -olefin mixtures obtained in stage c) or of the partial stream with an aromatic hydrocarbon in the presence of an alkylation catalyst to form alkyl aromatic compounds where, prior to the reaction, 0 to 60% by weight, based on the c 8-16 -olefin mixtures obtained in stage c), of linear olefins may additionally be added, e) optional sulfonation of the alkyl aromatic compounds obtained in stage d) and neutralization to give alkylarylsulfonates, where, prior to the sulfonation, 0 to 60% by weight, based on the alkyl aromatic compounds obtained in stage d), of linear alkylbenzenes may additionally be added if no admixing has taken place in stage d), f) optional mixing of the alkylarylsulfonates obtained in stage e) with 0 to 60% by weight, based on the alkylarylsulfonates obtained in stage e), of linear alkylarylsulfonate, if no admixing has taken place in stages d) and e).

    PROCEDIMIENTO PARA LA PRODUCCION DE 1,6-HEXANODIOL.
    2.
    发明专利
    PROCEDIMIENTO PARA LA PRODUCCION DE 1,6-HEXANODIOL. 未知

    公开(公告)号：ES2270165T3

    公开(公告)日：2007-04-01

    申请号：ES03799469

    申请日：2003-12-03

    Applicant: BASF AG

    Inventor： FISCHER ROLF-HARTMUTH ,  KRUG THOMAS ,  HAUNERT ANDREA ,  ROPER MICHAEL ,  SIRCH TILMAN ,  STUER WOLFRAM

    IPC: C07C29/17 ,  C07C29/149 ,  C07C31/20 ,  C07C67/347 ,  C07C69/593

    Abstract: Procedimiento para la producción de 1,6-hexanodiol con una pureza de >_99,5% en peso mediante dimerización catalítica de ésteres del ácido acrílico e hidrogenación catalítica de los diésteres del ácido hexenodioico así obtenidos para dar 1,6-hexanodiol, en el que a) se dimeriza el éster del ácido acrílico de C1 a C8 en presencia al menos de un compuesto de rodio para dar mezclas predominantemente de diésteres de los ácidos 2 y 3-hexenodioico, b) se hidrogena el producto de salida de la dimerización obtenido en presencia de catalizadores que contienen predominantemente cobre como componente de hidrogenación, libres de cromo y c) se purifica el 1,6-hexanodiol bruto así obtenido mediante la destilación fraccionada.

    METHOD FOR PRODUCING DIALDEHYDES AND/OR ETHYLENICALLY UNSATURATED MONOALDEHYDES BY HYDROFORMYLATING ETHYLENICALLY UNSATURATED COMPOUNDS
    3.
    发明专利
    METHOD FOR PRODUCING DIALDEHYDES AND/OR ETHYLENICALLY UNSATURATED MONOALDEHYDES BY HYDROFORMYLATING ETHYLENICALLY UNSATURATED COMPOUNDS 未知

    公开(公告)号：AU2003267348A1

    公开(公告)日：2004-04-08

    申请号：AU2003267348

    申请日：2003-09-12

    Applicant: BASF AG

    Inventor： SAVA XAVIER ,  LOBER OLIVER ,  BEY OLIVER ,  STEPHAN JURGEN ,  HAESE FRANK ,  VOLLAND MARTIN ,  AHLERS WOLFGANG ,  EBEL KLAUS ,  PACIELLO ROCCO ,  ROPER MICHAEL ,  MACKEWITZ THOMAS ,  BOHM VOLKER

    IPC: C07B61/00 ,  C07C45/50 ,  C07C47/12 ,  C07F9/572 ,  C07F9/655 ,  C07F9/6558 ,  C07F9/6584 ,  C07F9/6596 ,  C07C47/21

    Abstract: A process for the production of dialdehydes and/or ethylenically unsaturated monoaldehydes by reaction of at least one compound having at least two ethylenically unsaturated double bonds with carbon monoxide and hydrogen in the presence of a hydroformylation catalyst comprising at least one complex of a Group VIII metal with at least one ligand comprising a pnicogen chelate compound. A process for the production of dialdehydes and/or ethylenically unsaturated monoaldehydes by reaction of at least one compound having at least two ethylenically unsaturated double bonds with carbon monoxide and hydrogen in the presence of a hydroformylation catalyst comprising at least one complex of a Group VIII metal with at least one ligand comprising a pnicogen chelate compound of formula (1). Q = bridging group of formula (2); A1, A2 = O, S, SiRaRb, NRc or CRdRe; Ra-Rc = H, alkyl, cycloalkyl, heterocycloalkyl, aryl or heteroaryl; Rd, Re = H, alkyl, cycloalkyl, heterocycloalkyl, aryl or heteroaryl or two Rd groups and/or two Re groups form an intermolecular bridging group D; D = bivalent bridging group of formula (3)-(6); R9,R10 = H, alkyl, cycloalkyl, aryl, halo, trifluoromethyl, carboxyl, carboxylate or cyano or together form a 3-4C alkylene bridge; R11-R14 = H, alkyl, cycloalkyl, aryl, halo, trifluoromethyl, COOH, carboxylate, cyano, alkoxy, SO3H, sulfonate, NE1E2, alkylene-NE1E2E3+X-, acyl or nitro; C = 0 or 1; Y = chemical bond; RI-RVI = H, alky, cycloalkyl, heterocycloalkyl, aryl or heteroaryl; COORf, COO-M+, SO3Rf, SO3-M+, NE1E2, NE1E2E3+X-, alkylene-NE1E2E3+X-, ORf, SRf, (CHRgCH2O)xRf, (CH2N(E1))xRf, (CH2CH2N(E1))xRf, halo, trifluoromethyl, nitro, acyl or cyano or 2 neighboring groups, together with two neighboring C atoms of the benzene ring to which they are bonded form a condensed ring system of 1-3 further rings; Rf, E1-E3 = H, alkyl, cycloalkyl or aryl; R9 = H, methyl or ethyl; M+ = cation, X-=anion; x = 1-120; a, b = 0 or 1; Pn = P, As or Sb; R1-R4 = heteroaryl, heteroaryloxy, alkyl, alkoxy, aryl, aryloxy, cycloalkyl, cycloalkoxy, heterocycloalkyl, heterocycloalkoxy or NE1E2 with the proviso that is R1 and R3 are bonded via the N atom to the pnicogen atom bonded pyrrole ring or R1 with R2 and/or R3 together with R4 form a divalent group E of formula Py-I-W or R1 and R2 and/or R3 and R4 form a bispyrrole group of formula Py-I-Py; Py = pyrrole group that is bonded via its N atom to Pn; I = chemical bond, O, S, SiRaRb, NRc, optionally substituted 1-10C alkylene or CRhCRi; W = cycloalkyl, cycloalkoxy, aryl, aryloxy, heteroaryl or heteroaryloxy; Rh and Ri = H, alkyl, cycloalkyl, heterocycloalkyl, aryl or heteroaryl

    4.
    发明专利
    未知

    公开(公告)号：ES2199546T3

    公开(公告)日：2004-02-16

    申请号：ES99904776

    申请日：1999-01-14

    Applicant: BASF AG

    Inventor： GEISSLER BERNHARD ,  ROPER MICHAEL ,  ZELLER EDGAR ,  PACIELLO ROCCO ,  DECKER JURGEN ,  VOSS HARTWIG

    IPC: B01J31/22 ,  B01J31/16 ,  B01J31/18 ,  B01J31/20 ,  C07B61/00 ,  C07C27/20 ,  C07C29/16 ,  C07C31/125 ,  C07C45/50 ,  C07C47/02 ,  C08G73/02

    Abstract: The invention relates to a method for the production of aldehydes or aldehydes and alcohols by hydroformylation of olefins in the presence of a complexing catalyst homogeneously dissolved in a reaction mixture, containing a metal of Group VIIIa of the periodic table of the elements and a phosphorus-free, polydentate nitrogen compound suitable for complex formation as ligand at temperatures ranging from 50 to 100° C. and pressures from 20 to 1,000 bar and recirculating the catalyst complex in the hydroformylation reaction, wherein a) derivatized polyamines are used that are substantially non-water soluble and suitable for complex formation and have a mean molecular weight of more than 1,000 Dalton and at least 10 nitrogen atoms; b) the catalyst complex remaining in the bottom of the distillation column and the excess ligands obtained from the reaction mixture are recirculated totally or partially in the hydroformylation once the hydroformylation reaction and the separation or partial separation by distillation of the aldehydes and the alcohols has been completed; c) continues or at least batchwise evacuation of at least part of the high boiler from the bottom of the distillation of the reaction mixture is then carried out.

    9.
    发明专利
    未知

    公开(公告)号：ES2163191T3

    公开(公告)日：2002-01-16

    申请号：ES97938853

    申请日：1997-07-23

    Applicant: BASF AG

    Inventor： FISCHER ROLF ,  PACIELLO ROCCO ,  ROPER MICHAEL ,  SCHNURR WERNER

    IPC: B01J23/44 ,  B01J23/46 ,  B01J23/75 ,  C07B61/00 ,  C07C209/48 ,  C07C209/60 ,  C07C211/12 ,  C07C253/30 ,  C07C255/24

    Abstract: PCT No. PCT/EP97/03987 Sec. 371 Date Feb. 1, 1999 Sec. 102(e) Date Feb. 1, 1999 PCT Filed Jul. 23, 1997 PCT Pub. No. WO98/05631 PCT Pub. Date Feb. 12, 1998The invention concerns a process for the preparation of 6-aminocapronitrile or 6-aminocapronitrile-hexamethylene diamine mixtures by: a) reacting 5-formylvaleronitrile with ammonia and hydrogen in the presence of hydrogenation catalysts selected from the group consisting of metals or metal compounds rhenium, copper and elements of group VIII of the periodic table of elements, a hydrogenation discharge product being obtained; and b) extracting from the hydrogenation discharge product 6-aminocapronitrile and optionally hexamethylene diamine, provided that the hydrogenation catalyst does not contain copper, nickel or copper and nickel as it's only components.

    10.
    发明专利
    未知

    公开(公告)号：ID30314A

    公开(公告)日：2001-11-22

    申请号：ID20012126

    申请日：2000-03-31

    Applicant: BASF AG

    Inventor： MAAS HEIKO ,  ROPER MICHAEL

    IPC: B01J23/46 ,  B01J31/22 ,  C07B61/00 ,  C07C41/30 ,  C07C43/15 ,  C11D1/72

    Abstract: The invention relates to a method for producing alkapolyenyl compounds by effecting the homogeneously catalyzed reaction of 1-substituted alka-2,7-dienes of formula (I) and/or of 3-substituted alka-1,7-dienes of formula (II), in particular, octa-2,7-dienylethers, in the presence of rhodium compounds, whereby at least one mineral acid and/or at least one inorganic halogenide is dissolved in the reaction mixture. In this method, mineral acids and/or inorganic halogenides are used as cocatalysts which are dissolved in the reaction mixture. The products which are produced by using the inventive method are used as intermediate products in the production of surface-active materials.

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