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    제초활성을 갖는9-(5-이속사졸린메톡시페닐)이미노-8-치아-1,6-디아자비시클로[4.3.0]노난-7-온 유도체
    31.
    发明公开
    제초활성을 갖는9-(5-이속사졸린메톡시페닐)이미노-8-치아-1,6-디아자비시클로[4.3.0]노난-7-온 유도체 失效
    9-（5-异丙氧基乙基苯基）亚氨基-8-三噻基-1,6-二氮杂双环[4.3.0 |具有除草活性的非 - 7-酮衍生物

    公开(公告)号：KR1020040017892A

    公开(公告)日：2004-03-02

    申请号：KR1020020049819

    申请日：2002-08-22

    Applicant: 한국화학연구원

    Inventor： 유응걸 ,  전동주 ,  김형래 ,  송종환 ,  박관용 ,  하진열 ,  김진석

    IPC: C07D495/04

    Abstract: PURPOSE: Provided are derivatives of 9-(5-isoxazolinemethoxyphenyl)imino-8-thia-1.6-diazabicylco£4.3.0|nonane-7-one, represented by the formula(1) and herbicides containing them as active ingredients and having excellent herbicidal activity and selectivity when applied to a rice paddy. CONSTITUTION: Derivatives are represented by the formula(1), wherein R is C1-C6 alkyl, phenyl or substituted phenyl, wherein substituents are 1-3 of halogen atom, C1-C3 alkyl, C1-C3 alkoxy, C1-C3 haloalkyl, cyano, nitro, carboxyl and esters of carboxy acid.

    Abstract translation: 目的：提供由式（1）表示的9-（5-异恶唑啉甲氧基苯基）亚氨基-8-硫杂-1,6-二氮杂双环[4.3.0]壬烷-7-酮和含有它们作为活性成分并具有优异的除草剂的衍生物 施用于水稻时的除草活性和选择性。 构成：衍生物由式（1）表示，其中R是C1-C6烷基，苯基或取代的苯基，其中取代基是1-3的卤素原子，C1-C3烷基，C1-C3烷氧基，C1-C3卤代烷基， 氰基，硝基，羧基和羧酸的酯。

    3-클로로-2-(4-클로로-2-플루오로-5-히드록시페닐)-4,5,6,7-테트라히드로-2Ｈ-인다졸의 제조방법
    32.
    发明公开
    3-클로로-2-(4-클로로-2-플루오로-5-히드록시페닐)-4,5,6,7-테트라히드로-2Ｈ-인다졸의 제조방법 失效
    制备3-氯-2-（4-氯-2-氟-5-羟基苯基）-4,5,6,7-四氢-2H-吲哚的方法

    公开(公告)号：KR1020030095677A

    公开(公告)日：2003-12-24

    申请号：KR1020020033207

    申请日：2002-06-14

    Applicant: 한국화학연구원

    Inventor： 유응걸 ,  전동주 ,  김형래 ,  송종환 ,  박관용

    IPC: C07D231/54

    Abstract: PURPOSE: A process for preparing 3-chloro-2- (4-chloro-2-fluoro-5-hydroxyphenyl)- 4,5,6,7-tetrahydro-2H-indazole is provided, thereby improving its preparation yield and converting by-products of the preparation into starting material. CONSTITUTION: A process for preparing 3-chloro-2- (4-chloro-2-fluoro-5-hydroxyphenyl)- 4,5,6,7-tetrahydro-2H-indazole of the formula 1 comprises the steps of: reacting 2- (2-fluoro-4-chloro-5-hydroxyphenyl)- 2,3a,4,5,6,7- hexahydroindazole-3-one of the formula 2 with phosgene; concentrating the phosgene reaction mixture under reduced pressure; dissolving the concentrate in an organic solvent; adding ammonia water or hydroxide solution to the organic solvent and filtering solids; and distilling the filtrated solution, wherein the organic solvent is ethylacetate; the addition of ammonia water or hydroxide solution is carried out at room temperature; the solids are mainly constituted of a compound of the formula 2, and the by-products of the reaction include a dimer represented by the formula 3a, 3b or 3c.

    Abstract translation: 目的：提供3-氯-2-（4-氯-2-氟-5-羟基苯基）-4,5,6,7-四氢-2H-吲唑的制备方法，从而提高其制备产率，并通过 - 制备成原料的产品。 构成：式1的3-氯-2-（4-氯-2-氟-5-羟基苯基）-4,5,6,7-四氢-2H-吲唑的制备方法包括以下步骤：使2 - （2-氟-4-氯-5-羟基苯基）-2,3a，4,5,6,7-六氢吲唑-3-酮与光气; 在减压下浓缩光气反应混合物; 将浓缩物溶解在有机溶剂中; 向有机溶剂中加入氨水或氢氧化物溶液并过滤固体; 并蒸馏过滤的溶液，其中有机溶剂是乙酸乙酯; 在室温下加入氨水或氢氧化钠溶液; 固体主要由式2的化合物构成，反应的副产物包括由式3a，3b或3c表示的二聚体。

    이속사졸기로 치환된 신규한 광변색성 디아릴에텐계 화합물
    33.
    发明公开
    이속사졸기로 치환된 신규한 광변색성 디아릴에텐계 화합물 失效
    采用ISOXAZOL集团取代的新型光致变色二氧化钛

    公开(公告)号：KR1020020071408A

    公开(公告)日：2002-09-12

    申请号：KR1020010011544

    申请日：2001-03-06

    Applicant: 한국화학연구원

    Inventor： 김은경 ,  조성윤 ,  전동주 ,  김영미

    IPC: C07D413/14

    CPC classification number: C07D413/14 ,  C07D333/56 ,  C07D333/58 ,  C08K5/0041 ,  C08K5/353

    Abstract: PURPOSE: Provided is a novel photochromic diarylethene substituted with isoxazol group. Therefore, the photochromic diarylethene is excellent in dispersion with fluoro diacrylate monomer capable of being photopolymerized and a thin film manufactured therefrom has excellent photochromic property when irradiating UV and mechanical strength. CONSTITUTION: The novel photochromic diarylethene substituted with isoxazol group is represented by the formula(1) and manufactured by the steps of: formylating diarylethene compound of the formula(2); adding NH2OH·HCl and basic solution sequentially then adding N-chlorosuccin imide(NSC); and adding R2 substituted acetylene compound and basic catalyst.

    Abstract translation: 目的：提供用异恶唑基取代的新型光致变色二烯丙烯。 因此，光致变色二芳基烯与能够光聚合的氟二丙烯酸酯单体的分散性优异，并且由其制造的薄膜在照射UV和机械强度时具有优异的光致变色性。 构成：由异恶唑基取代的新型光致变色二芳基乙烯由式（1）表示，通过以下步骤制备：将式（2）的二芳基乙烯化合物酰化; 依次加入NH2OH·HCl和碱性溶液，然后加入N-氯琥珀酰亚胺（NSC）; 并加入R2取代的乙炔化合物和碱性催化剂。

    제초활성을 갖는 5-벤질옥시메틸-1,2-이속사졸린 유도체화합물
    35.
    发明公开
    제초활성을 갖는 5-벤질옥시메틸-1,2-이속사졸린 유도체화합물 有权
    具有除草活性的5-苄氧基甲基-1,6-异恶唑烷酮衍生物

    公开(公告)号：KR1020020019750A

    公开(公告)日：2002-03-13

    申请号：KR1020000052917

    申请日：2000-09-07

    Applicant: 한국화학연구원

    Inventor： 유응걸 ,  김형래 ,  전동주 ,  송종환 ,  김경만 ,  이정노 ,  김형철 ,  홍경식

    IPC: A01N43/80

    CPC classification number: A01N43/80

    Abstract: PURPOSE: Provided is 5-benzyloxymethyl-1,2-isoxazoline derivative which has an excellent herbicidal activity. Also, provided are its manufacturing method and herbicides containing the derivative as an active ingredient. CONSTITUTION: 5-benzyloxymethyl-1,2-isoxazoline derivative is represented by the formula(I), wherein X1, X2 and X3 individually represent hydrogen, methyl group, ethyl group, halogen group, methoxy group or nitro group (provided that it is an exception that X1, X2 and X3 are decimals all together); Y1, Y2 and Y3 are individually hydrogen or fluorine.

    Abstract translation: 目的：提供具有优异除草活性的5-苄氧基甲基-1,2-异恶唑啉衍生物。 此外，其制造方法和含有该衍生物作为活性成分的除草剂。 构成：5-苄氧基甲基-1,2-异恶唑啉衍生物由式（I）表示，其中X1，X2和X3各自表示氢，甲基，乙基，卤素基，甲氧基或硝基（条件是它是 一个例外，X1，X2和X3都是小数） Y1，Y2和Y3分别为氢或氟。

    전이금속 함유 전구체, 이의 제조방법 및 이의 용도
    37.
    发明公开
    전이금속 함유 전구체, 이의 제조방법 및 이의 용도 有权
    含过渡金属的前体及其制备方法和用途

    公开(公告)号：KR1020170037102A

    公开(公告)日：2017-04-04

    申请号：KR1020150136231

    申请日：2015-09-25

    Applicant: 한국화학연구원

    Inventor： 박보근 ,  정택모 ,  김창균 ,  전동주 ,  한정환 ,  한성호 ,  이선주

    IPC: C07F15/06 ,  C07F13/00 ,  H01M4/525 ,  H01M4/505

    Abstract: 본발명은전이금속함유전구체, 이의제조방법및 이를이용하여박막을제조하는방법에관한것으로, 본발명에따른전이금속함유전구체는열적안정성과휘발성이개선되어낮은온도에서도쉽게양질의코발트산화물또는망간산화물을포함하는박막의제조가가능하다.

    Abstract translation: 本发明涉及含有过渡金属的前体，其制备方法以及使用该前体制备薄膜的方法，其中根据本发明的含过渡金属的前体具有改进的热稳定性和挥发性， 可以制造含有氧化物的薄膜。

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