11.
    发明专利
    未知

    公开(公告)号:DE2801031A1

    公开(公告)日:1978-08-17

    申请号:DE2801031

    申请日:1978-01-11

    Applicant: IBM

    Abstract: An NMR (nuclear magnetic resonance) spectrometer has a permanent magnet provided with a field coil. A lock system cyclically pulses a deuterium lock sample to produce a FID (free induction decay) signal that is analyzed by measuring the time interval during which the FID signal crosses the zero axis a predetermined number of times. The measured interval is compared to a predetermined interval or set point, and the current through the field coil is adjusted in the direction tending to correct the field strength so as to maintain the measured interval equal to the preset interval. Such measurement, comparison and adjustment are done several times each second. When the sample is removed, the lock system retains the last field setting achieved with the sample.

    12.
    发明专利
    未知

    公开(公告)号:DE2755091A1

    公开(公告)日:1978-07-06

    申请号:DE2755091

    申请日:1977-12-10

    Applicant: IBM

    Abstract: A method is described for the quantitative analysis of a solution in which the solvent produces a nuclear magnetic resonant (NMR) spectral peak that dominates the system. A first spectrum containing the peak is made by operation of a nuclear magnetic resonant spectrometer at a first gain setting. The NMR apparatus is a pulse-modulated, Fourier-transform type spectrometer. A second spectrum is produced in which a 180 DEG pulse is applied to invert the spectral component magnetization followed after a period of time by a 90 DEG pulse. The period of time is sufficient to allow the solvent or component producing the unwanted peak to relax from the inverted state to a point where there is minimum magnetization along the longitudinal axis. At this point, in many solutions the other components have completely relaxed so that the 90 DEG pulse produces a free induction decay signal which, after undergoing the Fourier-transformation, yields a spectrum that does not include any significant peak due to the solvent. Thereafter, the quantitative analysis is performed by measuring the areas under the respective component peaks and simultaneously solving a series of equations in which the weight of the various components is proportional to the respective areas under the peaks and to the gain settings of the spectrometer.

    13.
    发明专利
    未知

    公开(公告)号:DE69324439D1

    公开(公告)日:1999-05-20

    申请号:DE69324439

    申请日:1993-10-29

    Applicant: IBM

    Abstract: A lithographic imaging process is provided for use in the manufacture of integrated circuits. A substrate is coated with a polymeric film comprising a vinyl polymer, a photosensitive acid generator, and acid labile groups. It is then heated to typically just above the glass transition temperature of the polymer, but below the cleavage temperature of the acid labile groups. The film is then expose imagewise to radiation to generate free acid, and the film is once more heated, again to typically just above the glass transition temperature of the polymer, but below the cleavage temperature of the acid labile groups. Finally the image is developed. The process provides protection to the photoresist film from airborne chemical contaminants.

    17.
    发明专利
    未知

    公开(公告)号:IT1150095B

    公开(公告)日:1986-12-10

    申请号:IT2672080

    申请日:1980-12-18

    Applicant: IBM

    Abstract: A method and an apparatus for line narrowing in nuclear magnetic resonance (NMR) studies in solids is described. The method employs quasi-continuous amplitude modulation of an rf field (10) wherein the field is eliminated at intervals (18) for short periods of time at or about the time when the amplitude for both the maximum and minimum approach zero, these intervals creating windows where the NMR signal can be observed.

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